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Engineering hierarchical heterostructure material based on metal-organic frameworks and cotton fiber for high-efficient microwave absorber

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Nano Research 2022年第8期15卷 6841-6850页

作者： Yan Guo Hu Liu Dedong Wang Zeinhom m.El-Bahy Jalal T.Althakafy hala m.Abo-dief Zhanhu Guo Ben Bin Xu Chuntai Liu Changyu Shen Key Laboratory of materials Processing and mold(Zhengzhou University) Ministry of EducationNational Engineering Research Center for Advanced Polymer Processing TechnologyZhengzhou UniversityZhengzhou 450002China Department of Chemistry Faculty of ScienceAl-Azhar UniversityNasr City 11884CairoEgypt Department of Chemistry Faculty of Applied ScienceUmm Al-Qura UniversityMecca 21955Saudi Arabia Department of Chemistry College of ScienceTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia Integrated Composites Laboratory(ICL) Department of Chemical&Biomolecular EngineeringUniversity of TennesseeKnoxvilleTN 37996USA Department of mechanical and Construction Engineering Faculty of Engineering and EnvironmentNorthumbria UniversityNewcastle upon TyneNE18STUK

Rational construction of hierarchical multi-component materials with abundant heterostructure is evolving as a promising strategy to achieve excellent metal-organic frameworks(mOFs)based electromagnetic wave(EmW)***,hierarchical heterostructure WS_(2)/CoS_(2)@carbonized cotton fiber(CCF)was fabricated using the ZIF-67 mOFs nanosheets anchored cotton fiber(ZIF-67@CF)as a precursor through the tungsten etching,sulfurization,and carbonization *** from the synergetic effect of dielectric-magnetic dual-loss mechanism,the hierarchical heterostructure and multicomponent of WS_(2)/CoS_(2)@CCF also display improved impedance ***,numerous W-S-Co bands and heterojunction interfaces of heterogeneous WS_(2)/CoS_(2)are beneficial to promoting additional interfacial/dipole polarization loss and conductive loss,thereby enhancing the EmW attenuation *** on the percolation theory,a good balance between impedance matching and EmW absorption capacity was achieved for the WS_(2)/CoS_(2)@CCF/paraffin composite with 20 wt.%filler loading,exhibiting strong EmW absorption capability with a minimum reflection loss(RLmin)value of−51.26 dB at 17.36 GHz with 2 mm thickness and a maximum effective absorption bandwidth(EABmax)as wide as 6.72 *** research will provide new guidance for designing high-efficient mOFs derived EmW absorbers.

关键词： hierarchical heterostructure sulfurization metal-organic framework microwave absorber

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Tellurium intervened Fe-N codoped carbon for improved oxygen reduction reaction and high-performance Zn-air batteries

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Journal of materials Science & Technology 2023年第6期137卷 215-222页

作者： Rui Wang Zihan meng Xuemin Yan Tian Tian ming Lei Rami Adel Pashameah hala m.bo-dief Hassan Algadi Nina Huang Zhanhu Guo Haolin Tang State Key Laboratory of Advanced Technology for materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China Foshan Xianhu Laboratory of the Advanced Energy Science and Technology Guangdong Laboratory Xianhu Hydrogen ValleyFoshan 528200China College of Chemistry and Environmental Engineering Yangtze UniversityJingzhou 434023China State Key Laboratory of Information Photonics and Optical Communications Beijing University of Posts and TelecommunicationsBeijing 100876China Department of Chemistry Faculty of Applied ScienceUmm Al-Qura UniversityMakkah 24230Saudi Arabia Department of Science and Technology University College-RanyahTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia Department of Electrical Engineering Faculty of EngineeringNajran UniversityP.O.Box 1988Najran 11001Saudi Arabia College of materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan 030024China Department of Chemical and Bimolecular Engineering Integrated Composites Laboratory(ICL)University of TennesseeKnoxvilleTN 37996USA Guangdong Hydrogen Energy Institute of WHUT Xianhu Hydrogen ValleyFoshan 528200China

Pyrolysis-acquired iron and nitrogen codoped carbon(Fe-N-C)has been comprehensively investigated for its promising oxygen reduction reaction(ORR)catalytic performance and structural *** modification of non-metal elements with larger atomic radius and the corresponding intrinsic microstructure-property relations are rarely *** this study,tellurium(Te)intervened Fe-N-C was prepared by micelles-induced polymerization with Te nanowires as an in-situ intervening *** out-plane bonding of Te with Fe induced the increase of both N content and proportion of pyridinic N on the material surface,thus improving the ORR catalytic *** assembled Zn-air battery demonstrated a maximum power density of 250 mW/cm^(2)and excellent rate capability under various discharge current densities,which was much better than the Pt/***,the current work demonstrates a novel Te/Fe-N-C material and reveals an original Te intervened Fe-N-C strategy and N reconfiguration mechanism,which is of great significance for the design of key materials in energy-related fields.

