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电化学分析方法在中药质量控制中的研究进展

分析化学 2024年第1期52卷 22-34页

作者：潘彦冰 Awais IHSAN 施敏马雯雯 ghulam murtaza 胡克菲李竣黄先菊程寒中南民族大学药学院伊斯兰堡COMSATS大学生物科技学院伊斯兰堡COMSATS大学药学院元莱健康产品(武汉)有限公司国家中医药管理局民族药学三级实验室

中药质量控制是保证中药现代化、产业化以及国际化的核心问题。与其它分析方法相比，电化学分析法具有灵敏度高、检测速度快和成本低等优点，是中药质量控制的重要手段，具有广阔的发展前景。本文综述了近年来电化学方法在中药质量控制... 详细信息

中药质量控制是保证中药现代化、产业化以及国际化的核心问题。与其它分析方法相比，电化学分析法具有灵敏度高、检测速度快和成本低等优点，是中药质量控制的重要手段，具有广阔的发展前景。本文综述了近年来电化学方法在中药质量控制方面的研究进展，介绍了电化学指纹图谱技术在中药鉴别方面的研究概况，着重归纳了电化学技术在分析中药有效成分和有害物质中的应用，包括黄酮类、生物碱类、醌类、苷类、重金属和农药残留等，并展望了电化学方法在中药质量控制领域的发展前景。

关键词：电化学方法指纹图谱中药质量控制评述

来源：博看期刊

Electronic and thermoelectric properties of YbMg_(2)X_(2)(X=P,As,Sb,Bi)zintl compounds by first-principles method

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Journal of Rare Earths 2024年第1期42卷 147-154,I0006页

作者： Sajid Khan Dil Faraz Khan R.Neffati Tariq Usman Muhammad Waqar Ahsraf Shamim Khan Saeed Ullah Jan G.murtaza Department of Physics University of Science&Technology BannuBannu28100Pakistan Department of Physics Faculty of ScienceKing Khalid UniversityP.O.Box 9004AbhaSaudi Arabia Laboratoire de Physique de La Matiere Condensee Departement de PhysiqueFaculte des Sciences de TunisUniversite Tunis El ManarCampus Universitaire1060TunisTunisia Department of Physics Shaoxing UniversityShaoxing312000China Department of Mathematics&Natural Sciences Prince Mohammad Bin Fahd UniversityAlkhobar31952Saudi Arabia Materials Modeling Lab Department of PhysicsIslamia College Peshawar25120KhyberPakhtunkhwaPakistan

In this work the structural,electronic and thermoelectric properties of YbMg_(2)X_(2)(X=P,As,Sb,Bi)zintl compounds were investigated comprehensively using first principles *** electronic properties were studied using PBE GGA,TB-mBJ and hybrid(YS-PBE0)*** the structural parameters of optimized structures are in harmonious agreement to the available *** band structure study illustrates that the titled materials manifest metallic and semi metallic nature using PBE and TB-mBJ potentials while they show wide band gap semiconducting behavior by following hybrid(YS-PBE0)*** density of states(TDOS)and partial density of states(PDOS)were also calculated to glimpse the contribution of orbitals of atoms in the formation of *** properties were studied by using BoltzTraP2 code employed to *** get enormous values of Seebeck coefficient(S),power factor(PF)and thermoelectric figure of merit(ZT)for all the samples YbMg_(2)X_(2)(X=P,As,Sb,Bi),Moreover,the overwhelming transport properties for the titled compounds indicate the optimum level of carriers’concentration which pinpoints these materials to be better thermoelectrics in the 1-2-2 zintl family.

关键词： Zintl compounds Hybrid functional Band structure Thermoelectrics Rare earths

OffSig-SinGAN: A Deep Learning-Based Image Augmentation Model for Offline Signature Verification

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Computers, Materials & Continua 2023年第7期76卷 1267-1289页

作者： M.Muzaffar Hameed Rodina Ahmad Laiha Mat Kiah ghulam murtaza Noman Mazhar Faculty of Computer Science and Information Technology University of MalayaKuala Lumpur46400Malaysia Department of Computer Science Bahauddin Zakariya UniversityMultan60000Pakistan Department of Computer Science Sukkur Institute of Business Administration UniversitySukkur65200Pakistan

