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Precise separation and efficient recovery of Pd(Ⅱ) from high-level liquid waste by XAD-based adsorbents

Rare Metals 2024年第10期43卷 5372-5390页

作者： Hao-Ran Dong Shun-Yan Ning zeng-Yuan Li Si-zhi Xu Feng-Tao Hu Feng Gao You-Bin Wang Li-Feng Chen Xiang-Biao Yin Toyohisa Fujita Mohammed F.Hamza Yue-Zhou Wei School of Resources Environment and MaterialsGuangxi University School of Nuclear Science and Technology University of South China

Efficient separation of palladium (Pd（II）) from high-level liquid waste （HLLW） not only helps the safe disposal of nuclear waste,but also is a vital importan supplement to Pd（II） ***,16 kinds of nove Amberlite XAD resins-based adsorbents were prepared by vacuum impregnation method for the separation of Pd（II）from simulated HLLW,and the MMBT/XAD7HP prepared using 4-methyl-2-mercaptobenzothiazole （MMBT） as ligand and Amberlite XAD7HP resin （XAD7HP） as the carrier was selected as the optimal research *** analysis experiments proved the successful preparation of MMBT/XAD7HP,which exhibited ultrahigh adsorption selectivity for Pd（II）(distribution coefficient （Kd）≥12584.5 ml·g-1,separation factor (SFPd/M)≥2818.4) and superior adsorption capacity(Q≥130.1 mg·g-1).The adsorption kinetics and adsorption isotherms for Pd（II） matched with pseudo-secondorder （PSO） kinetics model and Langmuir model,indicating that the adsorption mode for Pd（II） by MMBT/XAD7 HP was monolayer chemical *** dynamic column experiments showed that MMBT/XAD7 HP achieved efficiently separation of Pd（II） from simulated HLLW,and the recovery rate was nearly 100% The adsorption mechanism was analyzed by Fourier transform infrared spectroscopy （FTIR）,X-ray photoelectron spectroscopy （XPS） and density functional theory（DFT）,and the ultrahigh selectivity of MMBT/XAD7 HP is attributed to the preferred affinity of the soft-N,S donor atoms in MMBT for Pd（II）.MMBT has the shortest frontline molecular orbital energy band gap （HOMO–LUMO） among the four ligands,which makes it easier to become an electron donor to attract Pd2+to participate in ***3-participates in the adsorption to keep charge *** summary,MMBT/XAD7 HP has broad application prospects for the treatment of Pd（II） in HLLW

关键词： Adsorption Column experiments HLLW Palladium XAD

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Lithium carbonate-induced giant goiter and subclinical hyperthyroidism in a patient with schizophrenia:A case report and review of literature

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World Journal of Clinical Cases 2024年第20期12卷 4357-4364页

作者： Xing-Ming Chen zhi-Li Jiang Xiang Wu Xu-guang Li Department of Psychiatry The Affiliated Brain Hospital of Guangzhou Medical UniversityGuangzhou 510370Guangdong ProvinceChina Department of General Surgery The Affiliated Brain Hospital of Guangzhou Medical UniversityGuangzhou 510370Guangdong ProvinceChina Key Laboratory of Neurogenetics and Channelopathies of guangdong Province The Ministry of Education of ChinaGuangzhou Medical UniversityGuangzhou 511436Guangdong ProvinceChina

BACKGROUND Lithium carbonate is used to manage various mood disorders,but it can cause thyroid abnormalities,including goiter,hypothyroidism,and *** rare cases,it can lead to giant goiter and subclinical hyperthyroidism,which may require surgical intervention in severe *** SUMMARY This case represents a rare development of giant goiter and subclinical hyperthyroidism in a schizophrenia patient who was subjected to prolonged lithium carbonate *** enlarged thyroid gland caused pressure on the airway and recurrent laryngeal nerve,which led to respiratory distress,hoarseness,and *** immediate danger of suffocation required urgent surgical *** this report,we describe the case of a 41-year-old Chinese *** sheds light on the etiology and challenges associated with managing a giant *** patient underwent a subtotal thyroidectomy to relieve airway compression and facilitate airway *** to the procedure,the patient was given iodine to ***,changes were made to the psychiatric medication *** surgery,the patient's respiratory function and vocal cord functionality improved significantly,and her mental state remained *** It is essential to monitor thyroid function,test thyroid antibody levels,and perform thyroid ultrasounds consistently in all patients undergoing long-term lithium carbonate *** vigilance helps prevent severe and potentially life-threatening thyroid enlargement.

