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Journal of Iron and Steel Research International 2024年第6期31卷 1502-1513页

作者： Bo-lin Yang Chang-liu Kuang Zheng-long Liu Chao Yu cheng-ji deng Jun Ding The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081HubeiChina

ZrB_(2)-based ceramic composites were prepared by spark plasma sintering using ZrB_(2) powder prepared by molten salt method as raw material and SiC and nano-graphite as *** effects of nano-graphite addition on the physical properties and oxidation resistance of ZrB_(2)-based ceramic samples were *** results show that the addition of an appropriate amount of nano-graphite can effectively improve the density of ZrB_(2)-based ceramic composites and improve the physical properties of the *** flexural strength of the ceramic sample with 8 vol.%nano-graphite reached 418.54 MPa,which was 53.14% higher than that of ZrB_(2)-SiC ceramic material(273.31 MPa),and its oxidation resistance was also significantly *** demonstrats that the addition of an appropriate amount of nano-graphite can effectively improve the physical properties and oxidation resistance of ZrB_(2)-SiC ceramic *** prolonging its service life in application and promoting the development of ZrB_(2)-based ceramic composites,it is of great significance for clean steel smelting.

关键词： ZrB_(2)-SiC-graphite electrode ceramic ZrB_(2)-based ceramic composite Nano-graphite Physical property Oxidation resistance

A review on graphite surface modification methods towards low carbon-containing refractories

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Journal of Iron and Steel Research International 2024年第6期31卷 1291-1303页

作者： Ting-ting Zhang Jun Ding Bei-yue Ma Zheng-long Liu Chao Yu cheng-ji deng The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081HubeiChina School of Metallurgy Northeastern UniversityShenyang 110819LiaoningChina

The rapid development of iron and steel metallurgy technology has promoted the continuous innovation and iteration of carbon-containing refractories for clean steel *** meet the high-quality requirements for clean steel production and full exploit the performance advantages of carbon-containing refractories in dynamic smelting environment,it is necessary to explore the role of graphite and modified graphite in carbon-containing *** on this,graphite surface modification methods,including surfactants,surface oxidation,and surface coating,and their applications in carbon-containing refractories are *** advantages and disadvantages of each method are analyzed for practical ***,combined with the existing problems,the application prospect of improved graphite in carbon-containing refractories is discussed.

关键词： Graphite Carbon-containing refractory Clean steel Surface modification Service performance

Effect of micro-Al_(2)O_(3) powders on oxidation and corrosion behaviors of low-carbon MgO-C refractories

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Journal of Iron and Steel Research International 2024年第6期31卷 1522-1534页

作者： Yang Chen Zeng-yi Li Hao-bo Tan Yu-ran Fu Jun Ding cheng-ji deng Chao Yu School of Materials Science and Engineering Hunan Institute of TechnologyHengyang 421002HunanChina The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081HubeiChina

To solve the problem of poor high-temperature service performance caused by low carbonization of MgO-C refractories,low-carbon MgO–C refractories with excellent thermal shock,oxidation and corrosion resistances were successfully designed by using SiC whiskers as reinforcing phases and introducing micro-Al_(2)O_(3) powders as *** results indicated that the addition of micro-Al_(2)O_(3) powders optimized the internal structure of the material,like the columnar β-Si_(3)N_(4) with a stepped distribution and the mosaic structure formed between granular and flaky Mg_(2)SiO_(4),which synergistically strengthened and toughened the material and gave the material excellent mechanical properties and thermal shock ***,the cold modulus of rupture and cold crushing strength after thermal shock were increased by 4.1 and 20.3 MPa,***,the addition of micro-Al_(2)O_(3) powders promoted the formation of fine particles of Mg_(2)SiO_(4),MgAl_(2)O_(4) and MgO,as well as a dense protective layer of Mg_(2)SiO_(4) in the material under high-temperature ***,spinel and high-temperature solid solution were formed in the corrosion *** oxidation and corrosion resistances were greatly improved by 41%and 15%,respectively.

