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Ultralight and superelastic MXene/reduced graphene oxide aerogels for electromagnetic interference shielding

Nano Research 2025年第1期18卷 1-9页

作者： Xinfeng Zhou Yang Dai Guoyao Yue Yiman zhang Lulu Li Zhong-Zhen Yu Peng Min hao-bin zhang 21 State Key Laboratory of Organic-Inorganic Composites College of Materials Science and EngineeringBeijing University of Chemical TechnologyBeijing 100029China Beijing Key Laboratory of Advanced Functional Polymer Composites College of Materials Science and EngineeringBeijing University of Chemical TechnologyBeijing 100029China Present address:BOE Technology Innovation Center BOE Technology Group Co.Ltd.Beijing 100176China Xi’an Modern Chemistry Research Institute Xi’an 710065China

Lightweight aerogels feature multifunctionality and a high porosity,yet accompanied with poor structure recovery under large strain *** this work,we develop an air bubble-ice crystal dual template and annealing strategy to integrate low density and high resilience for the conductive transition metal carbides/nitrides(MXene)composite *** air bubbles and ice crystals synergistically exclude the nanosheets to the gas-liquid interfaces,thereby constructing unique Y-shaped junctions and robust *** annealing process greatly enhances the interlayer *** external load,the Yshaped structures prevent the stress concentration at the junctions by transferring the forces to the skeleton for maintaining structural *** addition,the wrinkled and thick cell walls,together with the enhanced interlayer interactions,endow the aerogel with exceptional structural stability and *** a result,the MXene/reduced graphene oxide(RGO)composite aerogels exhibit superelasticity with reversible compressive strains of up to 95%.In addition,the electron bridging effect of the RGO sheets affords the aerogel to deliver excellent electromagnetic interference shielding performance,as high as 46.3 dB at 2.5 ***,the remarkable reshapeability of the aerogels allows for precise regulation of structure and performance(33.5-75.1 dB)by a simple wetting compression *** summary,this work offers helpful inspirations for developing lightweight and superelasticity aerogels for extensive applications.

关键词： lightweight superelasticity MXene aerogel electromagnetic interference shielding reshapeability

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Electrically Conductive and Flame Retardant Graphene/Brominated Polystyrene/Maleic Anhydride Grafted High Density Polyethylene Nanocomposites with Satisfactory Mechanical Properties

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Chinese Journal of Polymer Science 2019年第5期37卷 509-517页

作者： Yu Chen Jian Yao Ming-Ke Xu Zhi-Guo Jiang hao-bin zhang National Key Laboratory of Advanced Composites Beijing Institute of Aeronautical Materials Beijing Key Laboratory of Advanced Functional Polymer Composites College of Materials Science and EngineeringBeijing University of Chemical Technology

Electrically conductive and flame-retardant maleic anhydride grafted high-density polyethylene(MA-HDPE) nanocomposites with satisfactory mechanical properties are fabricated by melt compounding MA-HDPE with polyethyleneimine(PEI)-modified reduced graphene oxide(PEI@RGO) as the conductive nanofiller and brominated polystyrene(BPS) as the flame retardant. The modification with PEI significantly improves the interfacial compatibility and dispersion of the RGO sheets in the MA-HDPE matrix, leading to electrically conductive nanocomposites with enhanced mechanical properties. Furthermore, the addition of 25 wt% of BPS makes the nanocomposite flame-retardant with a UL-94 V-0 rating. Thus, the multifunctional RGO/MA-HDPE nanocomposites with good electrical, flameretardant, and mechanical properties would have potential applications in construction and pipeline fields.

关键词： Polymer nanocomposites High density polyethylene Graphene Electrical conductivity Flame retardancy

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Highly conductive calcium ion-reinforced MXene/sodium alginate aerogel meshes by direct ink writing for electromagnetic interference shielding and Joule heating

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Journal of Materials Science & Technology 2023年第4期135卷 213-220页

作者： Cheng-zhang Qi Xinyu Wu Ji Liu Xin-Jie Luo hao-bin zhang Zhong-Zhen Yu Beijing Key Laboratory of Advanced Functional Polymer Composites Beijing University of Chemical TechnologyBeijing 100029China State Key Laboratory of Organic-Inorganic Composites College of Materials Science and EngineeringBeijing University of Chemical TechnologyBeijing 100029China School of Chemistry CRANN and AMBERTrinity College DublinD2DublinIreland