关键词： Lithium carbonate Giant goiter Subclinical hyperthyroidism Schizophrenia Subtotal thyroidectomy Case report

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液晶分子优化给体材料组装制备高性能有机太阳能电池

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高分子学报 2024年第6期55卷 698-708页

作者：曾光张奔李耀文苏州大学苏州市新型半导体光电材料与器件重点实验室苏州215123

活性层形貌优化是实现高效、稳定的体异质结有机太阳能电池(OSC)的关键,添加剂工程被广泛用于优化OSC活性层的膜形貌.基于此,本文工作提出了一种利用具有简单结构的液晶分子4-氰基-4'-庚基联苯(7-CB)作为添加剂优化给体聚合物(PM6)在共... 详细信息

活性层形貌优化是实现高效、稳定的体异质结有机太阳能电池(OSC)的关键,添加剂工程被广泛用于优化OSC活性层的膜形貌.基于此,本文工作提出了一种利用具有简单结构的液晶分子4-氰基-4'-庚基联苯(7-CB)作为添加剂优化给体聚合物(PM6)在共混膜中聚集行为的策略.通过掠入射广角X射线散射、原位吸收光谱及分子动力学模拟等表征发现,7-CB通过与PM6的烷基侧链之间的范德华力和CH/π相互作用诱导PM6规整排列,增强了PM6之间的相互作用,提高了活性层薄膜的结晶度.得益于此,无任何后处理的活性层薄膜中电荷传输得到改善,电荷重组被大幅抑制.基于7-CB处理的PM6:L8-BO制备的硬质和柔性二元OSCs效率分别从15.41%和14.90%提高到18.01%和17.26%.

关键词：有机太阳能电池添加剂自组装

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铁磁畴壁中自旋极化电流诱导的左旋极化自旋波

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物理学报 2024年第14期73卷 222-227页

作者：刘想王希光李志雄郭光华中南大学物理学院长沙410083

极化指的是波偏振的方式,是波的一个基本性质.利用波的极化可以进行信息的编码,这一编码方式在光学和声学中得到广泛应用.利用自旋波进行信息的传递和处理是磁子学的主要研究课题.然而在铁磁材料中,由于只存在右旋极化的自旋波,利用波... 详细信息

极化指的是波偏振的方式,是波的一个基本性质.利用波的极化可以进行信息的编码,这一编码方式在光学和声学中得到广泛应用.利用自旋波进行信息的传递和处理是磁子学的主要研究课题.然而在铁磁材料中,由于只存在右旋极化的自旋波,利用波的极化进行信息的编码在铁磁自旋波器件中始终没有实现.前期研究发现,通过自旋极化电流可以在铁磁体中产生左旋极化自旋波,从而有望实现利用极化编码的自旋波器件.然而在一个均匀磁化铁磁体中产生左旋极化自旋波所需的电流密度过大,实验上难以实现.磁畴壁可作为自旋波波导,且畴壁中自旋波的截止频率趋近于零.本文从朗道-栗弗席兹方程出发,研究了在自旋极化电流存在的条件下磁畴壁中自旋波的色散关系和传播特性,证明只需要很小的自旋极化电流就可在畴壁中产生稳定的左旋极化自旋波.微磁学模拟证明了理论分析结果.该项研究为研制基于极化编码信息的自旋波器件提供了一个实际可行的方案.

关键词：自旋波磁畴壁自旋极化电流微磁学

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Plasma metabolites and risk of myocardial infarction:a bidirectional Mendelian randomization study

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Journal of Geriatric Cardiology 2024年第2期21卷 219-231页

作者： Dong-Hua LI Qiang WU Jing-Sheng LAN Shuo CHEN You-Yi HUANG Lan-Jin WU zhi-Qing QIN Ying HUANG Wan-Zhong HUANG Ting zeng Xin HAO Hua-Bin SU Qiang SU Department of Cardiovascular Medicine Minzu Hospital of Guangxi Zhuang Autonomous RegionGuangxiChina Senior Department of Cardiology the Sixth Medical CenterChinese PLA General HospitalBeijingChina Library of Graduate School Chinese PLA General HospitalBeijingChina Department of Cardiology Jiangbin Hospital of Guangxi Zhuang Autonomous RegionGuangxiChina Health Management Institute the Second Medical CenterChinese PLA General HospitalBeijingChina