关键词： Low-carbon MgO-C refractory Oxidation resistance Corrosion resistance Thermal shock resistance Micro-Al_(2)O_(3)powder

Enhanced oxidation resistance of low-carbon MgO-C refractories with ternary carbides:a review

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Journal of Iron and Steel Research International 2022年第7期29卷 1052-1062页

作者： Chao Yu Bo Dong Yu-feng Chen Bei-yue Ma Jun Ding cheng-ji deng Hong-xi Zhu jing-hui Di The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081HubeiChina School of Metallurgy Northeastern UniversityShenyang 110819LiaoningChina

The demand for low-carbon MgO–C refractories is ever growing to meet the development of advanced steelmaking technologies and efficient energy ***,to improve the oxidation resistance and inhibit the weakness of low-carbon MgO–C refractories,antioxidants are *** application of ternary carbides that focused on improving the oxidation performance of MgO–C refractories has been explored,and the ternary carbides including Al_(4)O_(4)C,Al8B_(4)C_(7),Al_(4)SiC_(4),Ti_(2)AlC,Ti_(3)AlC_(2),and Ti_(3)SiC_(2)have been proved *** crystal structure,physical properties,oxidation behavior,and synthesis of these ternary carbides were summarized,and their oxidation mechanism in assisting antioxidation of MgO–C refractories was *** addition,the potential aspects related to the usage and development of ternary carbides in low-carbon MgO–C refractories were proposed.

关键词： Low-carbon MgO–C refractory Ternary carbide MAX phase Oxidation mechanism Oxidation resistance

Selective sintering of magnesia-calcia materials by utilizing hot spots during induction sintering process

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Journal of Iron and Steel Research International 2024年第8期31卷 1914-1922页

作者： Yun-jie Dong Zhou-fu Wang Hao Liu Yan Ma Xi-tang Wang Nian Yi Zhong-feng Xia Yu-xuan Zhu cheng-ji deng Ling Zhang The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081HubeiChina School of Materials and Metallurgy University of Science and Technology LiaoningAnshan 110325LiaoningChina

Magnesia-calcia refractories are widely used in the production process of clean steel due to their excellent high-tem-perature stability,slag resistance and ability to purify molten ***,there are still problems such as difficult sintering and easy ***-calcia materials with various calcium oxide contents were prepared by using induction sintering,and the sintering property combined with the hydration resistance of the materials was *** experimental results showed that the magnesia-calcia materials prepared under induction field had higher density,microhardness and hydration *** particular,the relative density of induction sintered magnesia-calcia materials with 50 mo1%CaO was greater than 98%,and the average grain size of CaO was 4.56μm,which was much larger than that of traditional sintered *** order to clarify the densification and microstructure evolution mechanism of the magnesia-calcia materials,the changes in temperature and magnetic field throughout the sintering process were analyzed by using finite element *** results showed that the larger heating rate and higher sintering temperature under the induction sintering mode were beneficial to the rapid *** addition,the hot spots generated within the material due to the difference in high-temperature electric conductivity between MgO and CaO were the critical factor to realize selective sintering in MgO-CaO system,which provides a novel pathway to solve the problem of difficult sintering and control the microstructure of high-temperature composite material used in the field of high-purity steel smelting.

关键词： Magnesia-calcia material Induction sintering Hot spot Selective sintering Density Microstructure control Hydration resistance

High‑Entropy Electrode Materials:Synthesis,Properties and Outlook

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Nano-Micro Letters 2025年第1期17卷 472-506页

作者： Dongxiao Li Chang Liu Shusheng Tao jieming Cai Biao Zhong jie Li Wentao deng Hongshuai Hou Guoqiang Zou Xiaobo ji College of Chemistry and Chemical Engineering Central South UniversityChangsha 410083People’s Republic of China School of Chemistry and Chemical Engineering Hunan Institute of EngineeringXiangtan 411104People’s Republic of China

