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Research on thermal insulation materials properties under HTHP conditions for deep oil and gas reservoir rock ITP-Coring

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Petroleum Science 2024年第4期21卷 2625-2637页

作者： Zhi-Qiang he he-ping xie Ling Chen Jian-ping Yang Bo Yu Zi-Jie Wei Ming-Zhong Gao State Key Laboratory of Intelligent Construction and healthy Operation and Maintenance of Deep Underground Engineering College of Water Resource and HydropowerSichuan UniversityChengdu610065SichuanChina Guangdong Provincial Key Laboratory of Deep Earth Sciences and Geothermal Energy Exploitation and Utilization Institute of Deep Earth Sciences and Green EnergyCollege of Civil and Transportation EngineeringShenzhen UniversityShenzhen518060GuangdongChina School of Mechanical Engineering Sichuan UniversityChengdu610065SichuanChina College of Polymer Science and Engineering Sichuan UniversityChengdu610065SichuanChina

Deep oil and gas reservoirs are under high-temperature conditions,but traditional coring methods do not consider temperature-preserved measures and ignore the influence of temperature on rock porosity and permeability,resulting in distorted resource *** development of in situ temperaturepreserved coring(ITP-Coring)technology for deep reservoir rock is urgent,and thermal insulation materials are ***,hollow glass microsphere/epoxy resin thermal insulation materials(HGM/EP materials)were proposed as thermal insulation *** materials properties under coupled hightemperature and high-pressure(HTHP)conditions were *** results indicated that high pressures led to HGM destruction and that the materials water absorption significantly increased;additionally,increasing temperature accelerated the *** temperatures directly caused the thermal conductivity of the materials to increase;additionally,the thermal conduction and convection of water caused by high pressures led to an exponential increase in the thermal *** temperatures weakened the matrix,and high pressures destroyed the HGM,which resulted in a decrease in the tensile mechanical properties of the *** materials entered the high elastic state at 150℃,and the mechanical properties were weakened more obviously,while the pressure led to a significant effect when the water absorption was above 10%.Meanwhile,the tensile strength/strain were 13.62 MPa/1.3%and 6.09 MPa/0.86%at 100℃ and 100 MPa,respectively,which meet the application requirements of the self-designed coring ***,K46-f40 and K46-f50 HGM/EP materials were proven to be suitable for ITP-Coring under coupled conditions below 100℃ and 100 *** further improve the materials properties,the interface layer and EP matrix should be *** results can provide references for the optimization and engineering application of materials and thus technical support for deep oil and gas resourc

关键词： Deep oil and gas reservoir rock In situ temperature-preserved coring(ITPCoring) Hollow glass microsphere/epoxy resin thermal insulation materials(HGM/EP materials) High-temperature and high-pressure(HTHP) Physical and mechanical properties

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The role of natural fracture activation in hydraulic fracturing for deep unconventional geo-energy reservoir stimulation

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Petroleum Science 2023年第4期20卷 2141-2164页

作者： Jun Wang he-ping xie Stephan KMatthai Jian-Jun Hu Cun-Bao Li Guangdong Provincial Key Laboratory of Deep Earth Sciences and Geothermal Energy Exploitation and Utilization Institute of Deep Earth Sciences and Green EnergyShenzhen UniversityShenzhen518060GuangdongPR China Shenzhen Key Laboratory of Deep Engineering Sciences and Green Energy College of Civil and Transportation EngineeringShenzhen UniversityShenzhen518060GuangdongPR China Department of Infrastructure Engineering University of MelbourneMelbourneVIC3010Australia MOE Laboratory of Deep Earth Science and Engineering Sichuan UniversityChengdu610065SichuanPR China

