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Coating powder beds with liquids and foams based on viscous formulations using a twin screw mixer:A continuous process study

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Particuology 2024年第10期93卷 364-376页

作者： Mohamed S.Manga Dimitrios Kontziampasis Mustafa Al-Maqdad Sean Clifford Serafim Bakalis david W.york School of Chemical and Process Engineering Faculty of Engineering and Physical SciencesUniversity of LeedsLeedsLS29JTUK School of Mechanical Engineering Faculty of Engineering and Physical SciencesUniversity of LeedsLeedsLS29JTUK School of Science and Engineering University of DundeeDD14HNDundeeScotlandUK Dundee International Institute of Central South University Tongzipo RoadCentral South UniversityChangshaHunan410013China Department of Chemical Engineering School of EngineeringUniversity of NewcastleNewcastleNE17RUUK School of Chemical Engineering University of BirminghamBirminghamB152TTUK Department of Chemical Engineering Faculty of EngineeringUniversity of NottinghamNG72RDUK

Coating with viscous formulations has been essential in numerous industries as it can be a means for providing functionalization, additional properties, as well as other benefits. However, there have been scarce studies that have investigated and proposed methodologies in literature. Continuous coating of powders with viscous liquids poses as a promising technology, which has been mentioned in some studies, but has not yet been thoroughly investigated. This paper employs the use of image processing and analysis, in combination with statistical analysis of particles to evaluate the effectiveness of foams and liquids as a means of coating powder beds. Two different sizes of twin screw mixers that are working in continuous operation are employed, and a new continuous foaming device is fabricated and used for the experiments of coating. The effect of materials and process parameters (as for example rotational speed, and flowrate) on the quality of coating are investigated. Image analysis is used to assess the coating quality. The results clearly showcase the potential of using twin screw mixers for coating purposes and not only for mixing. The hypothesis that using large bubble foams to improve the coating of viscous liquids on particles is proven correct, as they provide higher quality coatings compared to their equivalent liquids, when used in the twin screw mixer. Surprisingly, using a larger scale twin screw mixer, does not show a substantial effect on the mixing, regarding quality, however there is still a requirement for mix optimization for achieving scale-up of this process. These results provide a new pathway for coating powders with viscous formulations in industrial applications, requiring less energy and effort in this process, and can pave the way towards introducing more sustainable industrial methodologies for coating.

关键词： Powder coating Continuous processing Viscous liquid Foam Image analysis Positron emission particle traking(PEPT)

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ZnO nanofluids-A potential antibacterial agent

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Progress in Natural Science:Materials International 2008年第8期18卷 939-944页

作者： Malcolm Povey david york Procter Department of Food Science University of Leeds Leeds LS2 9JT UK Procter and Gamble Newcastle Technical Centre Newcastle-upon-Tyne NE12 9TS UK

In this work, ZnO nanofluids were produced by a medium mill with a pH value of about 7.2 and characterized by Nano-Sizer and SEM. After milling, ZnO nanofluids were formed with an average particle size of 198.4 nm. The ZnO nanofluids used for testing were stored for different periods (1-, 90- and 120-day) and kept in different conditions (under the light and in the dark). The antibacterial activities of these ZnO nanofluids were evaluated by estimating the reduction ratio of the bacteria treated with ZnO. The results showed that the ZnO nanofluid stored for 120 days under the light had the best antibacterial behavior against Escherichia coli DH5a. SEM images suggest that an interaction between the ZnO particles and the E. coli bacteria cells caused by electrostatic forces might be a mechanism.

关键词： Antibacterial Nanofluids ZnO E. coli Photocatalysis

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The impact of raw material properties and process conditions on the color of a powdered formulated detergent product

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Particuology 2019年第4期17卷 35-41页

作者： Mohamed S. Manga david Willis Nurafiqah M. Ali david W. york School of Chemical and Process Engineering Faculty of Engineering University of Leeds Woodhouse Lane Leeds LS2 9JT United Kingdom

The appearance of deterge nt powder plays an importa nt role in con sumer perception of powder effectiveness for cleaning applications. In this study, we investigated the influence of numerous formulation and processing conditions on product discoloration. Product color was scrutinized using the L*a*b* color space, and in particular, L* and b*. Particle size, the method for introducing the optical brightener, and the raw material grade were very important in con trolling the optical properties of detergent granules. As the particle size decreased, the light reflected to the observer appeared brighter and bluer. This was observed as increased whiteness from L*= 84.03 with a particle size of >841 μm to L*= 90.59 with a particle size of <250 μm. Reducing the level of impurities found in the raw materials by changing the material source also improved color definition. A key finding is that the optical brightener should be applied by spraying and prepared by dispersion rather than dissolution. This improves the distribution within the granules and increases the whiteness when compared with pouring the brightener into the agglomeration vessel. Additional spray applications highlighted that brightener on the granule surface influenced whiteness more than embedded brightener. In addition, we report on the effects of the drying temperature and mixer impeller speed on powder color.

