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Solar-assisted photocatalytic water splitting using defective UiO-66 solids from modulated synthesis

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nano research 2024年第5期17卷 4134-4150页

作者： Celia m.rueda-navarro maría Cabrero-Antonino Paula Escamilla Valentín Díez-Cabanes Dong Fan Pedro Atienzar Belén Ferrer Ignacio Vayá Guillaume maurin Herme G.Baldoví Sergio navalón Departamento de Química Universitat Politècnica de ValènciaCamino de Vera s/nValencia 46022Spain Instituto de Ciencia molecular(ICmOL) Universitat de ValènciaPaterna 46980Spain ICGm Univ.MontpellierCNRSENSCMMontpellier34095France Instituto de Tecnología Química(UPV-CSIC) Universitat Politècnica de ValènciaAvenida de los Naranjos s/nValencia 46022Spain

metal-organic frameworks(mOFs)are attracting increasing interests as photocatalysts for solar-driven hydrogen production from *** paper reports on a comparative study of using either acetic acid(AA)or trifluoroacetic acid(TFA)as the representative UiO-66 organic modulators for synthesizing visible light responsive UiO-66(Zr)-X(X:nH_(2) or nO_(2))photocatalysts for water *** results show that photocatalytic hydrogen generation from a water/methanol mixture can be improved by varying the nature and amount of the modulator employed to prepare the different UiO-66(Zr)-X(X:nH_(2) or nO_(2))solid ***-66(Zr)-nH_(2) was the most active photocatalyst,followed by UiO-66(Zr)-nO_(2),both prepared with 12 equivalents of AA with respect to the organic *** UiO-66(Zr)-nH_(2) solid was more active than the parent mOF in photocatalytic overall water splitting(OWS)(H_(2) and O_(2) production of 450 and 160μmol·g^(-1),respectively,in 5 h;apparent quantum yield(AQY)at 400 nm of 0.06%)in the absence of methanol and compares favourably with analogous *** on the photocatalytic activity of the most active solids of both series was obtained by means of a series of techniques,including ultraviolet-visible(UV-vis)diffuse reflectance,X-ray photoelectron spectroscopy(XPS),laser flash photolysis(LFP),electron spin resonance(ESr),photoluminescence and photoelectrochemical measurements together with density functional theory(DFT)*** results showed that organic acid modulators can be used to enhance the photocatalytic activity of missing linker UiO-66 defective materials in solar-powered water splitting.

关键词： heterogeneous photocatalysis metal-organic frameworks(mOFs) UiO-66 materials carboxylic acid modulators water splitting solar light

DFT investigation of half-metallic ferromagnetic rare earth based spinels mgHo_(2)Z_(4)(Z=S,Se)

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Journal of rare Earths 2024年第1期42卷 121-128,I0005页

作者： maiza Zanib mumtaz manzoor n.A.noor m.Waqas Iqbal mazia Asghar H.H.Hegazy A.Laref Department of Physics Riphah International UniversityLahore CampusPakistan research Centre for Advanced materials Science King Khalid UniversityP.O.Box 9004AbhaSaudi Arabia Department of Physics Faculty of ScienceKing Khalid UniversityP.O.Box 9004AbhaSaudi Arabia Department of Physics and Astron.my College of ScienceKing Saud UniversityRiyadh11451Saudi Arabia

Half-metallic ferromagnetism,mechanical as well as thermoelectric properties for rare earth-based spinels mgHo_(2)Z_(4)(Z=S,Se)were investigated using density functional theory(DFT).Structural optimization was done with Perdew-Burke-Ehrenzorf(PBE)sol-generalized gradient approximation(GGA)to calculate the lattice constant of both spinels comparable to experimental *** addition,Born stability criteria and negative formation energy show that our studied spinels are also structurally and dyn.mically stable in the cubic *** ferromagnetic(Fm)state stability,we also calculated the energy differences among Fm,antiferromagnetic(AFm),and non.magnetic(nm)***,Curie temperatures of ferromagnetic phases were also *** used Trans-Blaha improved BeckeJohnson(TB-mBJ)potential functional for electronics as well as magnetic characteristics,which lead to the consistent explanation of half-metallic ferromagnetism,representing the whole band-occupancy in.material with exact detail of density of states(DOS).The stable Fm state was examined in spinels due to the exchange splitting of Ho cation consisting of p-d hybridizations compatible with the result achieved for electronics band structure and ***,spin.magnetic moment was explained in terms of anion,cation,and sharing charge on studied *** addition,the calculated thermoelectric properties clearly show that operation range of these systems may be utilized by future experimental works for identifying the potential applications of these systems.

