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Microstructural evolution and superelastic properties of ultrafine-graine d NiTi-base d shape memory alloy via sintering of amorphous ribbon precursor

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Journal of Materials Science & Technology 2023年第7期138卷 80-92页

作者： W.S.Cai H.z.Lu H.z.Li z.Liu H.b.Ke W.H.Wang C.Yang National Engineering Research Center of Near-net-shape Forming for Metallic Materials Guangdong Provincial Key Laboratory for Processing and Forming of Advanced Metallic MaterialsSouth China University of TechnologyGuangzhou 510640China Songshan Lake Materials Laboratory Dongguan 523808China Institute of Physics Chinese Academy of SciencesBeijing 100190China

NiTi-based shape memory alloys(SMAs)are considered as cutting-edge intelligent functional ***,it remains a great challenge to obtain ultrafine-grained(UFGed)bulk materials with mm-scale size as well as outstanding superelastic ***,UFGed bulk Ti_(35)zr_(15)Ni_(35)Cu_(15)NiTi-based SMA is successfully prepared via spark plasma sintering of amorphous ribbon precursor at different sintering temperatures,and microstructural evolution and superelastic properties are symmetrically *** is found that its grain size ranges from UFG to micro-grain with increased sintering temperature regard-less of the predominant b2 matrix in all bulk ***,the orientation relationships between b2 matrix and nano-scale fcc(Ti,zr)_(2)Ni precipitate evolve from coherent to ***,the UFGed samples exhibit perfect superelasticity with the high recoverable strain of∼5.8%,the stable recov-ery rate above 99%,and the great critical stress inducing martensitic transformation higher than 1 GPa,far superior to the corresponding ones of suction-cast micro-grained TizrNiCu ***,the perfect superelasticity is attributed to the good resistance to dislocation slip or grain boundary slip by residual nano-scale amorphous phase or secondary phase of coherent and semi-coherent fcc(Ti,zr)_(2)Ni *** addition,the gentle superelastic plateau is associated to the favorable transfer stress and the strong ability to accommodate dislocation movement,which is generated by the coherent interface between nano-scale fcc(Ti,zr)_(2)Ni and UFGed b2 *** results suggest that spark plasma sintering of amorphous alloy precursor is a feasible route to obtaining excellent superelasticity in NiTi-based SMAs.

关键词： Shape memory alloy Amorphous alloy Microstructure Superelasticity

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Mechanism transition of cross slip with stress and temperature in face-centered cubic metals

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Journal of Materials Science & Technology 2020年第22期54卷 159-171页

作者： K.Q.Li z.J.zhang J.X.Yan J.b.Yang z.F.zhang Laboratory of Fatigue and Fracture for Materials Institute of Metal ResearchChinese Academy of SciencesShenyang110016China School of Materials Science and Engineering University of Science and Technology of ChinaShenyang 110016China

A/2 screw dislocation is commonly dissociated into two /6 Shockley partial dislocations on{111} planes in face-centered cubic *** the two partials are not purely screw,different mechanisms of cross-slip could take place,depending on the stacking fault energy,applied stress and tempe *** is crucial to classify the mechanisms of cross-slip because each mechanism possesses its own reaction path with a special activation *** this work,molecular dynamics simulations have been performed systematically to explore the cross-slip mechanism under different stresses and temperatures in three different metals Ag,Cu and Ni that have different stacking fault energies of 17.8,44.4 and 126.8 mJ/m^2,re *** Ag and Cu with low stacking fault energy,it is observed that the cross-slip mechanism of screw dislocations changes from the Fleischer obtuse angle(FLOA),to the Friedel-Escaig(FE),and then to the FL acute angle(FLAA) at low temperatures,with increasing the applied ***,when the temperature increases,the FE mechanism gradually becomes dominant,while the FLAA only occurs at the high stress *** particular,the FLOA has not been observed in Ni because of its high stacking fault energy.

关键词： Cross-slip Molecular dynamics simulation Face-centered cubic metals Stacking fault energy

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Effect of post weld artificial aging and water cooling on microstructure and mechanical properties of friction stir welded 2198-T8 Al-Li joints

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Journal of Materials Science & Technology 2022年第28期123卷 92-112页

作者： Y.Tao z.zhang P.Xue D.R.Ni b.L.Xiao z.Y.Ma Institute of Metal Research Chinese Academy of SciencesShenyang 110016China