关键词： Detergent powder Powder processing Powder discoloration Optical brightener Characterization

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Composite microcapsules with enhanced mechanical stability and reduced active ingredient leakage

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Particuology 2016年第3期14卷 40-46页

作者： Yue Long Kai Song david york Zhibing Zhang Jon A. Preecea School of Chemistry University of Birmingham Edgbaston Birmingham B 15 2TT UK Laboratory of Bio-lnspired Smart Interface Science Technical Institute of Physics and Chemistry Chinese Academy of Sciences Beijing 100190 China Institute of Particle Science & Engineering School of Process Environmental and Materials Engineering University of Leeds Leeds LS2 9J UK School of Chemical Engineering University of Birmingham Edgbaston Birmingham B15 2TT UK

A calcium shellac （CS） matrix was used to encapsulate polymeric melamine formaldehyde microcapsules （A） or CaCO3 nanoparticles-stabilized microcapsules （B）, both of which encapsulated an oil-based active ingredient, producing A-CS or B-CS composite microcapsules. The mechanical properties and oil release profiles of the composite microcapsules were evaluated. The composite microcapsules showed enhanced mechanical stability and reduced leakage of the active ingredient hv one order of magnitude.

关键词： Composite Microcapsule Calcium shellac Mechanical property Control release Perfume oil

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Sorption of inorganic nanoparticles in woven cellulose fabrics

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Particuology 2009年第2期7卷 121-128页

作者： Dan H. Marsh D. Jason Riley david york Andrew Graydon School of Chemistry University of NottinghamUniversity ParkNottinghamNG7 the School of Chemistry University of BristolCantocks CloseBristolBS8 1TSUK.2RDUK Department of Materials Imperial College LondonExhibition RoadLondonSW7 2AZUK the School of Chemistry University of BristolCantocks CloseBristolBS8 1TSUK. Procter & Gamble Technical Centres Ltd. Newcastle Upon TyneNE12 9TSUK

Titanium dioxide was deposited from aqueous suspension onto cellulosic surfaces. Titania was sourced from Degussa （P25TM, 70：30 anatase：rutile）. Dry uptake of particles was shown to be rapid and dominant with one-third of the deposition occurring in less than 30 s and over one-half in the first minute. Isotherms were recorded to compare the rate of titanium deposition on dry and pre-wetted cotton. In the dry case uptake reached a maximum in 30 min whereas in the pre-wetted case the uptake was seen to continue beyond 180 min. A broad trend of higher deposition occurring at lower pH was seen, corresponding to the region where surface charges were opposite and thus attractive. Dry pickup was less significant at high pH. The response to varying ionic strength was complex and was attributed to the combined effect of charge screening, particle aggregation and consequent particle entrapment or occlusion. Titania deposition into the interstices of woven cotton sheets resulted in the formation of inorganic, nanoparticulate skeletons which could be isolated by controlled combustion of the cellulose and thus cotton was suggested to have potential for the templated synthesis of high surface area semiconductor materials.

关键词： Titania Cellulose Sorption Zeta potential Templated material

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Effects of laponite and silica nanoparticles on the cleaning performance of amylase towards starch soils

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Particuology 2009年第6期7卷 459-465页

作者： Wai Peng Lee Alberto Martinez Dan Xu Anju Brooker david W. york Yulong Ding Institute of Particle Science Engineering University of Leeds Leeds LS2 9IT UK Procter Gamble Newcastle Technical Centre Newcastle upon Tyne NE12 9TS UK

This work aims to understand the effect of nanoparticle-enzyme interactions and how such interactions affect starch based soil removal. Silica and laponite are used as the model nanoparticles, and s-amylase is employed as the model enzyme. The results show that, if the nanoparticles and enzyme are added simultaneously, laponite enhances the enzyme performance toward starch soil removal, whereas silica imposes a small effect on the enzymatic activity towards the same soil substrates. However, when nanoparticles are added first, the enzyme activity is not affected much by laponite but is hindered significantly by silica nanoparticles. Furthermore, sequential addition of the enzyme followed by silica nanoparticles improves soil removal. Electron microscopic analyses, measurements of the enzyme activity in suspen- sions of nanoparticles, and particle size characterisation suggest that dense coverage of soil surface by the silica nanoparticles be likely a mechanism for the experimentally observed hindrance of soil removal when silica nanoparticles are added before enzyme.