The presence of sealed or semi-sealed,multiscale natural fracture systems appears to be crucial for the successful stimulation of deep *** explore the reaction of such systems to reservoir stimulation,a new numerical simulation approach for hydraulic stimulation has been developed,trying to establish a realistic model of the physics *** new model successfully reproduces dynamic fracture activation,network generation,and overall reservoir permeability *** outputs indicate that natural fractures facilitate stimulation far beyond the near-wellbore area,and can significantly improve the hydraulic conductivity of unconventional geo-energy *** to our model,the fracture activation patterns are jointly determined by the occurrence of natural fractures and the in situ ***-density natural fractures,high-fluid pressure,and low effective stress environments promote the formation of complex fracture networks during *** or multicluster fracturing treatments with an appropriate spacing also increase the stimulated reservoir area(SRA).The simulation scheme demonstrated in this work offers the possibility to elucidate the complex multiphysical couplings seen in the field through detailed site-specific modeling.

关键词： Natural fractures DFM Unconventional geo-energy reservoir Fracture reactivation Hydraulic stimulation

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In-situ pressure-preserved coring for deep exploration:Insight into the rotation behavior of the valve cover of a pressure controller

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Petroleum Science 2023年第4期20卷 2386-2398页

作者： Da Guo he-ping xie Ling Chen Zhong-Ya Zhou he-ping Lu Lin Dai Ding-Ming Wang Tian-Yu Wang Ju Li Zhi-Qiang he Yun-Qi Hu Ming-Zhong Gao School of Mechanical Engineering Sichuan UniversityChengduSichuan610065China MOE Key Laboratory of Deep Underground Science and Engineering College of Water Resource and HydropowerSichuan UniversityChengduSichuan610065China Guangdong Provincial Key Laboratory of Deep Earth Sciences and Geothermal Energy Exploitation and Utilization Institute of Deep Earth Sciences and Green EnergyCollege of Civil and Transportation EngineeringShenzhen UniversityShenzhenGuangdong518060China Petroleum Engineering Technology Research Institute of Sinopec Jianghan Oilfield Company WuhanHubei430035China

In-situ pressure-preserved coring(IPP-Coring)is considered to be the most reliable and efficient method for the identification of the scale of oil and gas *** IPP-Coring,because the rotation behavior of the pressure controller valve cover in different medium environments is unclear,interference between the valve cover and inner pipe may occur and negatively affect the IPP-Coring success *** address this issue,we conducted a series of indoor experiments employing a high-speed camera to gain greater insights into the valve cover rotation behavior in different medium environments,e.g.,air,water,and simulated drilling *** results indicated that the variation in the valve cover rotation angle in the air and fluid environments can be described by a one-phase exponential decay function with a constant time parameter and by biphasic dose response function,*** rotation behavior in the fluid environments exhibited distinct elastic and gravitational acceleration *** the fluid environments,the density clearly impacted the valve cover closing time and rotation behavior,whereas the effect of viscosity was very *** can be attributed to the negligible influence of the fluid viscosity on the drag coefficient found in this study;meanwhile,the density can increase the buoyancy and the time period during which the valve cover experienced a high drag *** these results,control schemes for the valve cover rotation behavior during IPP-Coring were proposed for different layers and geological conditions in which the different drilling fluids should be used,e.g.,the use of a high-density valve cover in high-pore pressure layers.

关键词： In-situ coring Pressure coring Pressure controller Rotation behavior Drilling fluid

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Hollow glass microspheres/silicone rubber composite materials toward materials for high performance deep in-situ temperaturepreserved coring

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Petroleum Science 2022年第1期19卷 309-320页

作者： Jian-ping Yang Ling Chen Xiao-Bin Gu Zhi-Yu Zhao Cheng-Hang Fu Dong-Sheng Yang Dong-Zhuang Tian Zhi-Sheng Chen he-ping xie College of Polymer Science and Engineering Sichuan UniversityChengdu610065China Guangdong Provincial Key Laboratory of Deep Earth Sciences and Geothermal Energy Exploitation and Utilization Institute of Deep Earth Sciences and Green EnergyCollege of Civil and Transportation EngineeringShenzhen UniversityShenzhen518060China School of Mechanical Engineering Sichuan UniversityChengdu610065China Jinshi Drilltech Company Limited Tangshan063004Hebei Institute of New Energy and Low-Carbon Technology Sichuan UniversityChengdu610065China College of Water Resource&Hydropower Sichuan UniversityChengdu610065China Xi'an Research Institute China Coal Technology&Engineering Group CorpXi'an710077China