BACKGROUND Myocardial infarction(MI)is a critical cardiovascular event with multifaceted etiology,involving several genetic and environmental *** is essential to understand the function of plasma metabolites in the development of MI and unravel its complex *** This study employed a bidirectional Mendelian randomization(MR)approach to investigate the causal relationships between plasma metabolites and MI *** used genetic instruments as proxies for plasma metabolites and MI and conducted MR analyses in both directions to assess the impact of metabolites on MI risk and vice *** addition,the large-scale genome-wide association studies datasets was used to identify genetic variants associated with plasma metabolite(1400 metabolites)and MI(20,917 individuals with MI and 440,906 individuals without MI)*** variance weighted was the primary method for estimating causal *** estimates are expressed as beta coefficients or odds ratio(OR)with 95%*** We identified 14 plasma metabolites associated with the occurrence of MI(P<0.05),among which 8 plasma metabolites[propionylglycine levels(OR=0.922,95%CI:0.881–0.965,P<0.001),gamma-glutamylglycine levels(OR=0.903,95%CI:0.861–0.948,P<0.001),hexadecanedioate(C16-DC)levels(OR=0.941,95%CI:0.911–0.973,P<0.001),pentose acid levels(OR=0.923,95%CI:0.877–0.972,P=0.002),X-24546 levels(OR=0.936,95%CI:0.902–0.971,P<0.001),glycine levels(OR=0.936,95%CI:0.909–0.964,P<0.001),glycine to serine ratio(OR=0.930,95%CI:0.888–0.974,P=0.002),and mannose to trans-4-hydroxyproline ratio(OR=0.912,95%CI:0.869–0.958,P<0.001)]were correlated with a decreased risk of MI,whereas the remaining 6 plasma metabolites[1-palmitoyl-2-arachidonoyl-GPE(16:0/20:4)levels(OR=1.051,95%CI:1.018–1.084,P=0.002),behenoyl dihydrosphingomyelin(d18:0/22:0)levels(OR=1.076,95%CI:1.027–1.128,P=0.002),1-stearoyl-2-docosahexaenoyl-GPE(18:0/22:6)levels(OR=1.067,95%CI:1.027–1.109,P=0.001),alpha-ketobutyrate levels(OR=1.108,95%

关键词： infarction alterations diagnosis

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Systematizing Teacher Development:A Review of Foreign Language Teacher Learning

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Chinese Journal of Applied Linguistics 2024年第3期47卷 518-523,526页

作者： guang zeng Xiamen University Tan Kah Kee College

Foreign language teaching practice is developing rapidly,but research on foreign language teacher learning is currently relatively fragmented and *** book Foreign Language Teacher Learning,written by Professor Kang Yan from Capital Normal University,published in September 2022,makes a systematic introduction to foreign language teacher learning,which to some extent makes up for this *** book presents the lineage of foreign language teacher learning research at home and abroad,analyzes both theoretical and practical aspects,reviews the cuttingedge research results,and foresees the future development trend,painting a complete research picture for researchers in the field of foreign language teaching and teacher education as well as front-line teachers interested in foreign language teacher *** is an important inspiration for conducting foreign language teacher learning research in the *** this paper makes a review of the book from aspects such as its content,major characteristics,contributions and limitations.

关键词： foreign language teacher learning foreign language teacher education foreign language teaching teacher development

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Mental health and insomnia problems in healthcare workers after the COVID-19 pandemic:A multicenter cross-sectional study

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World Journal of Psychiatry 2024年第5期14卷 704-714页

作者： Wei Ding Min-Zhong Wang Xian-Wei zeng Zhen-Hua Liu Yao Meng Hui-Ting Hu Yuan Zhang Yu-guang Guan Fan-Gang Meng Jian-Guo Zhang Shu Wang Department of Public Health Liaocheng People’s HospitalLiaocheng 252000Shandong ProvinceChina Department of Neurology Shandong Provincial Hospital Affiliated to Shandong First Medical UniversityJinan 250021Shandong ProvinceChina Department of Neurosurgery Qilu Hospital of Shandong UniversityJinan 250012Shandong ProvinceChina Sleep Medicine Center Shandong Provincial Hospital Affiliated to Shandong First Medical UniversityJinan 250021Shandong ProvinceChina Department of Neurology The First Affiliated Hospital of Shandong First Medical UniversityJinan 250014Shandong ProvinceChina Department of Neurology Heze Mudan People’s HospitalHeze 274000Shandong ProvinceChina Neonatal Center Beijing Children's HospitalCapital Medical UniversityNational Center for Children's HealthBeijing 100045China Department of Neurosurgery SanBo Brain HospitalCapital Medical UniversityBeijing 100093China Department of Neurosurgery Beijing Tiantan HospitalCapital Medical UniversityBeijing 100070China