High-entropy materials represent a new category of high-performance materials,first proposed in 2004 and extensively investigated by researchers over the past two *** definition of high-entropy materials has continuously *** the last ten years,the discovery of an increasing number of high-entropy materials has led to significant advancements in their utilization in energy storage,electrocatalysis,and related domains,accompanied by a rise in techniques for fabricating high-entropy electrode ***,the research emphasis has shifted from solely improving the performance of high-entropy materials toward exploring their reaction mechanisms and adopting cleaner preparation ***,the current definition of high-entropy materials remains relatively vague,and the preparation method of high-entropy materials is based on the preparation method of single metal/low-or medium-entropy *** should be noted that not all methods applicable to single metal/low-or medium-entropy materials can be directly applied to high-entropy *** this review,the definition and development of high-entropy materials are briefly ***,the classification of high-entropy electrode materials is presented,followed by a discussion of their applications in energy storage and catalysis from the perspective of synthesis ***,an evaluation of the advantages and disadvantages of various synthesis methods in the production process of different high-entropy materials is provided,along with a proposal for potential future development directions for high-entropy materials.

关键词： High-entropy Energy storage Electrode materials

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Transient chemical-mediated epigenetic modulation confers unrestricted lineage potential on human primed pluripotent stem cells

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Science China Life Sciences 2025年

作者： Shi Chen Yuanyuan He Lejun Lv Bei Liu cheng Li Hongkui deng Jun Xu Department of Cell Biology School of Basic Medical Sciences Peking University Stem Cell Research Center Peking University Health Science Center Peking University Academy of Advanced Interdisciplinary Studies Peking University BeiCell Therapeutics School of Life Sciences Center for Bioinformatics Center for Statistical Science Peking University MOE Engineering Research Center of Regenerative Medicine School of Basic Medical Sciences State Key Laboratory of Natural and Biomimetic Drugs Peking University Health Science Center and the MOE Key Laboratory of Cell Proliferation and Differentiation College of Life Sciences Peking-Tsinghua Center for Life Sciences Peking University

Human primed pluripotent stem cells are capable of generating all the embryonic ***,their extraembryonic trophectoderm potentials are *** remains unclear how to expand their developmental potential to trophectoderm *** we show that transient treatment with a cocktail of small molecule epigenetic modulators imparts trophectoderm lineage potentials to human primed pluripotent stem cells while preserving their embryonic *** chemically treated cells can generate trophectoderm-like cells and downstream trophoblast stem cells,diverging into syncytiotrophoblast and extravillous trophoblast *** and CUT&Tag analyses reveal that these induced cells share transcriptional profiles with in vivo trophectoderm and cytotrophoblast,and exhibit reduced H3K27me3 modification at gene loci specific to trophoblast lineages compared with primed pluripotent *** exploration highlighted the critical roles of epigenetic modulators HDAC2,EZH1/2,and KDM5s in the activation of trophoblast lineage *** findings demonstrate that transient epigenetic resetting activates unrestricted lineage potential in human primed pluripotent stem cells,and offer new mechanistic insights into human trophoblast lineage specification and in vitro models for studying placental development and related disorders.

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基于模糊数学评价法优化对虾真空油炸工艺

南方农业学报 2017年第7期48卷 1266-1273页

作者：朱由珍吉薇吉宏武高静刘书成郝记明邓楚津广东海洋大学食品科技学院广东湛江524088 广东省水产品加工与安全重点实验室广东湛江524088 广东省海洋食品工程技术研究中心广东湛江524088 广东普通高等学校水产品深加工重点实验室广东湛江524088

【目的】优化凡纳滨对虾真空油炸工艺条件,为开发凡纳滨对虾即食品提供技术参考。【方法】以新鲜凡纳滨对虾为原料、模糊数学感官评分(Y)为考察指标,在单因素试验的基础上,选择真空油炸温度(A)、真空油炸时间(B)和真空度(C)为自变量,利... 详细信息