Although MXene sheets possess high electrical conductivity and rich surface chemistry and are well suit-able for fabricating electrically conductive nanocomposites for electromagnetic interference(EMI)shield-ing applications,it remains challenging for MXene nanocomposites to achieve tunable EMI shielding per-formances and customized ***,an aqueous MXene/sodium alginate ink is developed to print aerogel meshes with customized geometries using a direct ink writing *** ion-enhanced strategy is proposed to reinforce the printed aerogel meshes by multi-level *** resultant 3D printed aerogel mesh exhibits an ultrahigh electrical conductivity of 2.85×10^(3)S m^(−1),outstanding mechanical properties,and excellent structural stability in wet *** importantly,a wide range of tunable EMI shielding efficiencies from 45 to 100 dB is achieved by the structural design of the 3D printed ion-enhanced MXene/sodium alginate aerogel *** a Joule heater,in addition,the printed aerogel meshes can achieve a wide temperature range of 40-135℃at low driving *** work demonstrates a direct ink writing approach for the fabrication of ion-enhanced MXene/sodium al-ginate aerogel meshes with tunable EMI shielding properties and multi-functionalities for applications in many scenarios.

关键词： MXene inks Aerogels Electromagnetic interference shielding Direct ink writing Joule heating

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Direct ink writing of multifunctional gratings with gel-like MXene/norepinephrine ink for dynamic electromagnetic interference shielding and patterned Joule heating

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Nano Research 2024年第3期17卷 1585-1594页

作者： Pei-Zhu Jiang Zhiming Deng Peng Min Lvxuan Ye Cheng-zhang Qi hao-Yu Zhao Ji Liu hao-bin zhang Zhong-Zhen Yu Beijing Key Laboratory of Advanced Functional Polymer Composites Beijing University of Chemical TechnologyBeijing 100029China State Key Laboratory of Organic-Inorganic Composites College of Materials Science and EngineeringBeijing University of Chemical TechnologyBeijing 100029China School of Chemistry CRANN and AMBERTrinity College DublinDublin D02PN40Ireland

Intelligent electromagnetic interference(EMI)shielding modulators with a wide tuning range and cyclic stability are urgently needed but their fabrication remains challenging.A gel-like MXene/norepinephrine ink is developed and multifunctional MXene gratings with wide EMI shielding effectiveness(SE)tuning range,superior reversibility,and high mechanical flexibility are constructed by direct ink writing approach for dynamic EMI shielding and patterned Joule heating *** modulable MXene/norepinephrine grating with a high conductivity of 3510 S·cm-1 can conveniently realize the seamless modulation of the EMI SE by adjusting the angle between the MXene grating filaments and the electric field of the incident electromagnetic waves,offering highly reversible switching between shielding“On”(28.0 dB)and“Off”(0.5 dB)***,due to the optimized integration of the MXene ink and the rationally designed pattern,a superior specific EMI SE of 95,688.2 dB·cm^(2)·g^(-1) is achieved in the“On”***,the MXene/norepinephrine ink can be used to fabricate many complex patterned gratings with superior stability,instant responsibility,and superb mechanical flexibility,exhibiting a unique patterned Joule heating *** writing of multifunctional gratings paves a means for developing intelligent EMI shielding materials,wearable electronic devices,and advanced thermal management materials.

关键词： MXene ink direct ink writing electromagnetic interference shielding multifunctional gratings Joule heating

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Strong and conductive reduced graphene oxide-MXene porous films for efficient electromagnetic interference shielding

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Nano Research 2022年第6期15卷 4916-4924页

作者： Yu zhang Ming-Ke Xu Zhenguo Wang Tianyu Zhao Liu-Xin Liu hao-bin zhang Zhong-Zhen Yu State Key Laboratory of Organic-Inorganic Composites College of Materials Science and EngineeringBeijing University of Chemical TechnologyBeijing 100029China Beijing Key Laboratory of Advanced Functional Polymer Composites Beijing University of Chemical TechnologyBeijing 100029China

Lightweight,flexible,and electrically conductive porous films are promising for efficient electromagnetic interference(EMI)***,the mechanical and electrical properties of porous films are far from ***,we fabricate mechanically flexible and electrically conductive reduced graphene oxide(rGO)-Ti_(3)C_(2)T_(x)MXene(rG-M)porous films with optimized continuous cellular morphology by a controlled hydrazine foaming *** presence of MXene prevents excessive expansion of the rG-M film,improves the electron conduction paths,and enhances the mechanical *** resultant rG-M porous film has superior mechanical and electric performances compared to its rGO counterpart,giving one of the highest tensile strengths(24.5 MPa)among the porous films,a high electrical conductivity of 74.4 S·cm^(−1),and an excellent broadband EMI shielding from 8 to 26.5 GHz.A high EMI shielding effectiveness of 52.6 dB is achieved for the porous film by adjusting its thickness and treatment procedure,providing a feasible fabrication route for lightweight and high-performance EMI shielding materials.