关键词： Ho-based spinels DFT simulations mechanical parameters Electronic properties Hm ferromagnetism Figure of merit

neurocircuit regeneration by extracellular matrix reprogramming

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neural regeneration research 2025年第8期20卷 2300-2301页

作者： Shengzhang Su Ian n.Levasseur Kimberly m.Alonge Department of medicinal Chemistry University of WashingtonSeattleWAUSA Department of Chemistry University of WashingtonSeattleWAUSA Department of medicine University of Washington Medicine Diabetes InstituteSeattleWAUSA

The brain's extracellular matrix(ECm),which is comprised of protein and glycosaminoglycan(GAG)scaffolds,constitutes 20%-40%of the human brain and is considered one of the largest influencers on brain cell functioning(Soles et al.,2023).Synthesized by neural and glial cells,the brain's ECm regulates a myriad of homeostatic cellular processes,including neuronal plasticity and firing(miyata et al.,2012),cation buffering(moraws ki et al.,2015),and glia-neuron interactions(Anderson et al.,2016).Considering the diversity of functions,dyn.mic remodeling of the brain's ECm indicates that this understudied medium is an active participant in both normal physiology and neurological diseases.

关键词： al. matrix programming

Beyond dentistry:could prevention and screening for neurodegenerative diseases start in the dental office?

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neural regeneration research 2024年第1期19卷 156-157页

作者： Francesca r.Buccellato Daniela Galimberti Gianluca m.Tartaglia Department of Biomedical Surgical and Dental SciencesUniversity of MilanMilanItalyFondazione IRCCS Ca’GrandaOspedale Maggiore PoliclinicoMilanItaly

The differential diagnosis of neurodegenerative diseases is complex and relies on clinical assessment,biomarker levels in cerebrospinal fluid,neuroimaging and neuropsychological *** efforts of the scientific community are focused on two aspects:a)the discovery of min.mally invasive biomarkers;b)the discovery of early biomarkers that can predict the progression to clinical disease in the presymptomatic stage of a *** the impact of the n.mber of patients affected by chronic neurodegenerative diseases on public health expenditures,early diagnosis seems to be a primary need of our society.

关键词： diagnosis diseases prevention

measurement of yields and angular distributions ofγ-quanta from the interaction of 14.1 meV neutrons with oxygen,phosphorus,and sulfur

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Chinese Physics C 2024年第3期48卷 79-92页

作者： D.n.Grozdanov n.A.Fedorov S.B.Dabylova Yu.n.Kopatch I.n.ruskov V.r.Skoy T.Yu.Tretyakova C.Hramco P.I.Kharlamov G.V.Pampushik P.G.Filonchik A.V.Andreev Joint Institute for nuclear research(JInr) DubnaRussia Institute for nuclear research and nuclear Energy Bulgarian Academy of SciencesSofiaBulgaria Faculty of Physics Lomonosov Moscow State UniversityMoscowRussia L.n.Gumilyov Eurasian national University AstanaKazakhstan Skobeltsyn Institute of nuclear Physics Moscow State UniversityMoscowRussia Institute of Chemistry of moldova ChisinauRepublic of Moldova moscow Institute of Physics and Technology MoscowRussia

A study of the inelastic scattering of neutrons with an energy of 14.1 meV on the nuclei of oxygen,phosphorus,and sulfur was performed at the TAnGrA facility at JInr(Dubna).The experiment aimed to refine existing data and obtain new data on the yields and angular distributions ofγ-quanta emitted by the studied nuclei due to neutron-induced nuclear reactions using the tagged neutron *** types of detector systems were used to registerγ-***γ-ray yields were measured using a high-purity germanium(HPGe)*** angular distributions ofγ-rays were obtained using a system of 18 scintillation detectors based on bismuth germanite Bi_(4)Ge_(3)O_(12)(BGO)located around the *** performed experiments measured the yields of two transitions for the reaction of tagged neutrons with 16O,nine transitions for the reaction with ^(31)P,and nine transitions for the reaction with ^(32)S for the first *** angular anisotropy of theγ-radiation accompanying the inelastic scattering of neutrons with an energy of 14.1 meV on ^(31)P nuclei was also measured for the first time.