BACKGROUND Healthcare workers(HCWs)are at increased risk of contracting coronavirus disease 2019(COVID-19)as well as worsening mental health problems and *** problems can persist for a long period,even after the ***,less is known about this *** To analyze mental health,insomnia problems,and their influencing factors in HCWs after the COVID-19 *** This multicenter cross-sectional,hospital-based study was conducted from June 1,2023 to June 30,2023,which was a half-year after the end of the COVID-19 ***-stratified population-based cluster sampling was applied at the provincial level for Chinese *** such as anxiety,depression,and insomnia were evaluated by the Generalized Anxiety Disorder-7,Patient Health Questionnaire-9,and Insomnia Severity *** influencing the symptoms were identified by multivariable logistic *** A total of 2000 participants were invited,for a response rate of 70.6%.A total of 1412 HCWs[618(43.8%)doctors,583(41.3%)nurses and 211(14.9%)nonfrontline],254(18.0%),231(16.4%),and 289(20.5%)had symptoms of anxiety,depression,and insomnia,respectively;severe symptoms were found in 58(4.1%),49(3.5%),and 111(7.9%)of the ***,female sex,and hospitalization for COVID-19 were risk factors for anxiety,depression,and insomnia symptoms;moreover,death from family or friends was a risk factor for insomnia *** the COVID-19 outbreak,most[1086(76.9%)]of the participating HCWs received psychological interventions,while nearly all[994(70.4%)]of them had received public psychological *** 102(7.2%)of the HCWs received individual counseling from *** Although the mental health and sleep problems of HCWs were relieved after the COVID-19 pandemic,they still faced challenges and greater risks than did the general *** risk factors would help in providing targeted *** addition,although a major proportion of

关键词： COVID-19 Mental health Psychological symptoms Insomnia Sleep disorders Cross-sectional study Epidemiological study

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不协调广义多尺度决策系统的最优尺度组合的层次关系

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控制与决策 2024年第6期39卷 2041-2050页

作者：曾华鑫吴伟志浙江海洋大学信息工程学院浙江舟山316022 浙江海洋大学浙江省海洋大数据挖掘与应用重点实验室浙江舟山316022

多尺度信息系统是一类特殊的对象-属性值系统,数据集中的每个对象在每个属性下根据不同的尺度或粒度可呈现出不同的值,并从细粒度属性值域到粗粒度属性值域间存在粒信息变换函数.从多尺度数据集中的每个属性中选择一个满足预设条件的尺... 详细信息

多尺度信息系统是一类特殊的对象-属性值系统,数据集中的每个对象在每个属性下根据不同的尺度或粒度可呈现出不同的值,并从细粒度属性值域到粗粒度属性值域间存在粒信息变换函数.从多尺度数据集中的每个属性中选择一个满足预设条件的尺度用于最终的决策分析(这个过程称为最优尺度组合选择)是多尺度决策系统知识获取的关键问题.针对不协调广义多尺度决策系统的最优尺度组合选择问题,首先,通过引入三层思维提出广义决策类最优尺度组合和对象最优尺度组合的概念,讨论两者间的层次关系;然后,提出属性约简诱导的最优尺度组合和关键尺度组合的概念,讨论对象关键尺度组合与广义决策类关键尺度组合间的层次关系;最后,依据对象关键尺度组合与广义决策类关键尺度组合间的层次关系给出两者间互相计算的方法.

关键词：粒计算粗糙集信息系统多尺度信息系统最优尺度组合

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Neurosyphilis complicated by anti-γ-aminobutyric acid-B receptor encephalitis: A case report

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World Journal of Clinical Cases 2024年第11期12卷 1960-1966页

作者： Ya-Xiu Fang Xiao-Ming Zhou Dong Zheng guang-Hui Liu Peng-Bo Gao Xiao-Zhen Huang zhi-Cheng Chen Hui Zhang Lin Chen Ya-Fang Hu Department of Neurology The Affiliated Brain Hospital of Guangzhou Medical UniversityGuangzhou 510000Guangdong ProvinceChina Department of Neurology Nanfang HospitalSouthern Medical UniversityGuangzhou 510000Guangdong ProvinceChina

