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Optimization of the Aqueous Decoction Process of Combretum micranthum Leaves

Food and Nutrition Sciences 2023年第3期14卷 277-286页

作者： Papa Guedel Faye edouard mbarick ndiaye Samba Baldé Alioune Sow Omar Khatab Cissé Nicolas Cyrille Ayessou Mady Cisse Laboratory of Water Energy Environment and Industrial Processes (LE3PI) Polytechnic Higher School Cheikh Anta Diop University of Dakar (ESP-UCAD) Dakar Senegal UFR Agronomic Sciences Aquaculture and Agrifood Technologies Gaston BERGER University Dakar Senegal National School of Agriculture Iba Der THIAM University Thies Senegal Center for Studies on Food Security and Functional Molecules (CESAM) Dakar Senegal

This work proposes to compare the extraction of total polyphenols and the coloring obtained after several series of decoction at 100°C/20min, of whole or crushed leaves of Combretum micranthum. The total phenolic content of the extracts obtained after decoction was determined by Folin’s method. The color parameters were measured using a colorimeter based on the CIELAB system. The analysis of variance (ANOVA) shows significant differences (p 0.05) on different parameters evaluated. The Minitab 19 software was used to classify the extracts according to the color parameters (L, A, and B). The results showed that the maximum of polyphenols (21.67%) was extracted in the crushed leaves after three series of decoctions while with the whole leaves the maximum of 16.17% is obtained after six series of decoctions. The concentration of total polyphenols becomes low from four series of decoctions with 0.146 g·AG·100 g-1 MS. The red and yellow coloring drops respectively by 85 and 69% with crushed leaves and 64 and 21% with whole leaves. The conductivity and the brix of the extracts fall according to the series of decoctions. These results show that for optimal use of C. micranthum leaves in traditional medicine, crushed leaves and three series of decoctions are indicated and sufficient.

关键词： Combretum micranthum Extraction Decoction Polyphenols Coloring

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Effect of Sodium Carbonate on Extraction by Aqueous Decoction of Total Polyphenols from Crushed and Whole Leaves of Combretum micranthum

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Food and Nutrition Sciences 2023年第9期14卷 812-823页

作者： Papa Guedel Faye Lahat Niang edouard mbarick ndiaye Oumar Ibn Khatab Cisse Alioune Sow Nicolas Cyrille Ayessou Mady Cisse Laboratory of Water Energy Environment and Industrial Processes (LE3PI) Polytechnic Higher School Cheikh Anta Diop University of Dakar (ESP-UCAD) Dakar Senega Center for Studies on Food Security and Functional Molecules (CESAM) Dakar Senegal National School of Agriculture Iba Der THIAM University Thiès Senegal UFR Agronomic Sciences Aquaculture and Agrifood Technologies Gaston BERGER University Saint Louis USA

Sodium bicarbonate is sometimes used to aid in the extraction of total polyphenols. Its main effect is to increase the pH of the extraction solution. Raising the pH can cause changes in the chemical structure of polyphenols. This can lead to variations in their biological properties, solubility and stability. This work studied the effect of sodium carbonate on the extraction by aqueous decoction of total polyphenols from the leaves of Combretum micranthum. The content of total phenolic compounds in the extracts was estimated by the Folin-Ciocalteu method. The color of the samples was measured using a colorimeter (type: KONICA MINOLTA. Japan) based on the CIELAB color system. The results obtained were subjected to a one-way ANOVA analysis of variance with R software version 3.2.4 Revised (2018) and Minitab-18 software. The results reveal a drop in the concentration of extracted polyphenols proportional to the addition of sodium carbonate, i.e. a drop from 3.30 to 1.04 mg·AG·100 g-1 of extract on whole leaves and 3.921 to 2.551 mg·AG·100 g-1 extract on crushed leaves. On the other hand, the intensity of the coloring of the extracts increases significantly with the addition of sodium carbonate from 0.0 g·L -1 to 0.666 g·L-1.

关键词： Baking Soda Combrutum micranthum Extraction Decoction Polyphenols

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Secondary Metabolites and Antioxidant Activity of Different Parts of the Baobab Fruit (<i>Adansonia digitata</i>L.)