Deep petroleum resources are stored under high temperature and pressure conditions,with the temperature having a significant influence on the properties of *** in-situ temperature-preserved coring(ITP-coring)devices were developed to assess deep petroleum reserves ***,hollow glass microspheres(HGMs)/silicone rubber(SR)composites that exhibit excellent thermal insulation properties were prepared as thermal insulation materials for deep ITP-coring *** mechanism and process of heat transfer in the composites were explored,as well as their other *** results show that the HGMs exhibit good compatibility with the SR *** the volume fraction of the HGMs is increased to 50%,the density of the HGMs/SR composites is reduced from 0.97 to 0.56 g/cm^(3).The HGMs filler introduces large voids into the composites,reducing their thermal conductivity to 0.11 W/m·*** addition of HGMs into the composites further enhances the thermal stability of the SR,wherein the higher the HGMs filler content,the better the thermal stability of the *** significantly enhance the mechanical strength of the *** increase the compressive strength of the composites by 828%and the tensile strength by 164%.Overall,HGMs improve the thermal insulation,pressure resistance,and thermal stability of HGMs/SR composites.

关键词： In-situ temperature-preserved coring(ITP-coring) Deep in-situ conditions Thermal insulation materials HGMs/SR composites

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Magnetically controlled self-sealing pressure-preserved coring technology

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Petroleum Science 2024年第5期21卷 3464-3481页

作者： Gui-Kang Liu he-ping xie Cong Li Zhen-Xi You Xiao-Jun Shi Jian-Jun Hu Ming-Zhong Gao State Key Laboratory of Intelligent Construction and healthy Operation and Maintenance of Deep Underground Engineering College of Water Resource and HydropowerSichuan UniversityChengdu610065SichuanChina Guangdong Provincial Key Laboratory of Deep Earth Sciences and Geothermal Energy Exploitation and Utilization Institute of Deep Earth Sciences and Green EnergyCollege of Civil and Transportation EngineeringShenzhen UniversityShenzhen518060GuangdongChina School of Mechanical Engineering Sichuan UniversityChengdu610065SichuanChina

Pressure-preserved coring is an effective means to develop deep resources. However, due to the complexity of existing pressure-preserved technology, the average success rate of pressure-preserved coring is low. In response, a novel in situ magnetically controlled self-sealing pressure-preserved coring technology for deep reserves has been proposed and validated. This innovative technology distinguishes itself from conventional methods by employing noncontact forces to replace traditional pretensioning mechanisms, thereby enhancing the mechanical design of pressure-preserved coring equipment and significantly boosting the fault tolerance of the technology. here, we report on the design,theoretical calculations, experimental validation, and industrial testing of this technology. Through theoretical and simulation calculations, the self-sealing composite magnetic field of the pressure controller was optimized. The initial pre-tensioning force of the optimal magnetic field was 13.05 N. The reliability of the magnetically controlled self-sealing pressure-preserved coring technology was verified using a self-developed self-sealing pressure performance testing platform, confirming the accuracy of the composite magnetic field calculation theory. Subsequently, a magnetically controlled self-triggering pressure-preserved coring device was designed. Field pressure-preserved coring was then conducted,preliminarily verifying the technology's effective self-sealing performance in industrial ***, the technology was analyzed and verified to be adaptable to complex reservoir environments with pressures up to 30 MPa, temperatures up to 80℃, and p H values ranging from 1 to 14. These research results provide technical support for multidirectional pressure-preserved coring, thus paving a new technical route for deep energy exploration through coring.