BACKGROUND Syphilis is an infectious disease caused by Treponema pallidum that can invade the central nervous system,causing *** cases of anti-N-methyl-Daspartate receptor autoimmune encephalitis(AE)secondary to neurosyphilis have been *** report a neurosyphilis patient with anti-γ-aminobutyric acid-B receptor(GABABR)*** SUMMARY A young man in his 30s who presented with acute epileptic status was admitted to a local *** was diagnosed with neurosyphilis,according to serum and cerebrospinal fluid(CSF)tests for *** 14 d of antiepileptic treatment and anti-Treponema pallidum therapy with penicillin,epilepsy was controlled but serious cognitive impairment,behavioral,and serious psychiatric symptoms were *** was then transferred to our *** Mini-Mental State Examination(MMSE)crude test results showed only 2 *** magnetic resonance imaging revealed significant cerebral atrophy and multiple fluidattenuated inversion recovery high signals in the white matter surrounding both lateral ventricles,left amygdala and bilateral ***-GABABR antibodies were discovered in CSF(1:3.2)and serum(1:100).The patient was diagnosed with neurosyphilis complicated by anti-GABABR AE,and received methylprednisolone and *** treatment,his mental symptoms were *** impairment was significantly improved,with a MMSE of 8 *** anti-GABABR antibody titer decreased to 1:*** patient received methylprednisolone and penicillin after *** months later,the patient’s condition was stable,but the serum anti-GABABR antibody titer was 1:*** This patient with neurosyphilis combined with anti-GABABR encephalitis benefited from immunotherapy.

关键词： Anti-γ-aminobutyric acid-B receptor GABABR Neurosyphilis Tissue-based assay Magnetic resonance imaging Mini-mental state examination Case report

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Clinical and molecular characterization of 10 Chinese children with congenital adrenal hyperplasia due to 11beta‑hydroxylase deficiency

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World Journal of Pediatrics 2024年第4期20卷 422-433页

作者： Wen‑Li Lu Xiao‑Yu Ma Jiao Zhang Jun‑Qi Wang Ting‑Ting Zhang Lei Ye Yuan Xiao zhi‑Ya Dong Wei Wang Shou‑Yue Sun Chuan‑Yin Li Rong‑Gui Hu guang Ning Li‑Dan Zhang Department of Pediatrics Ruijin HospitalShanghai Jiao Tong University School of MedicineNo.197Ruijin 2nd RdHuangpu DistrictShanghai 200025China Department of Pediatric Genetic and Metabolic Endocrinology West China Second University HospitalSichuan UniversityNo.20Section 3Renmin South RoadSichuan 610041China Department of Endocrine and Metabolic Diseases Shanghai Clinical Center for Endocrine and Metabolic DiseasesRuijin HospitalShanghai Jiao Tong University School of MedicineShanghai 200025China Cancer Center School of MedicineShanghai Tenth People’s HospitalTongji UniversityYanchang Zhong Lu 301St RdJing’an DistrictShanghai 200031China

Background The clinical manifestations of nonclassical 11beta-hydroxylase deficiency are very similar to those of nonclassical 21-hydroxylase *** this study,we investigated the relationship between the clinical and molecular features of congenital adrenal hyperplasia caused by 11beta-hydroxylase deficiency and reviewed the related literature,which are expected to provide assistance for the clinical diagnosis and analysis of congenital adrenal *** Clinical data for 10 Chinese patients diagnosed with congenital adrenal hyperplasia in our hospital from 2018 to 2022 were retrospectively *** examined the effects of gene mutations on protease activity and constructed threedimensional structure prediction models of *** We describe 10 patients with 11beta-hydroxylase gene mutations(n=5,46,XY;n=5,46,XX),with 10 novel mutations were *** patients received treatment at an early stage,with an average age of 2.08±1.66 years,whereas male patients received treatment significantly later,at an average age of 9.77±3.62 *** most common CYP11B1 pathogenic variant in the Chinese population was found to be c.1360C>*** mutations lead to spatial conformational changes that affect protein *** Our study found that there was no significant correlation between each specific mutation and the severity of clinical *** patients with the same gene pathogenic variant may have mild or severe clinical *** correlation between genotype and phenotype needs further ***-dimensional protein simulations may provide additional support for the physiopathological mechanism of genetic mutations.

关键词： 11β-hydroxylase deficiency CYP11B1 Enzymatic activity Phenotype-genotype correlation Threedimensional protein simulations

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