关键词： tagged neutron.method yields of gamma-quanta high-resolution gamma-spectrometry neutron-nuclear reactions neutron scattering

Compression properties of cost-efficient porous expanded clay reinforced AA7075 syntactic foams fabricated by industrial-oriented die casting technology

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China Foundry 2024年第1期21卷 60-70页

作者： İsmail Cem Akgün Çağın Bolat Ali Gökşenli Faculty of mechanical Engineering Istanbul Technical University34437İstanbulTurkey Faculty of Engineering Samsun University55420SamsunTurkey

In today’s manufacturing industries,hard competition between rival firms makes it compulsory for researchers to design lighter and cheaper machine components due to the megatrends of cost-effectiveness and *** this point,alumin.m syntactic foams(ASFs)are new-generation engineering composites and come into the upfront as a *** to their features like low density,sufficient elongation,and perfect energy absorption ability,these advanced foams have been considerably seductive for many industrial sectors *** this study,an industrial-oriented automatic die casting technology was used for the first time to manufacture the combination of AA7075/porous expanded clay(PEC).micro evaluations(optical and FESEm)reveal that there is a homogenous particle distribution in the foam samples,and inspections are compatible with the other ASF ***,T6 aging heat treatment was operated on one half of the produced foams to explore the probable impact of aging on the compressive *** results show that PEC particles can be an alternative to expensive hollow spheres used in the previous ***,a favorable relationship is ascertained between the aging treatment and mechanical properties such as compression strength and plateau strength.

关键词： die casting porous materials metal matrix sytanctic foams expanded clay compressive deformation

Large magnetocaloric effect and magnetic properties of EurhO_(3)

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Journal of rare Earths 2024年第9期42卷 1724-1729,I0004页

作者： m.Lassri m.Sajieddine A.Elouafi A.El Hachmi S.El Ouahbi r.moubah Laboratory of Energy and materials Engineering(LGEm) University of Sultan Moulay SlimaneFaculty of Science and Technology(FST)BP 52323000Béni-MellalMorocco Institute of Applied Physics(IAP)-School of Industrial management(EmInES) Mohammed VI Polytechnic UniversityHay Moulay RachidLot 6603150Ben GuerirMorocco national School of Applied Sciences(EnSA) University of Sultan Moulay SlimaneBP 7725000KhouribgaMorocco Laboratory of mechanics Production and Industrial Engineering(LMPGI)Higher School of Technology of Casablanca(ESTC)University of Hassan II CasablancaCasablancaMorocco Laboratory of radiation on.matter and Instrumentation(LrmI) Faculty of Science and Technology(FST)SettatHassan I UniversitySettatMorocco Laboatory of Physics of Advanced materials and Thermic(LPmAT) Faculty of Science Ain Chock(FSAC)University of Hassan II CasablancaCasablancaMorocco

We report on the structural,magnetic,and magnetocaloric properties of EurhO_(3) *** oxidation states of Eu and rh ions were studied using X-ray photoelectron spectroscopy(XPS).It is found that the Eu ions are mainly in the divalent oxidation state while the rh ions have+4 ***_(3) powders are found to be antiferromagnetic with a second order magnetic transition at neel temperature(T_(n)=2.9 K).Analysis of the magnetic susceptibility versus temperature data in terms of the Curie=Weiss law:(χ=C/(T-θ_(W))) for T>T_(n),yields θ_(W)=-3.1 K and effective magne tic moment μ_(ff)^(exp),which is close to the theoretical value μ_(eff)^(theo).The magnetic entropy change(-Δ_(Sm)),was determined by em ploying the thermodyn.m ic maxwell's *** μ_0H=5 T and near T_(n),ΔS_(m)^(max) and relative cooling power(rCP) exhibit large values of 33.7 J/(kg·K) and 238 J/kg,*** large magnitude of-Δ_(Sm) and rCP show that the EurhO_(3) compound could be a potential candidate to be used in cryogenic magnetic refrigeration.