关键词： In situ pressure-preserved coring Magnetically controlled Self-sealing Magnetic design Deep earth exploration

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Optimal depth of in-situ pressure-preserved coring in coal seams considering roadway excavation and drilling disturbance

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Petroleum Science 2024年第5期21卷 3517-3534页

作者： Peng-Fei Cui De-Lei Shang Peng Chu Ju Li Da-Li Sun Tian-Yu Wang Ming-Zhong Gao he-ping xie State Key Laboratory of Intelligent Construction and healthy Operation and Maintenance of Deep Underground Engineering Institute of Deep Earth Sciences and Green EnergyShenzhen UniversityShenzhen518060GuangdongChina Guangdong Provincial Key Laboratory of Deep Earth Sciences and Geothermal Energy Exploitation and Utilization Shenzhen Key Laboratory of Deep Underground Engineering Sciences and Green EnergyCollege of Civil and Transportation EngineeringShenzhen UniversityShenzhen518060GuangdongChina State Key Laboratory of Hydraulics and Mountain River Engineering Sichuan UniversityChengdu610065SichuanChina School of Mechanical Engineering Sichuan UniversityChengdu610065SichuanChina Jinshi Drilltech Co. Ltd.Tangshan063004HebeiChina

Using pressure-preserved coring technique to determine in-situ gas content provides a more precise assessment of gas resource reserves and safeguard of mining safety in coal seams. How coring technique and depth affect the determination of gas content is unclear due to borehole zoning rupture caused by roadway excavation and drilling disturbance. To this end, a proposed coupling model of stress distribution and gas migration was simulated and validated by FLAC^(3D) and COMSOL Multiphysics considering superposition effects of roadway excavation and drilling disturbance. The findings indicate that the roadway surrounding rock displays distinct zoning features including stress relief zone, stress concentration zone that is composed of plastic zone, elastic zone, and original stress zone;and the broken situations depending on the borehole peeping are consistent with the corresponding simulation *** this basis, this study proposes a set of drilling coring depth calculation and prediction model for the gas desorption affected area under engineering disturbance. Optimal depth of coring drilling is not only approach to the in-situ coal bulk, but also can get the balance of the drilling workload and cost controlling. According to the typical mine site geological conditions and the numerical simulation results in this study, if the roadway excavation time is ~1 year, it is recommended that the pressure-preserved coring depth should be greater than 17 m.

关键词： In-situ fidelity coring In-situ pressure preserved coring Gas content Drilling disturbance Coring depth Excavation damage zone

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Influence of the mechanical properties of materials on the ultimate pressure-bearing capability of a pressure-preserving controller

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Petroleum Science 2024年第5期21卷 3558-3574页

作者： Xiao-Jun Shi he-ping xie Cong Li Gui-Kang Liu Zi-Jie Wei Tian-Yu Wang Ju Li Qiu-Yue Li State Key Laboratory of Intelligent Construction and healthy Operation and Maintenance of Deep Underground Engineering College of Water Resource and HydropowerSichuan UniversityChengdu610065SichuanChina Guangdong Provincial Key Laboratory of Deep Earth Sciences and Geothermal Energy Exploitation and Utilization Institute of Deep Earth Sciences and Green EnergyCollege of Civil and Transportation EngineeringShenzhen UniversityShenzhen518060GuangdongChina College of Mechanical Engineering Sichuan UniversityChengdu610065SichuanChina Jinshi Drilltech Co.Ltd. Tangshan063004HebeiChina