关键词： graphene MXene electromagnetic interference shielding porous films electrical conductivity

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Super-Tough and Environmentally Stable Aramid Nanofiber@MXene Coaxial Fibers with Outstanding Electromagnetic Interference Shielding Efficiency

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Nano-Micro Letters 2022年第7期14卷 72-85页

作者： Liu-Xin Liu Wei Chen hao-bin zhang Lvxuan Ye Zhenguo Wang Yu zhang Peng Min Zhong-Zhen Yu State Key Laboratory of Organic-Inorganic Composites College of Materials Science and EngineeringBeijing University of Chemical TechnologyBeijing 100029People’s Republic of China Beijing Key Laboratory of Advanced Functional Polymer Composites Beijing University of Chemical TechnologyBeijing 100029People’s Republic of China Beijing Advanced Innovation Center for Soft Matter Science and Engineering Beijing University of Chemical TechnologyBeijing 100029People’s Republic of China

Although electrically conductive and hydrophilic MXene sheets are promising for multifunctional fibers and electronic textiles,it is still a challenge to simultaneously enhance both conductivity and mechanical properties of MXene fibers because of the high rigidity of MXene sheets and insufficient inter-sheet ***,we demonstrate a core-shell wet-spinning methodology for fabricating highly conductive,super-tough,ultra-strong,and environmentally stable Ti_(3)C_(2)T_(x) MXene-based core-shell fibers with conductive MXene cores and tough aramid nanofiber(ANF)*** highly orientated and low-defect structure endows the ANF@MXene core-shell fiber with supertoughness of~48.1 MJ m^(-3),high strength of~502.9 MPa,and high conductivity of~3.0×10^(5)S m^(-1).The super-tough and conductive ANF@MXene fibers can be woven into textiles,exhibiting an excellent electromagnetic interference(EMI)shielding efficiency of 83.4 dB at a small thickness of 213μ***,the protection of the ANF shells provides the fibers with satisfactory cyclic stability under dynamic stretching and bending,and excellent resistance to acid,alkali,seawater,cryogenic and high temperatures,and *** oxidation resistance of the fibers is demonstrated by their wellmaintained EMI shielding *** multifunctional core-shell fibers would be highly promising in the fields of EMI shielding textiles,wearable electronics and aerospace.

关键词： Core-shell fibers MXene sheets Electromagnetic interference shielding Aramid nanofibers Super-toughness

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Multifunctional Waterborne Polyurethane Nanocomposite Films with Remarkable Electromagnetic Interference Shielding,Electrothermal and Solarthermal Performances

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Chinese Journal of Polymer Science 2023年第2期41卷 267-277页

作者： Ming-Ke Xu Xin-Jie Luo hao-bin zhang Yu zhang Lulu Li Xin-Feng Zhou Zhong-Zhen Yu Beijing Key Laboratory of Advanced Functional Polymer Composites Beijing University of Chemical TechnologyBeijing100029China State Key Laboratory of Organic-Inorganic Composites College of Materials Science and EngineeringBeijing University of Chemical TechnologyBeijing100029China

To impart polymers with high electrical conductivity and satisfactory electromagnetic interference shielding efficiency,it is crucial to efficiently construct interconnecting networks of conductive nanofillers in polymer ***,on the basis of the three-dimensional(3D)skeleton and volume-exclusion effect of silane-modified tetra-needle ZnO(ST-ZnO)whiskers and the high conductivity of two-dimensional MXene nanosheets,multifunctional MXene/ST-ZnO/waterborne polyurethane(MTW)nanocomposite films are fabricated by coating of MXene on ST-ZnO followed by compounding with waterborne *** 3D four-needles of the whiskers facilitate the formation of an interconnecting network in the waterborne polyurethane matrix,while the coating of MXene efficiently makes the interconnecting network of the whiskers conductive at a low amount of the *** resultant MTW ternary nanocomposite film exhibits not only a high electrical conductivity of 4.8×10^(4)S/m,but also an excellent electromagnetic interference shielding effectiveness of over 70 dB in the X-band at a low thickness of 100µ*** addition,the ternary film also exhibits outstanding Joule heating performances with an equilibrium temperature of 113℃at a low driving voltage of 3 *** multifunctional nanocomposite films are promising for applications in portable and wearable electronics and flexible electromagnetic interference shielding devices.

