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Synthesis and characterization of Y and Dy co-doped ceria solid electrolytes for IT-SOFCs:a microwave sintering

Rare Metals 2021年第11期40卷 3329-3336页

作者： ch.madhusudan Venkataramana Kasarapu Madhuri chittimadula Y.Suresh Reddy C.Vishnuvardhan Reddy Department of Physics Osmania UniversityHyderabadTelangana 500007India

In this communication,the electrical conductivities and thermal expansion studies of microwave sintered co-doped ceria Ce_(0.8)Y_(0.2-x)Dy_(x)O_(2-δ)(x=0,0.05,0.10,0.15 and 0.20) solid electrolyte materials for intermediate temperature solid oxide fuel cells(IT-SOFCs)synthesized by sol-gel auto-combustion method were *** sintering at 1300℃ for 30 min was used for making dense powder *** relative densities of all the samples are noticed above 95%.Raman spectrum was characterized by the presence of a very strong band near 460 cm^(-1),which along with X-ray diffraction(XRD) analysis ascertain the sample formation with a single-phase cubic fluorite *** lattice parameter values were calculated from XRD *** images show nearly uniform grains with distinct grain *** thermal expansion coefficients(TECs) are found to vary linearly with temperature and were measured in the range from 14.15 to 13.20×10^(-6)℃^(-1).The investigation on total ionic conductivity(TIC) was executed with variation in dopant concentration and relative oxygen *** impedance analysis reveals that the sample Ce_(0.80)Y_(0.10)Dy_(0.10)O_(2-δ) displays the highest TIC,i.e.,7.5×10^(-3) S·cm^(-1) at 500℃ and minimum activation energy 0.90 eV compared to *** the highest TIC and minimum activation energy,the Ce_(0.80)Y_(0.10)Dy_(0.10)O_(2-δ)might be the possible material as the solid electrolyte in intermediate temperature SOFCs.

关键词： Microwave sintering Ionic conductivity Co-doped ceria Solid electrolyte Intermediate temperature solid oxide fuel cells

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