Friction stir welding(FSW)under both air cooling and water cooling conditions with welding parameters of 800-1200 rpm rotation rates and 50-200 mm/min welding speeds was carried out on 2198-T8 Al-Li alloys,and post weld artificial aging was performed on the air cooled *** welding defects other than lazy S were observed in the nugget zone(Nz)for all *** air cooling condition,the lowest hardness zone(LHz)occurred in the heat affected zone(HAz).FSW resulted in gradual dissolution of original T_(1),θ′andδ′/β′from the base material(bM)to the thermo-mechanically affected zone(TMAz),and complete dissolution of all precipitates in the Nz withδ′/β′and Guinier-Preston zones precipitating during *** air cooled joints exhibited no noticeable changes in intrinsic tensile strength with a joint strength reaching 81.3%of the bM,but varied elongation with welding parameters,which was closely related to failure in the Nz and fracture along lazy *** weld artificial aging led to the largest hardness recovery in the TMAz but smaller hardness recovery in the initial LHz and the *** aging kinetics across the joint was determined by volume fraction of both original precipitate dissolu-tion during welding and coarse particles formed during aging,and by dislocation density inherited from *** weld artificial aging greatly enhanced the joint strength with the ultimate tensile strength reaching 87.3%of the *** compared to air cooling condition,water cooling hardly affected the Nz hardness and did not improve the joint strength,and the reason was discussed in light of precipitates,hardness changes and fracture behavior.

关键词： Friction stir welding Aluminum-lithium alloys Microstructure Mechanical properties

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Achieving Large-area bulk Ultrafine Grained Cu via Submerged Multiple-pass Friction Stir Processing

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Journal of Materials Science & Technology 2013年第12期29卷 1111-1115页

作者： P. Xue b.L. Xiao z.Y. Ma Shenyang National Laboratory for Materials Science Institute of Metal Research Chinese Academy of Sciences 72 Wenhua Road Shenyang 110016 China

Large-area bulk ultrafine grained （UFG） pure Cu was successfully prepared by multiple-pass overlapping friction stir processing （FSP） under additional rapid cooling. Overlapping FSP did not exert a significant effect on the microstructure and mechanical properties of the FSP UFG Cu. Similar average grain size was achieved in the transitional zone （Tz） of the multiple-pass FSP sample compared to that in the nugget zone of the single-pass FSP sample, and the Tz exhibited a strong {111}（112） type A fiber shear texture, Very weak softening occurred in the Tz of the multiple-pass FSP UFG Cu, resulting in a relatively uniform hardness distribution throughout the whole processed zone. A high yield strength of - 310 MPa and a uniform elongation of - 13% were achieved in the bulk FSP UFG Cu. This study provides an effective strategy to prepare large-area bulk IUFG materials.

关键词： Friction stir processing Multiple-pass Ultrafine grains Microstructure Mechanical properties

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Strategies for improving ductility of ordered intermetallics

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Progress in Natural Science:Materials International 2016年第1期26卷 1-12页

作者： z.b.Jiao J.H.Luan C.T.Liu Center for Advanced Structural Materials Department of Mechanical and Biomedical Engineering College of Science and Engineering City University of Hong Kong

Ordered intermetallics possess attractive high-temperature properties; however, low ductility and brittle fracture limit their use as engineering materials in many cases. This paper provides a comprehensive review on the recent progress in the development of ductile ordered intermetallics and summarizes the strategies used to improve the tensile ductility of ordered intermetallics, including control of ordered crystal structures,engineering grain-boundary structure and chemistry, eliminating environmental embrittlement, microstructure optimization, control of phase stability, and promoting transformation-/twining-induced plasticity. The basic ideas and related mechanisms underlying these ductilizing strategies are discussed. In addition, a brief mention of the current use of intermetallic alloys for structural and corrosion applications is made.

关键词： Ordered intermetallics Ductility Ductilizing strategy Microstructure Alloy design

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Diffusion behavior of Cr in gradient nanolaminated surface layer on an interstitial-free steel

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Journal of Materials Science & Technology 2019年第3期35卷 460-464页

作者： S.L.Xie z.b.Wang K.Lu Shenyang National Laboratory for Materials Science Institute of Metal Research Chinese Academy of Sciences School of Materials Science and Engineering University of Science and Technology of China

Nanolaminated structures composed of low-angle grain boundaries(LAGbs) possess high thermal stability. In this paper, a gradient nanolaminated(GNL) surface layer with smooth finish was fabricated on an interstitial-free steel by means of surface mechanical rolling treatment. Microstructural observations demonstrated that the average lamellar thickness is about 80 nm in the topmost surface layer and increases with increasing depth. High thermal stability was confirmed in the GNL surface layer after annealing at 500℃. Diffusion measurements showed that effective diffusivity of Cr in GNL layer is 4–6 orders of magnitude higher than lattice diffusivity within the temperature range from 400 to 500℃. This might be attributed to numerous LAGbs or dislocation structures with a higher energy state in the GNL surface layer. This work demonstrates the possibility to advanced chromizing(or other surface alloying)processes of steels with formation of GNL surface layer, so that a thicker alloyed surface layer with a stable nanostructure is achieved.