关键词： Te/Fe-N-C Assembly ORR Electrocatalysis Zn-air battery

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Vertically Aligned Silicon Carbide Nanowires/boron Nitride Cellulose Aerogel Networks Enhanced Thermal Conductivity and Electromagnetic Absorbing of Epoxy Composites

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Nano-micro Letters 2022年第7期14卷 209-227页

作者： Duo Pan Gui Yang hala m.bo-dief Jingwen Dong Fengmei Su Chuntai Liu Yifan Li Ben Bin Xu Vignesh murugadoss Nithesh Naik Salah mEl-Bahy Zeinhom mEl-Bahy minan Huang Zhanhu Guo Key Laboratory of materials Processing and mold(Zhengzhou University) Ministry of EducationNational Engineering Research Center for Advanced Polymer Processing TechnologyZhengzhou UniversityZhengzhou 450002People’s Republic of China Department of Chemistry College of ScienceTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia mechanical and Construction Engineering Faculty of Engineering and EnvironmentNorthumbria UniversityNewcastle upon Tyne NE18STUK Integrated Composites Laboratory(ICL) Department of Chemical and Biomolecular EngineeringUniversity of TennesseeKnoxvilleTN 37996USA Advanced materials Division Engineered Multifunctional Composites(EMC)Nanotech LLCKnoxvilleTN 37934USA College of materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan 030024People’s Republic of China Department of mechanical and manufacturing Engineering Manipal Institute of TechnologyManipal Academy of Higher EducationManipalKarnataka 576104India Department of Chemistry Turabah University CollegeTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia Department of Chemistry Al-Azhar UniversityNasr CityCairo 11884Egypt

With the innovation of microelectronics technology, the heat dissipation problem inside the device will face a severe test. In this work, cellulose aerogel(CA) with highly enhanced thermal conductivity(TC) in vertical planes was successfully obtained by constructing a vertically aligned silicon carbide nanowires(SiC NWs)/boron nitride(BN) network via the ice template-assisted strategy. The unique network structure of SiC NWs connected to BN ensures that the TC of the composite in the vertical direction reaches 2.21 W m^(-1) K^(-1) at a low hybrid filler loading of 16.69 wt%, which was increased by 890% compared to pure epoxy(EP). In addition, relying on unique porous network structure of CA, EP-based composite also showed higher TC than other comparative samples in the horizontal direction. meanwhile, the composite exhibits good electrically insulating with a volume electrical resistivity about 2.35 × 10^(11) Ω cm and displays excellent electromagnetic wave absorption performance with a minimum reflection loss of-21.5 dB and a wide effective absorption bandwidth(m 8.8 to 11.6 GHz. Therefore, this work provides a new strategy for manufacturing polymer-based composites with excellent multifunctional performances in microelectronic packaging applications.

关键词： Epoxy Ice template Vertical alignment Thermal conductivity multifunctionality

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Perfluorosulfonic acid proton exchange membrane with double proton site side chain for high-performance fuel cells at low humidity

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Journal of materials Science & Technology 2023年第35期166卷 155-163页

作者： Hongyun Tan Shengqiu Zhao S.Eltahir Ali Shuhong Zheng Abdullah K.Alanazi Rui Wang Haining Zhang hala m.Abo-dief Ben Bin Xu Hassan Algadi Handong Li Priyanka Wasnik Zhanhu Guo Haolin Tang State Key Laboratory of Advanced Technology for materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China Department of Science and Technology University College-RanyahTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia Department of Chemistry College of ScienceTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia Foshan Xianhu Laboratory of the Advanced Energy Science and Technology Guangdong Laboratory Xianhu Hydrogen ValleyFoshan 528200China Integrated Composites Laboratory(ICL) Mechanical and Construction EngineeringNorthumbria UniversityNewcastle Upon Tyne NE18STUK College of materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan 030024China Department of Electrical Engineering Faculty of EngineeringNajran UniversityNajran11001Saudi Arabia

Structural optimization of ionomers is an effective strategy for achieving high-performance proton ex-change membranes(PEms)under low relative humidity(RH)*** this study,sulfonimide group and trifluoromethanesulfonate acid(TFSA)ionic liquids were introduced to the perfluorosulfonic acid(PFSA)side chain,resulting in polymer membranes with varying chain lengths(i.e.,PFC_(2)-TF-SI,PFC_(4)-TF-SI,and PFC_(5)-TF-SI).This dual proton-conducting structure extended the length of the hydrophilic side chain and enhanced the hydrophobic-hydrophilic phase separation,aiding in the formation of proton transport ***,the proton conductivity of PFC_(5)-TF-SI and PFC_(2)-TF-SI membranes reached 7.1 and 10.6 mS/cm at 30%RH and 80℃,respectively,which were approximately 29.1%and 92.7%higher than that of the pristine PFC_(5)-SA membrane(5.5 mS/cm).Furthermore,the maximum power density of the PFC_(5)-TF-SI and PFC_(2)-TF-SI membranes from the built single fuel cell achieved 649 and 763 mW/cm^(2) at 30%RH and 80℃,respectively,which were higher than that of the pristine PFC_(5)-SA membrane(567 mW/cm^(2))by about 14.5%and 34.6%,***,this study provides a strategy for PEm design under low RH conditions.

