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Treatment of Materials Contaminated with Polychlorinated Biphenyls(Pcbs):Comparison of Traditional Method and Supercritical Fluid Extraction

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American Journal of Analytical Chemistry 2012年第12期3卷 891-898页

作者： Dannielle Jannaine Silva Felipe V.Pietri José Ermirio F.Moraes Reinaldo Camino Bazito camila gambini pereira Department of Chemical Engineering Federal University of Rio Grande do NorteNatalBrazil Department of Chemical Engineering Federal University of Sao PauloSao PauloBrazil Department of Chemistry University of Sao PauloSao PauloBrazil

The objective of this study was to develop an experimental methodology for the extraction of polychlorinated biphenyls (PCBs) from contaminated soil and wood material using the Soxhlet extraction method and supercritical fluid technology. The sample PCB contents were quantified using Gas Chromatography-Mass Spectrometry (GC/MS). Conventional extractions of PCBs from soil samples showed higher extraction yields for samples with the highest initial PCB levels and longest extraction times. Specific PCBs yielded 74.0% - 78.3% removal using ethanol as the solvent. 91.0% - 94.3% removal of the total PCB content was achieved using hexane as the solvent. Supercritical fluid extraction of soil samples resulted in 50.0% - 70.5% removal for specific PCBs and 57.3% removal of the total PCB content. For wood, the use of Soxhlet extraction resulted in 87.0% - 94.0% removal for specific PCBs and 95.0% - 96.3% removal of the total PCB content. Supercritical fluid extraction of wood samples resulted in 91.1% - 95.0% removal of specific PCBs and 95.1 % of the total PCB content.

关键词： Polychlorinated Biphenyls Extraction Soil Wood

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Effect of Blends Gasoline with Oxygenated Additives in the Performance of Internal Combustion Engine

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Journal of Power and Energy Engineering 2021年第7期9卷 1-9页

作者： Suzara Rayanne de Castro Sena André Luis Oliveira de Almeida Leonara Luizza da Costa Leite Jean Gustavo de Melo Araujo Eduardo Lins de Barros Neto camila gambini pereira Centre of Education and Research in Oil and Gas Federal University of Rio Grande do Norte (UFRN) Natal Brazil

The objective of this study was to evaluate the effect of blends of different oxygenated additives on gasoline in SI engine Otto cycle. The formulations analyzed were: pure gasoline (type A), common gasoline (type C), gasoline type A + 15% (v/v) oxygenated additives (ethanol, ethyl octanoate, ethyl oleate). The experiments were performed using engine Branco 4-stroke and 2-cylinder, electric dynamometer, exhaust system, control unit composed of Multi-K unit, variable selector and load cell, stroboscope tachometer, fuel supply system and stopwatch. The rotation was conserved at 4400 rpm and wheel power varied from 3 kW to 12 kW, with intervals of 3 kW to obtain hourly consumption curves and brake specific fuel consumption. Even esters and ethanol having lower heat of combustion, hourly consumption was similar to pure gasoline (type A). In relation to the brake specific fuel consumption, increasing the wheel power had a better conversion of the mass of fuel burned into energy. Thus, this study showed that the mixture of gasoline and esters (ethyl octanoate and ethyl oleate) presented good efficiency in terms of consumption. This research contributes to the needs and to the current studies in which industries started to add renewable products to petroleum-derived fuels;in order to obtain more sustainable fuels at lower costs.

关键词： Gasoline Oxygenated Additives Consumption

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