The pressure-preserving controller is the core part of deep in-situ pressure-preserving coring(IPP-Coring) system, and its pressure-preserving capability is the key to IPP-Coring technology. To achieve a good understanding of the influence of mechanical properties of materials on the ultimate pressure-bearing capability(UPB-Capability) of the pressure-preserving controller, the IPP-Coring experimental platform was developed to test the UPB-Capability of pressure-preserving controllers of four different materials. The experimental results show that the UPB-Capability of pressure-preserving controllers with different material varies greatly. A numerical model of the pressure-preserving controller was developed to study the influences of mechanical parameters of materials on the UPB-Capability of the pressurepreserving controller after the accuracy of the numerical model is verified by experiments. The results indicate that the yield strength(YS) and Poisson's ratio(PR) of the material have little effect on the UPB-Capability of the pressure-preserving controller, whereas the elastic modulus(EM) of the material has a significant effect. A generalized model of the UPB-Capability of the pressure-preserving controller is developed to reveal the mechanism of the influence of material properties on the UPB-Capability of the pressure-preserving controllers. Considering these results, the future optimization direction of the pressure-preserving controller and material selection scheme in practical engineering applications of the pressure-preserving controller are suggested.

关键词： In-situ pressure-preserving coring Pressure-preserving controller Material properties Ultimate pressure-bearing capability

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3D anisotropy in shear failure of a typical shale

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Petroleum Science 2023年第1期20卷 212-229页

作者： Zi-Dong Fan Li Ren he-ping xie Ru Zhang Cun-Bao Li Hui-Jun Lu An-Lin Zhang Qin Zhou Wei-Qiang Ling MOE Key Laboratory of Deep Earth Science and Engineering Sichuan UniversityChengduSichuan 610065China College of Architecture and Environment Sichuan UniversityChengduSichuan 610065China Institute of Deep Earth Sciences and Green Energy Shenzhen UniversityShenzhenGuangdong 518052China College of Water Resources and Hydropower Sichuan UniversityChengduSichuan 610065China

It is inadequate to study the shear failure anisotropy of shale in only 2D *** at a 3D analysis,a series of direct shear tests was conducted on Longmaxi shale with three typical bedding orientations:arrester,divider and short-transverse *** testing,acoustic emission(AE)and digital image correlation(DIC)techniques were simultaneously employed to monitor failure development,after testing,X-ray computed tomography(CT)scanning was adopted to acquire and reconstruct the fractures inside typical ruptured samples for more detailed *** results indicated that the shear strength parameters exhibited 3D anisotropies and those of the arrester sample did not have equivalent shear strength parameters to the shale *** maximum(minimum)shear strength and cohesion were obtained with the divider(short-transverse)orientation,and the internal friction angle reached its maximum(minimum)with the divider(arrester)*** the AE,DIC and CT techniques,four characteristic stress levels that can capture the progressive shear failure process of shale rocks were identified,and the onset and accelerated development of shear damage-induced dilation were observed at the crack initiation and coalesce stress thresholds,*** the crack coalescence stage,the dominated microcracking mechanism transferred from tensile-mode to *** the arrester and divider orientations,more tensile-mode AE events were generated due to the microcracking along the vertical *** with the divider samples,a more complex fracture network with a larger fracture area and volume was obtained in the arrester samples,whose strengths were smaller.

关键词： Shale Shear Acoustic emission Digital image correlation X-ray computed tomography Fracture network

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Therapeutic effect of traditional Chinese medicine on coagulation disorder and accompanying intractable jaundice in hepatitis B virus-related liver cirrhosis patients

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World Journal of Gastroenterology 2008年第39期14卷 6060-6064页

作者： Yang-Mei Li Hong-Zhi Yang Wei-Bing Guan Qian-Shan Ke Min Dai he-ping xie Shi-Jun Zhang Departmentof TCM The Third Affiliated Hospital of Sun Yat-Sen University 600# Tianhe Road Guangzhou 510630 Guangdong Province China Department of TCM The First Affiliated Hospital of Sun Yat-Sen University 58# Zhongshan Er Road Guangzhou 510080 Guangdong Province China

