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复方碘口腔喷雾原位膜的制备及促口腔溃疡修复评价

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中国药科大学学报 2024年

作者：张小军黄山芩郭潇涵季梦菲沈雁陈大全许颖 1.江苏大学药学院 2.中国药科大学药学院 3.烟台大学药学院江苏大学药学院中国药科大学药学院烟台大学药学院

采用原位凝胶技术，制备了新型复方碘口腔喷雾原位膜，用于发挥缓释作用，并促进口腔溃疡创面修复。首先以喷雾状态和成膜时间为指标，对喷雾药液的处方和工艺进行优化。以成膜时间和药膜黏附性为评价指标对药液混合比例进行考察。并对... 详细信息

采用原位凝胶技术，制备了新型复方碘口腔喷雾原位膜，用于发挥缓释作用，并促进口腔溃疡创面修复。首先以喷雾状态和成膜时间为指标，对喷雾药液的处方和工艺进行优化。以成膜时间和药膜黏附性为评价指标对药液混合比例进行考察。并对最优处方制备的复方碘口腔喷雾药液的药物含量、稳定性、pH、喷雾效果，及原位膜的成膜时间、溶解性、吸湿性、保湿性、体外释放等理化性质进行考察；此外，通过细胞实验考察了成膜材料的生物相容性及复方碘口腔喷雾原位膜的促迁移效果；采用兔口腔溃疡模型，对复方碘口腔喷雾在体成膜效果及促修复效果进行评价。实验结果显示，最优处方制备的药液A和药液B的pH分别为6.2.0}± 0.02. 6.42.± 0.03.符合正常口腔黏膜pH范围；稳定性好，具有良好的喷雾状态；药液B中碘含量为（{3.96 ± 0.0{3.mg/mL；原位膜体外成膜时间为（{3.8.3.± 3.6）s，口腔内成膜时间为（{3.3.3.± 4.6）s；2. h溶解率为（87.3.3.± {3.74）%，吸湿率为（{3.4.{3. ± 7.{3.）%，保湿率为（2..85 ± 2.50）%；复方碘口腔喷雾原位膜中碘含量为（47.42.± 0.3.）mg/g；具有良好的柔韧性和黏附性，并具有一定的缓释效果。细胞实验中，原位膜表现出良好的促成纤维细胞迁移作用。兔口腔溃疡实验表明，复方碘口腔喷雾在体可快速成膜，并可显著促进口腔溃疡修复。本研究所开发的复方碘口腔喷雾原位膜，制备工艺稳定，并可有效促进口腔溃疡创面修复，为口腔黏膜制剂的研究和开发提供了新思路，并具有良好的转化前景。

关键词：口腔喷雾原位膜复方碘口腔溃疡缓释促修复

Solvothermal synthesis of nanocrystalline FeS_2

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Science china(Physics,Mechanics & Astronomy) 2005年第2期48卷 188-200页

作者： CHEN Yanhua1. ZHENG Yufeng1. ZHANG Xiaogang2. SUN Yanfei1.& dong youzhong11. Physics Department of{1.,{2.,{3. 2. Institute of Applied Chemistry of{1.,{2.,{3. Physics Department of xinjiang university Urumqi 830046 China Institute of Applied Chemistry of xinjiang university Urumqi 830046 China

This paper reports on the synthesis of the nanocrystalline FeS2.via a solvent-thermal process. Using FeSO4 and NH2.SNH2.as precursors and polyvinyl- pyrrolidone (PVP) as a protective agent (dispersant), we have successfully synthesized nanocrystalline FeS2.both under acidic conditions (pH = 5) and under alkali conditions (pH = 1.) at various temperatures and for different time in alcohol-water solution. X-ray diffraction (XRD), Transmission electron microscopy (TEM) and Ultraviolet Visible (UV-VIS) spectroscopy were used to characterize the morphology, structure, particle size and optical characterization of sample synthesized under acidic condition, and the XRD pattern was refined by Rietveld method. The experimental result shows that nanocrystalline FeS2.with uniform size, highly crystallized quality and excellent dispersivity has been synthesized at 2.0℃for 3. h.

关键词： FeS2 (Pyrite), solvothermal, PVP, the Rietveld method.