关键词： Gradient nanolaminated structure Interstitial-free steel Diffusion Low-angle grain boundary Surface mechanical rolling treatment

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航道骨架护岸结构的稳定性影响规律及其优化

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水运工程 2024年第5期 200-206,214页

作者：梅蕊王法鑫张薇李昂孙阳河海大学港口海岸与近海工程学院江苏南京210024 河海大学淮安研究院江苏淮安223005

为探究不同结构形式航道骨架护岸结构的稳定性影响规律,选择出最佳护岸结构形式,并对该形式进行结构优化,结合沙河漯河—平顶山航运工程的实际情况,利用PLAXIS 3D分别建立了几种护坡的三维结构模型。结果表明:在人字形、菱形、拱形骨架... 详细信息

为探究不同结构形式航道骨架护岸结构的稳定性影响规律,选择出最佳护岸结构形式,并对该形式进行结构优化,结合沙河漯河—平顶山航运工程的实际情况,利用PLAXIS 3D分别建立了几种护坡的三维结构模型。结果表明:在人字形、菱形、拱形骨架3种形式中,使用拱形骨架时,岸坡的滑动破坏面范围最小,岸坡的安全系数最大;在设计拱形骨架护岸结构时,应首先考虑不同拱径对岸坡土体位移的影响,在对岸坡土体沉降控制较严格的工程上,可进一步考虑不同拱宽的设计取值对其不同影响;本工程建议拱形骨架护岸结构的设计参数由原设计方案(拱径2.5 m、拱宽0.05 m、埋深0.300 m)优化为正交方案(拱径4.5 m、拱宽0.05 m、埋深0.450 m),在减小岸坡土体位移的同时仅增加不到55 m3的混凝土用量。

关键词：拱形岸坡骨架护岸正交优化稳定性分析岸坡安全系数

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Distinct dendritic α phase emerging on the surface of primary α phase in a compressed near-α titanium alloy

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Journal of Materials Science & Technology 2018年第4期34卷 666-669页

作者： z.Liu z.b.zhao J.R.Liu Q.J.Wang R.Yang Institute of Metal Research Chinese Academy of Sciences School of Materials Science and Engineering University of Science and Technology of China

The characteristic of the surface morphology of primary α phase was studied in a deformed near-α tita- nium alloy. Dendritic α phase emerged on the surfaces of primary α phase when the alloy was air-cooled in α ＋β phase field after deformation. The dendritic α grain has the same orientation with its original primary α grain. The formation of the dendritic α phase could be explained by interface instability in epi- taxial growth process of the primary α phase. The dislocations induced by deformation could facilitate the formation of dendritic α phase leading to the dendritic α phase and more obvious with the increase of strain. The growth of dendritic α phase was finally limited by the nucleation of second α phase with cooling.

关键词： Epitaxial growth Dendritic α phase Microstructure Interface instability Hot deformation

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Production of Carbon Nanotubes over Pre-reduced LaCoO_3 Using Fluidized-bed Reactor

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Chinese Chemical Letters 2000年第11期11卷 1031-1034页

作者： Liu b.C. Liang Q. Tang S.H. Gao L.z. zhang b.L. Qu M.z. Yu z.L. Chengdu Inst. of Organic Chemistry Academia Sinica Chengdu 610041 China Nanjing Univ. of Chemical Technology Nanjing 210009 China

Carbon nanotubes were synthesized on a large scale by the catalytic decomposition of hydrocarbons over pre-reduced LaCoO3 using a fluidized-bed reactor. Reaction parameters such as reduction temperature, reduction tim... 详细信息

关键词： CNTs Production of Carbon Nanotubes over Pre-reduced LaCoO3 Using Fluidized-bed Reactor over

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Analysis of local crystallographic orientation in an annealed Ti60 billet

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Journal of Materials Science & Technology 2019年第4期35卷 591-595页

作者： z.b.zhao z.Liu Q.J.Wang J.R.Liu R.Yang Institute of Metal Research Chinese Academy of Sciences School of Materials Science and Engineering University of Science and Technology of China

A heterogeneous microstructure in terms of local orientation distribution is often found in near-α titanium alloys. The presence of large regions with similar crystallographic orientation, called ‘macrozones',could drastically decrease the fatigue performance of titanium alloys. The present work reports on the crystallographic orientation of a near-α titanium alloy, Ti60, billet after annealing in an α+β phase *** texture was found to be weak, and no obvious macrozone was found in our measured zone where the variant selection is suppressed. Meanwhile, in-depth electron backscattered diffraction(EbSD) analysis was applied to evaluate the final microstructure, and the mechanisms by which they formed were analyzed.

关键词： Titanium alloys Microstructure Texture Heat treatment EbSD

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