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Food and Nutrition Sciences 2021年第7期12卷 732-741页

作者： edouard mbarick ndiaye Y. El Idrissi Yousra Sow Alioune Nicolas Cyrille Ayessou Hicham Harhar Mady Cisse Mohamed Tabyaoui Laboratory of Water Energy Environment and Industrial Processes (LE3PI) ESP-UCAD Dakar Center of Studies on Food Security and Functional Molecules (CESAM-RESCIF) Dakar Senegal Laboratory of Materials Nanotechnology and Environment Faculty of Sciences-Rabat Mohammed V University of Rabat Rabat Morocco

The objective of this study was to determine the polyphenol, flavonoid and tannin content and the antioxidant power of methanolic extracts from the different parts of the Senegalese baobab fruit. Phytochemical screening revealed the presence of saponosides, tannins, alkaloids, sterols, flavonoids, coumarins and total sugars in all extracts from the fruit parts. The total polyphenol content was determined by the folin-ciocalteu method. This method is based on the quantification of the total concentration of hydroxyl groups present in the extract. In an alkaline medium, the reagent of folin-ciocalteu, oxidizes the phenols to ion phenolates and partially reduces its hetero-polyacids, hence the formation of a blue complex. The absorbance is read at 765 nm against a control. The Flavonoids vere determined using aluminum trichloride and sodium hydroxide. Aluminum trichloride forms a yellow complex with flavonoids and sodium hydroxyde forms a pink complex absorbing in the visible range at 510 nm. The alternative colorimetric method based on reactions with vanillin in an acidic medium made it possible to determine the tannin content. Absorbances were measured at 500 nm. The results show that the methanolic extracts of the fibers and shell have very high polyphenol, flavonoid and tannin contents. In fact, the polyphenol contents of the fiber (159.00 ± 0.93 μg EAG/mg extract) and shell (155.39 ± 0.89 μg EAG/mg extract) were much higher than those of the pulp (27.21 ± 0.26 μg EAG/mg extract) and seeds (18.36 ± 0.07 μg EAG/mg extract). In addition, the flavonoid contents of the fibers (97.64 ± 0.40 μg EQ/mg) and of the s

关键词： Adansonia digitata L. Fruit Pulp Seeds Shell

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Impact of Storage Conditions on the Physicochemical Characteristics of Baobab (Adansonia digitata L.) Seed Oil

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Food and Nutrition Sciences 2022年第4期13卷 373-386页

作者： edouard mbarick ndiaye Papa Guédel Faye Alioune Sow Khadim Niane Seyni ndiaye Samba Baldé Omar Ibn Khatab Cisse Nicolas Cyrille Ayessou Mady Cisse Laboratory of Water Energy Environment and Industrial Processes (LE3PI) Polytechnic Higher School Cheikh Anta Diop University of Dakar (ESP-UCAD) Dakar Center of Studies on Food Security and Functional Molecules (CESAM-RESCIF) ESP-UCAD Dakar Senegal UFR of Agronomic Sciences Aquaculture and Food Technologies (S2ATA) Gaston Berger University of Saint-Louis Saint-Louis Senegal National School of Agriculture Iba Der Thiam University of Thies Thies Senegal

The evolution of some quality markers of baobab (Adansonia digitata L.) was studied. Baobab oil extracted by pressing was packaged in 30 mL non-amber glass bottles and stored at different temperatures: 20°C, 30°C and 45°C. The physicochemical parameters (acid, peroxide, iodine, saponification, refraction and color indices) were determined during three months’ storage. A significant 5% increase in acid, peroxide and saponification value was observed over time. However, the iodine value decreased. The yellowing and refractive index remained stable while storage at 45°C caused the most significant changes in chemical parameters. The results obtained show that oils stored at 20°C had the lowest acid (2.42 ± 0.26 mg KOH/g) and peroxide (0.82 ± 0.25 mEqO2/Kg) value after three months of follow-up.

关键词： Adansonia digitata L. Oil Seeds Physicochemical Storage

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Improving the Quality of Baobab Oil by Filtration on Activated Carbon from the Fruit Capsules

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Journal of Materials Science and Chemical Engineering 2024年第1期12卷 69-83页

作者： edouard mbarick ndiaye Alioune Sow Papa Guédel Faye Kalidou Ba Mouhamed Ndoye Omar Ibn Khatab Cisse Nicolas Cyrille Ayessou Mady Cisse Laboratory of Water Energy Environment and Industrial Processes (LE3PI) ESP-UCAD Dakar Senegal Laboratoire of Biological Agronomic Food Sciences and Modeling of Complex Systems (LABAAM) UFR of Agronomic Sciences Aquaculture and Food Technologies (S2ATA) Gaston Berger University of Saint-Louis Saint-Louis Senegal National School of Agriculture University Iba Der Thiam of Thiès Thiès Senegal Center of Studies on Food Security and Functional Molecules (CESAM-RESCIF) ESP-UCAD Dakar Senegal

The baobab, Adansonia digitata L., plays an important role in the economy of local populations. Nowadays, baobab seed oil is highly prized for its many cosmetic and therapeutic applications, and for its composition of unsaturated fatty acids, sterols, and tocopherols. However, it undergoes numerous reactions during production, processing, transport, and storage, leading to undesirable products that make it unstable. The aim of this study was to provide local processors with innovative solutions for the treatment of unrefined vegetable oils. To this end, an experimental device for filtering crude oil on activated carbon made from fruit capsules was designed. The results obtained after the treatment show a significant decrease at (p 2/Kg), chlorophyll concentration (1.81 to 0.50 mg/Kg) and primary and secondary oxidation products. According to these results, activated carbon’s adsorptive power eliminates oxidation products and certain pro-oxidants such as chlorophyll, resulting in a cleaner, more stable and better storable oil.