关键词： Proton exchange membrane Structural design Dual proton conduction Hydrophilic channel Proton conductivity Fuel cells

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Synthesis, Structure Characterization and Biological Activity of a Novel Amino Acid Salt (hala)_8(H_30)_(10)[Pmo_(12)O_(40)]_6·22H_2O

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Chemical Research in Chinese Universities 2001年第4期17卷 356-361页

作者： HAN Zheng-bo WANG En-bo LUAN Guo-you HU Chang-wen CHANG Ya-ping LI Juan HU Ning-hai JIA Heng-qing Faculty of Chemistry Northeast Normal UniversityChangchun 130024P.R.China College of medicine Jilin UniversityChangchun 130021P.R.China Changchun Institude of Applied Chemistry Chinese Academy of Sciences.Changchun 130022P.R.China

A novel compound was synthesized and characterized by means of elemental analysis, IR and UV spectra, TG, CV and single crystal X-ray diffraction. The compound crystallized in an orthorhombic space group C222 with a = 1. 622 4(3) nm, b=3. 498 4(7) nm, c=l. 301 5(3) nm,V=7. 387(3) nm3, Z = 6, R1 = 0. 037 3, wR2 = 0. 114 0. The Ala (Ala = alanine) molecules were protonated at the amino nitrogen N (1) and the C (2) of Ala group with the terminal oxygen atom O(15), O(14), O(26) and O(27) of the polyoxometalates participating in the hydrogen bond network. The anti-tumor activity of the title compound was estimated against Hela and Pc-3m cancer cells.

关键词： Polyoxometalate Ala Crystal structure Antitumor activity

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Structural characteristics and implication on tectonic evolution of the Daerbute strike-slip fault in West Junggar area, NW China

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Frontiers of Earth Science 2018年第3期12卷 555-568页

作者： Kongyou WU Yangwen PEI Tianran LI Xulong WANG Yin LIU bo LIU Chao mA School of Geosciences China University of Petroleum Qingdao 266580 China Laboratory for marine mineral Resources Qingdao National Laboratory for Marine Science and Technology Qingdao 266071 China Key Laboratory of Tectonics and Petroleum Resources (China University of Geosciences) Ministry of Education Wuhan 430074 China Xinjiang Oilfield Company PetroChina Karamay 834000 China

The Daerbute fault zone, located in the northwestern margin of the Junggar basin, in the Central Asian Orogenic Belt, is a regional strike-slip fault with a length of 400 km. The NE-SW trending Daerbute fault zone presents a distinct linear trend in plain view, cutting through both the Zair mountain and the hala＇alate mountain. Because of the intense contraction and shearing, the rocks within the fault zone experienced high degree of cataclasis, schistosity, and mylonization, resulting in rocks that are easily eroded to form a valley with a width of 300- 500 m and a depth of 50-100 m after weathering and erosion. The well-exposed outcrops along the Daerbute fault zone present sub-horizontal striations and sub-vertical fault steps, indicating sub-horizontal shearing along the observed fault planes. Flower structures and horizontal drag folds are also observed in both the well-exposed outcrops and high-resolution satellite images. The distribution of accommodating strike-slip splay faults, e.g., the 973-pluton fault and the Great Jurassic Trough fault, are in accordance with the Riedel model of simple shear. The seismic and time-frequency electromagnetic （TFEm） sections also demonstrate the typical strike-slip characteristics of the Daerbute fault zone. Based on detailed field observations of well-exposed outcrops and seismic sections, the Daerbute fault can be subdivided into two segments： the western segment presents multiple fault cores and damage zones, whereas the eastern segment only presents a single fault core, in which the rocks experienced a higher degree of rock cataclasis, schistosity, and mylonization. In the central overlapping portion between the two segments, the sediments within the fault zone are primarily reddish sandstones, conglomerates, and some mudstones, of which the palynological tests suggest middle Permian as the timing of deposition. The deformation timing of the Daerbute fault was estimated by integrating the depocenters＇ basinward migrat

关键词： Daerbute fault structural characteristics deformation timing West Junggar

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