Offline signature verification(OfSV)is essential in preventing the falsification of *** learning(DL)based OfSVs require a high number of signature images to attain acceptable ***,a limited number of signature samples are available to train these models in a real-world *** researchers have proposed models to augment new signature images by applying various ***,on the other hand,have used human neuromotor and cognitive-inspired augmentation models to address the demand for more signature ***,augmenting a sufficient number of signatures with variations is still a challenging *** study proposed OffSig-SinGAN:a deep learning-based image augmentation model to address the limited number of signatures problem on offline signature *** proposed model is capable of augmenting better quality signatures with diversity from a single signature image *** is empirically evaluated on widely used public datasets;*** quality of augmented signature images is assessed using four metrics like pixel-by-pixel difference,peak signal-to-noise ratio(PSNR),structural similarity index measure(SSIM),and frechet inception distance(FID).Furthermore,various experiments were organised to evaluate the proposed image augmentation model’s performance on selected DL-based OfSV systems and to prove whether it helped to improve the verification accuracy *** results showed that the proposed augmentation model performed better on the GPDSsyntheticSignature dataset than other augmentation *** improved verification accuracy rate of the selected DL-based OfSV system proved the effectiveness of the proposed augmentation model.

关键词： Signature forgery detection offline signature verification deep learning image augmentation generative adversarial networks

Framework for fault-tolerant speed tracking control of gasoline engines using the first principle-based engine model

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Journal of Control and Decision 2023年第4期10卷 560-571页

作者： Raheel Anjum Ahmed Yar ghulam murtaza Qadeer Ahmed Aamer I.Bhatti Controls and Signal Processing Research Group(CASPR) Capital University of Science and TechnologyIslamabadPakistan Department of Mechanical Engineering College of E&MENational University of Sciences and TechnologyIslamabadPakistan Center for Automotive Research The Ohio State UniversityColumbusOHUSA Department of Electrical Engineering Capital University of Science and TechnologyIslamabadPakistan

Optimal engine torque management,a fundamental objective,depends predominantly on engine speed tracking *** ensures to attain desired speed profile in the presence of uncertainties,disturbances and *** the other hand,certain requirements such as emissions control,fuel efficiency and drivability are degraded in case of poorspeed ***,constraints on engine speed tracking performance are even more stringent for hybrid power-train architecture as crankshaft speed and engine torque are the basic variables for coordinated *** tracking is also considered essential for gearshift control ofthe automatic *** this research work,a framework for fault-tolerant speed tracking of the gasoline engine is proposed using the First Principle-based Engine Model(FPEM).A high-fidelity direct relationship between fuel injection input and engine speed is derived by the transformation of *** is induced in the fuel injection subsystem to generate the torque *** the proposed framework,a second-order sliding mode-based control technique is applied to track desired speed profile by mitigating the faultsin the fuel injection *** data acquired from the engine test rig is used to demonstrate the offline validity and fault tolerance capabilities of the proposed framework in MATLAB/Simulink.

关键词： Engine speed tracking fault-tolerant control gasoline engines sliding mode control

Factors affecting technical efficiency of small-scale apple farms in Balochistan Plateau, Pakistan

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Journal of Mountain Science 2017年第4期14卷 782-794页

作者： ghulam murtaza Gopal Bahadur THAPA Disaster Management and Development Studies University of Balochistan School of Environment Resources and Development Asian Institute of Technology

In Balochistan, Agriculture is dominated by small-scale farmers and the apple production sector is confronted with the chronic constraint of low output per unit of input. Although some agricultural policies have been implemented in this province, studies on effectiveness and impacts of such policies over apple production and farmers' performance are still limited. This study is an effort to bridge the research gap on this potential crop in the plateau by investigating technical and scale efficiency of 181 officially designated small-scale apple farmers in mountainous district Mastung in Balochistan; then explored factors that underlie differences in production inefficiency. A two-stage input-oriented Data Envelopment Analysis(DEA) methodology was employed to evaluate technical and scale efficiency followed by truncated bootstrapped regression framework to analyze the correlative determinants to efficiency. Average technical and scale efficiencies of larger landholders were higher than medium and small landholders. Analysis indicated that there is still ample scope for inefficient sample farmers to reduce the input use by 33% without compromising the given yield level. Maximum contributions to the total input savings were from the use of urea, farm yard manure(FYM) and labor-use. Farmer's experience, farm ownership, irrigation constraints, and farmer's access to trainings, credit and extension services significantly affected apple farmers' technical efficiency. Based on the findings of this study, strategies are suggested to enhancing efficiencies by farmers' capacity development through effective extension services and trainings and provision of adequate credit.