The regular representation and regular covariant representation of crossed products of Woronowicz C^(*)-algebras

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Science china Mathematics 2005年第9期48卷 1245-1259页

作者： ZHANG Xiaoxia~(1.2. & GUO Maozheng~(1.3. 1. School of Mathematical Sciences,Peking university,Beijing 1.0871.{1. 2. Department of Mathematics,Yantai university,Yantai 2.4005,{1. 3. LMAM,Peking university,Beijing 1.0871.{1. 1. School of Mathematical Sciences Peking University 100871 Beijing China 2. Department of Mathematics Yantai University 264005 Yantai China 3. LMAM Peking University 100871 Beijing China

In this paper,it is shown that the regular representation and regular covariant representation of the crossed products A×α G correspond to the twisted multiplicative unitary operators,where A is a Woronowicz C~*-algebra acted upon by a discrete group ***,it is also shown that the regular covariant C~*-algebra is the Woronowicz C~*-algebra which corresponds to a multiplicative ***,an explicit description of the multiplicative unitary operator for C(SU_q(2. )×α (?) is given in terms of those of the Woronowicz C~*-algebra C(SU_q(2. ) and the discrete group G.

关键词： multiplicative unitary operator, Woronowicz C*-algebra, crossed product.

CMC surfaces in the hyperbolic 3.space

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Chinese Science Bulletin 1998年第7期43卷 547-550页

作者： YU Zuhuan 1. 2.and LI Zhenqi 1. 3.1. Institute of Mathematics, Fudan university, Shanghai 2.043.,{1. 2. Department of Mathematics,Sichuan Union university, Chengdu 61.064,{1. 3. Department of Mathematics, Nanchang university, Nanchang 3. nstitute of Mathemalics Fudan University Shanghai China Department of Mathematics Sichuan Union University Chengdu China Department of Mathematics Nanchang University Nanchang China

CMC-H surfaces satisfying H≥1.are studied. It is proved that these surfaces possess a natural representation which is a generalization of the Bryant’s result.

关键词： hyperbolic space CMC surface Weierstrass representation.

Study on the two and three-parameter working stability regions of 3.-TZP suspension

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Science china(Technological Sciences) 2006年第5期49卷 547-568页

作者： CHEN Youqiang1. 2. ZHANG Xinni3. CHEN Sha’ou3.& QI Ping3.1. Department of Chemistry, Qingdao {2., Qingdao 2.6071.{1. 2. Department of Chemistry, Tsinghua {2., Beijing 1.0084,{1. 3. Department of Physics, Qingdao {2., Qingdao 2.6071.{1. 1. Department of Chemistry Qingdao University Qingdao 266071 China 2. Department of Chemistry Tsinghua University Beijing 100084 China 3. Department of Physics Qingdao University Qingdao 266071 China

We determined the variation tendency of viscosity (η) at various solids load- ing (α) for 3.-TZP suspension as a function of dispersant concentration (Cw) using vis- cosity measurement, measured the diameter of particles as a function of Cw in very dilute suspension using light scattering method, and obtained the surface features of the sedi- ment of suspension with different Cw using SEM. We also discussed the influence of the microstructure of adsorbed polymer layers on particles and their interactions in the dis- persing medium on the stability of suspension. Then two different stable states and two different unstable states for 3.-TZP suspension were given. Accordingly, the (Cw, η), (Cw, α), and (α, η) two-parameter, and (Cw, α, η) three-parameter stability maps were con- structed. Based on the DLVO theory calculations, the dispersant concentration, particle distance (r), and interparticle potential energy (VT) maps with various solids loading for 3.-TZP aqueous suspension were also constructed. In (Cw, r) two-parameter coordinate system, the stable motion region map for particles was established. The Cw, α, and VT,max (the highest potential energy) surface of the potential barrier map was obtained through calculation and simulation on the basis of the surfaces of Cw, r, VT maps introduced above. The (Cw, α) two-parameter stability map was then obtained from the Cw, α, VT,max map. The results showed that this theoretical map can qualitatively prove the experimentally obtained results—the existence of different dispersed states of particles in suspension system and the variation tendency of suspension stability with changing each parame- ter—were reasonable.

关键词： 3.-TZP, suspension, stability, DLVO theory, interparticle potential energy.

Direct CP violation in hadronic B decays

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Science china(Physics,Mechanics & Astronomy) 2006年第3期49卷 357-366页

作者： HONG Bihai1.2.& Lü Caidian3.1. Department of Physics, Lishui {2., Lishui 3.1}000,{1. 2. Department of Physics, Shanghai Jiaotong {2., Shanghai 2.003.,{3. 3. Institute of High Energy Physics, Beijing 1.0049,{1. Department of Physics Lishui University Lishui 323000 China Department of Physics Shanghai Jiaotong University Shanghai 200030 China Institute of High Energy Physics Beijing 100049 China

There are different approaches for the hadronic B decay calculations, recently. In this paper, we upgrade three of them, namely factorization, QCD factorization and the perturbative QCD approach based on kT factorization, using new parameters and full wave functions. Although they get similar results for many of the branching ratios, the direct CP asymmetries predicted by them are different, which can be tested by recent experimental measurements of B factories.

关键词： CP violation hadronic B decay factorization.