关键词： Electrical conductivity Electromagnetic interference shielding Nanocomposite films Waterborne polyurethane MXene nanosheets

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Direct Ink Writing of Highly Conductive MXene Frames for Tunable Electromagnetic Interference Shielding and Electromagnetic Wave-Induced Thermochromism

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Nano-Micro Letters 2021年第10期13卷 14-28页

作者： Xinyu Wu Tingxiang Tu Yang Dai Pingping Tang Yu zhang Zhiming Deng Lulu Li hao-bin zhang Zhong-Zhen Yu State Key Laboratory of Organic-Inorganic Composites College of Materials Science and EngineeringBeijing University of Chemical TechnologyBeijing 100029People’s Republic of China Beijing Key Laboratory of Advanced Functional Polymer Composites Beijing University of Chemical TechnologyBeijing 100029People’s Republic of China Beijing Advanced Innovation Center for Soft Matter Science and Engineering Beijing University of Chemical TechnologyBeijing 100029People’s Republic of China

The highly integrated and miniaturized next-generation electronic products call for high-performance electromagnetic interference(EMI)shielding materials to assure the normal operation of their closely assembled ***,the most current techniques are not adequate for the fabrication of shielding materials with programmable structure and controllable shielding ***,we demonstrate the direct ink writing of robust and highly conductive Ti3C2Tx MXene frames with customizable structures by using MXene/AlOOH inks for tunable EMI shielding and electromagnetic wave-induced thermochromism *** as-printed frames are reinforced by immersing in AlCl_(3)/HCl solution to remove the electrically insulating AlOOH nanoparticles,as well as cross-link the MXene sheets and fuse the filament interfaces with aluminum *** freeze-drying,the resultant robust and porous MXene frames exhibit tunable EMI shielding efficiencies in the range of 25-80 dB with the highest electrical conductivity of 5323 S m−***,an electromagnetic wave-induced thermochromic MXene pattern is assembled by coating and curing with thermochromic polydimethylsiloxane on a printed MXene pattern,and its color can be changed from blue to red under the high-intensity electromagnetic *** work demonstrates a direct ink printing of customizable EMI frames and patterns for tuning EMI shielding efficiency and visualizing electromagnetic waves.

关键词： MXene Electromagnetic interference shielding Direct ink writing Electrical conductivity Thermochromism

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Mo supported on natural rectorite catalyst for slurry-phase hydrocracking of vacuum residue:An effect of calcination

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Petroleum Science 2021年第6期18卷 1867-1876页

作者： Qing-Yan Cui hao-bin zhang Ting-Hai Wang Chao Yan Yan-Ning Cao Yuan-Yuan Yue Li-Long Jiang Xiao-Jun Bao College of Chemical Engineering Fuzhou UniversityFuzhou350108China

In order to develop high-efficiency and low-cost catalyst for the slurry-phase hydrocracking of vacuum residue(VR),the catalyst supported on natural rectorite was prepared,and the effect of calcination modification of rectorite on the catalyst properties and performance was *** support of rectorite and catalyst were characterized by XRD,FTIR,Py-FTIR,H_(2)-TPR and XPS to examine their structures and *** comparative reaction results show that VR conversions for the catalysts supported on calcined rectorite were similar with that on raw rectorite,possibly due to the VR cracking reaction controlled by the thermal cracking following free radical mechanism because of few acid sites observed on the catalysts ***,the yields of naphtha and middle distillates for the various catalysts were obviously different,and increased following as Rec-Mo(40.4 wt%)

关键词： Natural rectorite Catalyst Slurry-phase hydrocracking Vacuum residue Calcination

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聚合物基纳米复合材料结构设计与电磁屏蔽性能研究

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高分子学报 2020年第6期51卷 573-585,I0003页

作者：吴昕昱张好斌北京化工大学材料科学与工程学院北京100029

聚合物纳米复合材料以其质量轻、易加工成型、耐化学腐蚀等优秀特性成为电磁屏蔽材料的研究热点.复合材料的导电性是影响电磁屏蔽性能的关键因素,而聚合物基体中导电网络结构则决定了材料内部的电子传输效率,从而在很大程度上决定材料... 详细信息

聚合物纳米复合材料以其质量轻、易加工成型、耐化学腐蚀等优秀特性成为电磁屏蔽材料的研究热点.复合材料的导电性是影响电磁屏蔽性能的关键因素,而聚合物基体中导电网络结构则决定了材料内部的电子传输效率,从而在很大程度上决定材料导电性能.合理的结构设计可以解决纳米填料在基体中易团聚、难分散的问题,实现低渗滤阈值、高导电性能/电磁屏蔽与多功能化的统一.我们围绕聚合物纳米复合材料的关键科学问题展开研究,取得一些创新性研究成果:(1)通过填料/基体界面调控,实现复合材料连续导电网络的构筑,制备系列低渗滤阈值聚合物导电复合材料;(2)发展三维导电结构预先构筑新方法,制备出高效导电网络,实现电磁屏蔽复合材料结构功能一体化设计与制备;(3)提出构建多界面结构策略,实现聚合物电磁屏蔽复合材料的轻量化设计.本专论针对我们研究成果进行总结,并对高性能电磁屏蔽纳米复合材料的发展前景进行展望.

关键词：纳米复合材料石墨烯二维过渡金属碳/氮化物电磁屏蔽结构设计

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