关键词：技术效率小苹果巴基斯坦高原农场数据包络分析农业政策生产部门

Painlevé integrability and a collection of new wave structures related to an important model in shallow water waves

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理论物理通讯:英文版 2023年第7期75卷 70-80页

作者： Isma ghulam murtaza Nauman Raza Saima Arshed Department of Mathematics University of the PunjabLahore 54590Pakistan

This paper investigates the perturbed Boussinesq equation that emerges in shallow water *** perturbed Boussinesq equation describes the properties of longitudinal waves in bars,long water waves,plasma waves,quantum mechanics,acoustic waves,nonlinear optics,and other *** a result,the governing model has significant importance in its own *** singular manifold method and the unified methods are employed in the proposed model for extracting hyperbolic,trigonometric,and rational function *** solutions may be useful in determining the underlying context of the physical *** is worth noting that the executed methods are skilled and effective for examining nonlinear evaluation equations,compatible with computer algebra,and provide a wide range of wave *** addition to this,the Painlevétest is also used to check the integrability of the governing ***-dimensional and threedimensional plots are made to illustrate the physical behavior of the newly obtained exact *** makes the study of exact solutions to other nonlinear evaluation equations using the singular manifold method and unified technique prospective and deserving of further study.

关键词： soliton shallow water waves singular manifold method Painleve test

Enviro-Friendly Synthesis of Silver Nanoparticles Using Berberis lycium Leaf Extract and Their Antibacterial Efficacy

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Acta Metallurgica Sinica(English Letters) 2014年第1期27卷 75-80页

作者： Ansar Mehmood ghulam murtaza Tariq Mahmood Bhatti Rehana Kausar Department of Botany University of Azad Jammu and Kashmir (UAJK)Muzaffarabad-13100Pakistan Department of Chemical and Material Engineering Pakistan Institute of Engineering and Applied Sciences(PIEAS)Islamabad-45650Pakistan

In the present study, an enviro-friendly synthesis of silver nanoparticles from Berberis lycium Royle leaf extract and their antibacterial efficacy against five pathogenic bacteria were investigated. This biosynthesis technique is proved to be advantageous over physical and chemical methods as no toxic chemicals are used. The structural and morphological characterization was made by UV-visible spectroscopy, scanning electron microscopy, and transmission electron microscopy. The synthesized nanoparticles were oval, rectangular, and spherical in shape, size ranges from 8 to 100 nm and exhibited an absorption peak at 458 nm. The biosynthesized silver nanoparticles have shown good antibacterial effect toward tested bacteria. It is believed that these biosynthesized silver nanoparticles can play a vital role in nano-based products in future.

关键词： Antibacterial Berberis lycium Enviro-friendly Silver nanoparticles

An Optimized and Hybrid Framework for Image Processing Based Network Intrusion Detection System

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Computers, Materials & Continua 2022年第11期73卷 3921-3949页

作者： murtaza Ahmed Siddiqi Wooguil Pak Department of Information and Communication Engineering Yeungnam UniversityGyeongsan38541Korea

The network infrastructure has evolved rapidly due to the everincreasing volume of users and *** massive number of online devices and users has forced the network to transform and facilitate the operational necessities of *** these necessities,network security is of prime *** intrusion detection systems(NIDS)are among the most suitable approaches to detect anomalies and assaults on a ***,keeping up with the network security requirements is quite challenging due to the constant mutation in attack patterns by the *** paper presents an effective and prevalent framework for NIDS by merging image processing with convolution neural networks(CNN).The proposed framework first converts non-image data from network traffic into images and then further enhances those images by using the Gabor *** images are then classified using a CNN *** assess the efficacy of the recommended method,four benchmark datasets i.e.,CSE-CIC-IDS2018,CIC-IDS-2017,ISCX-IDS 2012,and NSL-KDD were *** proposed approach showed higher precision in contrast with the recent work on the mentioned ***,the proposed method is compared with the recent well-known image processing methods for NIDS.

关键词： Anomaly detection convolution neural networks deep learning image processing intrusion detection network intrusion detection

Comparison of bioavailability and pharmacokinetics of diclofenac sodium and diclofenac potassium in normal and dehydrated rabbits

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药学学报 2009年第1期44卷 80-84页

作者： Mahmood AHMAD Muhammad IQBAL ghulam murtaza Department of Pharmacy Faculty of Pharmacy and Alternative Medicines the lslamia University of Bahawalpur Bahawalpur 63100 Pakistan

Two different salts of diclofenac,diclofenac sodium and diclofenac potassium,in tablet dosage form were tested for their bioavailability and disposition kinetics in a group of eighteen rabbits in normal and experimentally induced dehydrated conditions with a wash out period of 7 days between both stages of *** and physiological parameters were also measured in both normal and dehydrated *** levels in plasma were determined using a validated reversed phase HPLC *** kinetic parameters ***0-∞,Cmax,Tmax and other disposition kinetics were obtained with non-compartmental *** parameters *** cell volume,plasma glucose and total lipid concentration in dehydrated rabbits increased *** concentration of diclofenac sodium and diclofenac potassium decreased significantly in water deprived *** comparison,diclofenac potassium in normal and dehydrated state of the same group of rabbits showed a significantly increased plasma concentration when compared with diclofenac sodium.

关键词：生物药效率药物动力学药物化学生物化学