关键词： Activated Carbon Adansonia digitata L. Baobab Fruit Baobab Oil Stability

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Processes for the Clarification of the Crude Oil of Baobab Seeds Extracted by Pressing on Activated Carbon Elaborated from the Capsules of the Fruit (Adansonia digitata L.)

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Advances in Chemical Engineering and Science 2023年第2期13卷 105-118页

作者： edouard mbarick ndiaye Alioune Sow Kalidou Ba Mouhamed Ndoye Yousra El Idrissi Seyni ndiaye Hamza El Moudden Papa Guedel Faye Hicham Harhar Nicolas Ayessou Mohamed Tabyaoui Mady Cisse Laboratory of Water Energy Environment and Industrial Processes (LE3PI) ESP-UCAD ESP-UCAD Cheikh Anta Diop University Dakar Senegal Laboratory of Materials Nanotechnology and Environment Faculty of Sciences-Rabat Mohammed V University of Rabat Rabat Morocco Laboratory of Biological Agronomic Food Sciences and Modeling of Complex Systems (LABAAM) UFR of Agronomic Scienc-es Aquaculture and Food Technologies (S2ATA) Gaston Berger University of Saint-Louis Saint-Louis Senegal Higher School of Technology of El Kelaa of The Sraghna Cadi Ayyad University Marrakech Morocco

The baobab, Adansonia digitata L. plays an important role in the economy of local populations. The oil from the seeds of the baobab fruit is nowadays highly prized because of its numerous cosmetic and therapeutic applications and its composition of unsaturated fatty acids, sterols and tocopherols. However, unlike refined oils, locally extracted baobab oil has not undergone purification operations to ensure its quality. Only a filtration on special cloths is carried out after decantation. Indeed, the oil obtained after pressing is cloudy because of the presence of various impurities. It therefore requires treatment operations to make it more attractive and of higher quality. Therefore, in order to provide innovative solutions to local companies to improve the quality of vegetable oils, a study of clarification (treatment) of crude oil is necessary. An experimental device has been developed in the laboratory. It includes a glass column and a filter bed of dune sand and activated carbon. This study has shown the efficiency of the experimental device. Indeed, the activated carbon, thanks to its adsorbing power, has allowed a significant decrease in turbidity at the 5% threshold, from 14.61 NTU for the raw oil to 0.08 NTU for the oil filtered on 3% carbon and 0.033 NTU for the oil filtered on 5% carbon. That is to say an abatement higher than 95%. This decrease in turbidity could be correlated with the decrease in brown index from 187.39a for the initial crude oil to 128.53d for the oil treated with 3% activated carbon versus 187.59a for the oil filtered on cloths. The lowest brown index was observed with the filtration using 5% activated carbon (35.99b). Thus, for the yellowness index, only the filtration on 5% charcoal allowed to obtain a significant decrease in yellowness. The yellowing index of the oil with 5% was 44.67b against 79.04a for the oil filtered with 3% activated carbon, 86.33a fo

关键词： Activated Carbon Baobab Oil Clarification Filtration Process

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Valorization of Natural Residue into Activated Carbon:Example of the Shells of the African Baobab Fruit(Adansonia digitata)L.

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材料科学与工程（中英文A版） 2022年第2期12卷 41-54页

作者： edouard mbarick ndiaye Kalidou Ba Alioune Sow Adama Diop Yousra El Idrissi Hamza El Moudden Papa Guedel Faye Hicham Harhar Nicolas Ayessou Mohamed Tabyaoui Mady Cisse Laboratory of Water Energy Environment and Industrial Processes(LE3PI) ESP-UCADESP-UCADCheikh Anta Diop UniversityBP 5085DakarSenegal Laboratory of Biological AgronomicFood Sciences and Modeling of Complex Systems(LABAAM)UFR of Agronomic SciencesAquaculture and Food Technologies(S2ATA)Gaston Berger University of Saint-LouisNgallele RoadBP 234Saint-LouisSenegal Laboratory of Materials Nanotechnology and EnvironmentFaculty of Sciences-RabatMohammed V University of RabatBP 1014RabatMorocco Higher School of Technology of El Kelaa of the Sraghna Cadi Ayyad UniversityBP 104El Kelaa of the SraghnaMorocco