【目的】优化凡纳滨对虾真空油炸工艺条件,为开发凡纳滨对虾即食品提供技术参考。【方法】以新鲜凡纳滨对虾为原料、模糊数学感官评分(Y)为考察指标,在单因素试验的基础上,选择真空油炸温度(A)、真空油炸时间(B)和真空度(C)为自变量,利用响应面法对真空油炸工艺进行优化。【结果】以感官评定为基础对真空油炸对虾的品质进行权重分析,得到权重集K={色泽0.205,形状0.125,油腻感0.270,酥脆度0.400}。建立二次多项回归方程:Y=71.76+5.40A+5.75B+7.34C+3.89AB+5.43AC+6.47BC-4.90A2-3.80B2;真空油炸温度、真空油炸时间、真空度及真空油炸时间与真空度的交互作用对感官评分有极显著影响(P<0.01),真空油炸温度与真空油炸时间、真空油炸温度与真空度的交互作用有显著影响(P<0.05)。通过响应面分析得到对虾真空油炸的最佳工艺条件为:真空油炸温度110℃、真空油炸时间50 min、真空度0.09 MPa,在此条件下的感官评分为90.09±1.27分,与预测值(94.51分)的误差较小,产品色泽均匀有光泽、口感酥脆、油含量适中、形态完整。【结论】响应面法优化的对虾真空油炸工艺具有操作简单、优化条件精确、结果显示直观等优点;建立的回归方程能反映各因素对指标的影响规律,并可进行实际预测。

关键词：凡纳滨对虾真空油炸响应面法模糊数学评价

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对NB-IoT网络建设方案的研究

通信电源技术 2017年第6期34卷 140-143页

作者：洪成洋邓继昌江苏省邮电规划设计院有限责任公司江苏南京210019

为研究基于移动现网资源建设NB-IoT网络方案,介绍了NB-IoT技术和NB-IoT整体网络结构,对比在各应用业务场景下NB-IoT采用1:N和1:1组网方式覆盖能力的差异性,分析了NB-IoT网络建设的四个关键点,对比三个频点选择方案和三个组网方案,提出... 详细信息

为研究基于移动现网资源建设NB-IoT网络方案,介绍了NB-IoT技术和NB-IoT整体网络结构,对比在各应用业务场景下NB-IoT采用1:N和1:1组网方式覆盖能力的差异性,分析了NB-IoT网络建设的四个关键点,对比三个频点选择方案和三个组网方案,提出了实际部署NB-IoT网络时的频谱策略、组网方案,并给出了低成本部署的策略以及现网改造建议,对后续NB-10T无线网规划和工程实施具有重要指导意义。

关键词：无线通信 NB-IoT FDD-LTE 组网低成本

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A versatile synthetic strategy towards rare earth based metal-organic frameworks

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Science China Chemistry 2025年

作者： Quan Shi Yun-Hao Xu Ming-Hui Chen Peng Zhao Wen-Bo deng ji Xiong Kai Guo Ya-Qing Feng Bao Zhang School of Chemical Engineering and Technology Tianjin University Tianjin Collaborative Innovation Center of Chemical Science and Engineering Guangdong Laboratory Chemistry & Fine Chemical Industry jieyang Center

Rare earth metal-organic frameworks (RE-MOFs) have drawn wide attention owing to diverse network structures and various application ***,due to the unpredictable formation of the nodes,it is still challenging to design novel RE-MOFs.A novel versatile strategy was developed employing a RE-acetate complex (RE2(CH3COO)6·4H2O) as a precursor to construct RE-MOFs.2D RE-MOFs (RE-DBP) and 3D RE-MOFs (RE-TCPP) could be obtained by using dicarboxylic porphyrin ligands H2DBP and tetracarboxylic porphyrin ligands H2TCPP,*** RE-MOFs were further synthesized to verify the universality of the *** crystalline RE-MOFs could also be prepared at room temperature via the developed strategy,which could significantly promote large-scale preparation and practical application of *** proof of the concept,the performance of porphyrin-based RE-MOFs was investigated in the photocatalytic cycloaddition of CO2with *** the RE-DBP(Co) MOFs,Tb-DBP(Co) exhibited the best photocatalytic performance,which was also greater than that of the corresponding 3D MOF Tb-TCPP(Co) due to the optimal 2D structure and thus the accelerated photogenerated charge separation and transfer *** work not only provides a novel versatile strategy to design and develop RE-MOFs,but also proposes a promising approach for the potential bulk production of RE-MOFs at room temperature.

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