Stress distribution rule of roadway affected by overhead mining in gently inclined coal seams group

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中国有色金属学会会刊：英文版 2011年第S3期21卷 529-535页

作者： KANG Qin-rong1. 2. TANG Jian-xin1. 2. HU Hai1. 2. ZHANG Wei-zhong1. 3.1. College of Resource and Environmental Sciences, Chongqing university, Chongqing 40003.,{1. 2. State Key Laboratory of Coal Mine Disaster Dynamics and Control, Chongqing university, Chongqing 40003.,{1. 3. School of Safety Science and Administration, Zhongnan university of Economics and Law, Wuhan 43.074,{1. [a] College of Resource and Environmental Sciences Chongqing University Chongqing 400030 China [b] State Key Laboratory of Coal Mine Disaster Dynamics and Control Chongqing University Chongqing 400030 China [c] School of Safety Science and Administration Zhongnan University of Economics and Law Wuhan 430074 China

In light of the severe deformation and destruction of the district raise tunnel in the mining area at the northern part of the Lubanshan colliery, by the theoretic analysis and numerical simulation, both the mining stress distribution in seams group and the deformation and destruction mechanism of floor district raise were investigated. The results show that, at the maximum vertical distance of 40 m, the abutment stress has an influence on the recovery of 2. and 3. coal seam and 8# coal seam at distance of 3. m. As a result, the recovery of 8# is rather than those of 2. or 3. coal seam, which contributes to the deformation and destruction of the district raise surrounding rock. The major factors affecting the abutment stress include the mining depth, mining height, residual gob space, adjacent working faces and short spacing coal seam recovery.

关键词： coal seams group stress distribution district raise surrounding rock deformation and destruction abutment stress

Online uniform machine covering with the known largest size

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Progress in Natural Science:Materials International 2007年第11期17卷 1271-1278页

作者： Cao Shunjuan1.2.and Tan Zhiyi1.3.1. Department of Mathematics, Zhejiang university, Hangzhou 3.0}02.,{1. 2. Department of Mathematics, Zhejiang Forestry university, Hangzhou 3.0}3.0,{1. 3. State Key Laboratory of CAD & CG, Zhejiang university, Hangzhou 3.0}02.,{1.) Department of Mathematics Zhejiang University Hangzhou 310027 China Department of Mathematics Zhejiang Forestry University Hangzhou 311300 China State Key Laboratory of CAD & CG Zhejiang University Hangzhou 310027 China

This paper investigates the semi-online scheduling problem with the known largest size on two uniform machines. The objective is to maximize the minimum machine completion time. Both lower bounds and algorithms are given. Algorithms are optimal for the majority values of s≥1. where s is the speed ratio of the two machines. The largest gap between the competitive ratio and the lower bound is about 0.064. Moreover, the overall competitive ratio 2.matches the overall lower bound.

关键词： scheduling and covering uniform machine design and analysis of algorithm online competitive ratio

Size distributions and magic number characteristics of cluster configurations formed during solidification processes of liquid metal Al

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Science china(Technological Sciences) 2006年第2期49卷 172-187页

作者： LIU Rangsu1. LIU Fengxiang1. {2. Kejun1. ZHENG Caixing1. LIU Hairong2. PENG Ping2.& LI Jiyong3.1. Department of Physics, Hunan {1., Changsha 41.082.{2. 2. Department of Material Science and Engineering, Hunan {1., Changsha 41.082.{2. 3. Department of Chemistry, Hunan {1., Changsha 41.082.{2. 1. Department of Physics Hunan University Changsha 410082 China 2. Department of Material Science and Engineering Hunan University Changsha 410082 China 3. Department of Chemistry Hunan University Changsha 410082 China

A molecular dynamics simulation study has been performed for a large systemconsisting of 1.0000 liquid metal Al atoms to investigate the formation and magic numbercharacteristics of the cluster configurations formed during the rapid solidification processes. Thecluster-type index method (CTIM) has been adopted to describe various types of clusterconfigurations. The results indicate that the icosahedral clusters (1. 0 1. 0) and theircombinations play the most important role in the rnicrostructure transitions during solidificationprocesses; for the cluster configurations of different levels formed by various combinations withdiffering numbers of basic clusters, their size distributions possess obvious magic number sequencewhich is in turn as 1.(1.), 1.(2.0}, 2.-2.(2.), 3.6}3.(3.6}, 3.-40, 43.44, 48..., (those in bracket arethe corresponding value in liquid state); the magic numbers correspond to the peak value positionsof the cluster numbers for corresponding level formed with various combinations by 1. 2. 3. 4, 5, 6,7, ...basic clusters, respectively. This magic number sequence is in good agreement with theexperimental results obtained by Harris et al. At the same time, this simulation study also gives ascientific and reasonable explanation to these experimental results.

关键词： liquid metal, solidification processes, cluster configuration, magic numbers, computer simulation.