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Particle size and packing characterization by diffuse light transmission

Particuology 2012年第5期10卷 619-627页

作者： henrik ehlers Jyrki Heinmki Jouko Yliruusi Division of Pharmaceutical Technology Faculty of Pharmacy P.O. Box 56 (Viikinkaari 5 E) FI-00014 University of Helsinki Finland Pharmaceutical Sciences Laboratory Department of Biosciences bo Akademi University BioCity Artillerigatan 6 20520 Turku Finland Department of Pharmacy Faculty of Medicine University of Tartu Nooruse 1 50411 Tartu Estonia

Particle size, packing density and blend composition of glass ballotini, microcrystalline cellulose pellets and theophylline granules were studied by diffuse light transmission. Diffuse visible light was directed to the sample and the intensity of the light transmitted to the opposite side of the sample was measured through a diffusing lens using a phototransistor, Light transmission was found to decrease with decreasing particle size and with increasing packing density, There was a correlation, though somewhat irregular, between light transmission and particle size for glass ballotini and microcrystalline cellulose pellets, and a strong near-linear correlation between light transmission and particle size for theophylline granules, The effect of packing density on light transmission was significant, Differentiating the composition of binary blends of microcrystalline cellulose pellets and glass ballotini and blends of theophylline granules was found possible on the basis of light transmission, The method proposed showed potential as a rapid, simple and inexpensive analytical tool for basic process diagnostics,

关键词： Light transmissionParticle sizePacking densityConvectionSegregation

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Advanced control and modeling of deposition processes

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Chinese Optics Letters 2013年第13期11卷 30-35页

作者： Detlev Ristau henrik ehlers Centre of Quantum Engineering and Space-Time Research Hannover Germany Department of Laser Components Laser Zentrum Hannover e.V. Hannover Germany

During the last decade, striking improvements could be achieved for the precise control of deposition processes in optical coating technology. For example, as a consequence of enormous progresses in measure- ment and computer technology, direct optical monitoring in a broad spectral range can be considered as a common tool in many production environments nowadays. Besides the development of the corresponding hardware and measurement channels, advanced approaches for the evaluation of the acquired data and new multiple sensor monitoring strategies moved into the focus of modern research on the way towards de- terministic deposition techniques. In this context, also innovative concepts for the simulation of deposition processes to forecast the result for a specified coating design and automatic online correction algorithms gained of importance to reduce the risk of failure in coating production. The present contribution will be dedicated to selected aspects in this field, especially addressing broad band optical monitoring systems. A short review on examples for existing hardware configurations and software tools will be presented illus- trating the advantages of modern process control techniques. Novel approaches based on the modeling of thin film growth are discussed as an additional strategy to improve the predictability of coating processes.

关键词： 310.1860 Deposition and fabrication 310.6845 Thin film devices and applications 280.4788 Optical sensing and sensors

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