关键词： Enzyme Nanoparticles Laponite Silica Interaction Starch

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Uncovering the functional basis of mantids that resemble plants

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Science China(Life Sciences) 2024年第1期67卷 215-216页

作者： Wei Zhang david JLohman State Key Laboratory of Protein and Plant Gene Research School of Life SciencesPeking UniversityBeijing 100871China Peking-Tsinghua Center for Life Sciences Academy for Advanced Interdisciplinary StudiesPeking UniversityBeijing 100871China Biology Department City College of New YorkCity University of New YorkNew York 10031 USA PhD Program in Biology City University of New YorkNew York 10016 USA Entomology Section National Museum of Natural HistoryManila 1000Philippines

Convergent evolution frequently causes one species to look like another to increase its ***“adaptive resemblance”takes many forms:edible species mimic noxious ones to avoid predation;camouflaged patterns allow an organism to blend into its environment;and being mistaken for an inedible object allows a prey species to masquerade as a twig or dead *** resemblance is relatively common in insects,which comprise around 60%of known species.

关键词： species functional mimic

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Learning to bag with a simulation‐free reinforcement learning framework for robots

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IET Cyber-Systems and Robotics 2024年第2期6卷 52-66页

作者： Francisco Munguia-Galeano Jihong Zhu Juan david Hernández Ze Ji Cooper Group University of LiverpoolLiverpoolUK School of Physics Engineering and Technology University of YorkYorkUK School of Computer Science and Informatics Cardiff UniversityCardiffUK School of Engineering Cardiff UniversityCardiffUK

Bagging is an essential skill that humans perform in their daily ***,deformable objects,such as bags,are complex for robots to manipulate.A learning-based framework that enables robots to learn bagging is *** novelty of this framework is its ability to learn and perform bagging without relying on *** learning process is accomplished through a reinforcement learning(RL)algorithm introduced and designed to find the best grasping points of the bag based on a set of compact state *** framework utilises a set of primitive actions and represents the task in five *** our experiments,the framework reached 60% and 80% success rates after around 3 h of training in the real world when starting the bagging task from folded and unfolded states,***,the authors test the trained RL model with eight more bags of different sizes to evaluate its generalisability.

关键词： reinforcement learning robot learning robotics

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Role of buccal mucosa graft ureteroplasty in the surgical management of pyeloplasty failure

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Asian Journal of Urology 2024年第3期11卷 373-376页

作者： Matthew Lee Elizabeth Nagoda david Strauss Matthew Loecher Michael Stifelman Lee Zhao Department of Urology Lewis Katz School of MedicineTemple UniversityPhiladelphiaPAUSA Department of Urology Hackensack Meridian School of MedicineHackensack University Medical CenterHackensackNJUSA Department of Urology New York University Grossman School of MedicineNew York University Langone Health SystemNew YorkNYUSA

Objective:Secondary pyeloplasty for recurrent ureteropelvic junction obstructions may be a safe and feasible surgical option for *** study aimed to demonstrate outcomes of utilizing a non-transecting buccal mucosa graft ureteroplasty for management of recurrent ureteropelvic junction obstruction after prior failed ***:We performed a retrospective review of our Collaborative of Reconstructive Robotic Ureteral Surgery database for all consecutive patients who underwent buccal mucosa graft ureteroplasty between April 2012 and June 2022 for management of recurrent ureteropelvic junction obstructions after prior failed *** primary outcome included surgical success which was defined as the absence of flank pain and no obstruction on ***:Overall,ten patients were included in our *** median stricture length was 2.5(interquartile range[IQR]1.8-4.0)*** median operative time was 230.5(IQR 199.5-287.0)min and median estimated blood loss was 50.0(IQR 28.8-102.5)*** a median follow-up of 10.3(IQR 6.2-14.8)months,80%of patients were surgically successful and there were no major(ClavieneDindo Grade>2)***:Buccal mucosa graft ureteroplasty is a valuable non-transecting surgical option for patients with recurrent ureteropelvic junction obstructions who failed prior pyeloplasty and has comparable outcomes to the literature regarding standard transecting techniques.

关键词： Ureteral obstruction Buccal mucosagraft Pyeloplasty Robotic Stricture

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Women in visual neural regeneration research

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Neural Regeneration Research 2025年第2期20卷 489-490页

作者： Tonia S.Rex david J.Calkins Vanderbilt Eye Institute Vanderbilt University Medical CenterNashvilleTNUSA

The year 2024 marks the 60^(th)anniversary of Title IX and 25 years since the New york Times revealed bias against female faculty members at the Massachusetts Institute of *** take an opportunity here to examine the state of gender bias in a relatively new yet already prominent field,neural regeneration in the visual system,for which there is a well-defined context useful for this *** National Eye Institute(NEI)provided the first round of research funding for its Audacious Goals Initiative(AGI)on visual neural regeneration in 2013 and the last round in ***,we focus on this *** sources included PubMed,the National Science Foundation(NSF),the NEI,the Blue Ridge Institute for Medical Research and data from the major professional organization for eye and vision research,the Association for Research in Vision and Ophthalmology(ARVO).

关键词： neural visual Times

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