This study deals with the valorization of natural residues into activated carbon prepared from waste“Baobab fruit shell”from the Fatick Region,***,after the preparation of the baobab shell,a chemical activation with orthophosphoric acid H3PO4(85%)was performed followed by pyrolysis at 530°*** eliminate possible carbonization residues,the activated carbons were impregnated in 0.1 M hydrochloric acid and/or soda solutions and then washed thoroughly with distilled water to obtain a pH between 6.5 and *** latter were then dried in an oven at 105°C for 24 h.A characterization was carried out to determine the moisture content,the ash content,the iodine and methylene blue indices,the surface functions and the pH at zero charge point(pHpzc).The moisture and ash contents were 1.87%and 0.72%,*** iodine and peroxide indices obtained were 939,09 mg/g and 575.73 mg/g,*** function analysis by Boehm’s method showed that the acidic functions were higher than the basic functions and their pHpzc was lower than *** best efficiency of methylene blue removal was 99.75%and was obtained with a mass of 0.150 g of activated carbon,pH equal to 10,an initial concentration of methylene blue of 200 mg/L and a contact time of 35 min.

关键词： Orthophosphoric acid activated carbon baobab fruit shell pyrolysis valorization

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Pleomorphic Nasopharyngeal Liposarcoma: An Aggressive Tumor

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International Journal of Otolaryngology and Head & Neck Surgery 2024年第1期13卷 11-15页

作者： Mame Sanou Diouf Sall Ahmadou Cheikhou ndiaye Ciré Thiam Amadou Abdoulaye Diop Deguenonvo Richard edouard Alain Diom Evelyne Siga ndiaye Malick Diallo Bay Karim Diouf Raymond ENT and Cervicofacial Surgery Department Idrissa Pouye General Hospital Grand-Yoff Dakar Senegal ENT Department Diamniadio Children’s Hospital Dakar Senegal ENT clinic Lamine Sine Diop Dakar Senegal ENT Department and Cervico-Facial Surgery H&#244pital de la paix Ziguinchor Senegal ENT and Cervicofacial Surgery Department Albert Royer Children’s Hospital Dakar Senegal

Nasopharyngeal liposarcoma is an extremely rare clinical entity. Less than ten cases have been reported in the literature. It mainly occurs in humans. The non-specificity of the clinical and radiological signs explains the difficulty of the diagnosis confirmed by anatomopathological and immunohistochemical examinations. Its pathogenesis remains obscure and often correlates with genetic abnormalities. Pleomorphic liposarcoma is its rarest subtype, remarkable for its aggressiveness and rapidity of growth. Complete surgical excision remains the treatment of choice. We report a case of liposarcoma whose diagnosis was made during histological examination coupled with immunohistochemistry. .

关键词： Liposarcoma Nasopharynx Pathology Immunohistochemistry

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Improving Postpartum Haemorrhage Management Using Simulation in Senegal: Midterm Results

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Open Journal of Obstetrics and Gynecology 2017年第13期7卷 1292-1299页

作者： Mamour Gueye Moussa Diallo Mame Diarra ndiaye Gueye Omar Gasama Abdoul Aziz Diouf Mouhamadou Mansour Niang Mohamed Diadhiou Astou Coly Niassy Serigne Modou Kane Gueye Marie edouard Faye Dieme Magatte Mbaye Philippe Marc Moreira Alassane Diouf Jean Charles Moreau Gynecologic and Obstetric Clinic Aristide Le Dantec Teaching Hospital Cheikh Anta Diop University Dakar Senegal

Objective: To assess a training approach in Emergency Obstetric and Neonatal Care (EmONC) to strengthen skills of healthcare providers and reduce maternal mortality. Materials and methods: The approach was based on the skills training using the so-called “humanist” method and “life saving skills”. Simulated practice took place in the classroom through thirteen clinical stations summarizing the clinical skills on EmONC. The evaluation was done in all phases and the results were recorded in a database to document the progress of each learner. Results: We trained 432 providers in 10 months. The increase in technical achievements of each participant was documented through a database. The combination of training based on the model “learning by doing” has ensured learning and mastering all EmONC skills particularly postpartum haemorrhage management and reduced missed learning opportunities. Conclusion: The impact of training on postpartum haemorrhage management and maternal mortality is a major challenge in terms of prospects.

关键词： Emergency Obstetric Care Postpartum Haemorrhage Training Simulation

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