AIM： TO observe the therapeutic effects of new traditional Chinese medicine （TClVl） therapy on coagulation disorder and accompanying intractable jaundice in HBV-related liver cirrhosis patients. METHODS： Using stratified random sampling according to fibrinogen （Fib） levels, 145 liver cirrhosis patients due to hepatitis B complicated by coagulation disorder were treated. Of them, 70 in research group were treated with TCM by ＂nourishing yin, cooling blood and invigorating blood circulation＂ and Western medicine, 75 in control group were treated with conventional Western medicine. The indexes of liver function, coagulation function and bleeding events were observed and compared. RESULTS： The prothrombin time （PT） was shorter and the fibrinogen （Fib） level was higher in the research group than in the control group （Fib = 1.6-2.0 g/L, 1.1-1.5 g/L, and ≤ 1.0 g/L）. The total bilirubin （TBIL） level was significantly lower in the research group than in the control group, except for the subgroup of FIB ≤ 1.0 g/L. CONCLUSION： TCM therapy can improve coagulation fuction and decrease TBIL.

关键词： Combination of traditional Chinese and Western medicine Liver cirrhosis Coagulation disorder Nourishing yin Cooling blood and invigorating blood circulation

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Research on in-situ condition preserved coring and testing systems

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Petroleum Science 2021年第6期18卷 1840-1859页

作者： he-ping xie Tao Liu Ming-Zhong Gao Ling Chen Hong-Wei Zhou Yang Ju Feng Gao Xiao-Bo Peng Xiong-Jun Li Rui-Dong Peng Ya-Nan Gao Cong Li Zhi-Qiang he Ming-Qing Yang Zhi-Yu Zhao Guangdong Provincial Key Laboratory of Deep Earth Sciences and Geothermal Energy Exploitation and Utilization Institute of Deep Earth Sciences and Green EnergyCollege of Civil and Transportation EngineeringShenzhen UniversityShenzhen518060GuangdongChina Shenzhen Key Laboratory of Deep Underground Engineering Sciences and Green Energy Shenzhen UniversityShenzhen518060GuangdongChina MOE Key Laboratory of Deep Earth Science and Engineering College of Water Resource and HydropowerSichuan UniversityChengdu 610065SichuanChina School of Mechanical Engineering Sichuan UniversityChengdu610065SichuanChina Institute of New Energy and Low-Carbon Technology Sichuan UniversityChengdu610065SichuanChina State Key Laboratory of Coal Resources and Safe Mining China University of Mining and Technology(Beijing)Beijing100083China Frontier Science Research Center for Fluidized Mining of Deep Underground Resources China University of Mining and TechnologyXuzhou221116JiangsuChina

As shallow resources are increasingly depleted,the mechanics'theory and testing technology of deep insitu rock has become *** coring technologies obtain rock samples without retaining the in-situ environmental conditions,leading to distortion of the measured ***,a coring and testing systems retaining in-situ geological conditions is presented:the coring system that obtains in-situ rock samples,and the transfer and testing system that stores and analyzes the rocks under a reconstructed *** ICP-Coring system mainly consists of the pressure controller,active insulated core reactor and insulation layer and sealing *** ultimate bearing strength of 100 MPa for pressurepreservation,temperature control accuracy of 0.97%for temperature-retained are ***_(4)and CO permeability of the optimized sealing film are as low as 3.85 and 0.33 ppm/*** average tensile elongation of the film is 152.4%and the light transmittance is reduced to 0%.Additionally,the pressure and steady-state temperature accuracy for reconstructing the in-situ environment of transfer and storage system up to 1%and±0.2 is *** error recorded of the noncontact sensor ring made of lowdensity polymer is less than 6%than that of the contact *** system can provide technical support for the deep in-situ rock mechanics research,improving deep resource acquisition capabilities and further clarifying deep-earth processes.

关键词： Deep mining In-situ environmental conditions In-situ condition preserved coring and testing In-situ transfer Deep-earth processes ICP-Coring In-situ condition-preserved coring

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