关键词： X-ray photoelectron spectroscopy Cryogenic magnetic refrigeration magnetic properties magnetocaloric effect rare earths

Extended Deep Learning Algorithm for Improved Brain Tumor Diagnosis System

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Intelligent Automation & Soft Computing 2024年第1期39卷 33-55页

作者： m.Adimoolam K.maithili n.m.Balamurugan r.rajkumar S.Leelavathy raju Kannadasan.mohd Anul Haq Ilyas Khan ElSayed m.Tag El Din Arfat Ahmad Khan Department of Computer Engineering Government Polytechnic CollegeSevvapetTiruvallurTamil Nadu602025India Department of Computer Science and Engineering KG Reddy College of Engineering and TechnologyHyderabadTelangana500075India Department of Computer Science and Engineering Sri Venkateswara College of EngineeringSriperumbudurChennai602117India Department of Computer Science and Engineering Annamalai UniversityChidambaramTamil Nadu608002India Department of Computer Science and Engineering Aarupadai Veedu Institute of TechnologyVinayaka Mission Research FoundationPaiyanurTamil Nadu603104India Department of Electrical and Electronics Engineering Sri Venkateswara College of EngineeringSriperumbudur602117India Department of Computer Science College of Computer and Information SciencesMajmaah UniversityAl-Majmaah11952Saudi Arabia Department of mathematics College of Science Al-ZulfiMajmaah UniversityAl-Majmaah11952Saudi Arabia Electrical Engineering Department Faculty of Engineering&TechnologyFuture University in EgyptNew Cairo11835Egypt Department of Computer Science College of ComputingKhon Kaen UniversityKhon Kaen40002Thailand

At present,the prediction of brain tumors is performed using machine Learning(mL)and Deep Learning(DL)*** various mL and DL algorithms are adapted to predict brain tumors to some range,some concerns still need enhancement,particularly accuracy,sensitivity,false positive and false negative,to improve the brain tumor prediction system ***,this work proposed an Extended Deep Learning Algorithm(EDLA)to measure performance parameters such as accuracy,sensitivity,and false positive and false negative *** addition,these iterated measures were analyzed by comparing the EDLA method with the Convolutional neural network(Cnn)way further using the SPSS tool,and respective graphical illustrations were *** results were that the mean performance measures for the proposed EDLA algorithm were calculated,and those measured were accuracy(97.665%),sensitivity(97.939%),false positive(3.012%),and false negative(3.182%)for ten *** in the case of the Cnn,the algorithm means accuracy gained was 94.287%,mean sensitivity 95.612%,mean false positive 5.328%,and mean false negative 4.756%.These results show that the proposed EDLA method has outperformed existing algorithms,including Cnn,and ensures symmetrically improved *** EDLA algorithm introduces novelty concerning its performance and particular activation *** proposed method will be utilized effectively in brain tumor detection in a precise and accurate *** algorithm would apply to brain tumor diagnosis and be involved in various medical diagnoses *** the quantity of dataset records is enormous,then themethod’s computation power has to be updated.

关键词： Brain tumor extended deep learning algorithm convolution neural network tumor detection deep learning

Prompt neutron emission in ^(250)no spontaneous fission associated with ground and isomeric state decays

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Chinese Physics C 2024年第6期48卷 112-117页

作者： r.S.mukhin A.V.Isaev A.V.Andreev m.L.Chelnokov V.I.Chepigin H.m.Devaraja I.n.Izosimov A.A.Kuznetsova O.n.malyshev A.G.Popeko Yu.A.Popov A.rahmatinejad B.Sailaubekov T.m.Shneidman E.A.Sokol A.I.Svirikhin.m.S.Tezekbayeva m.A.Bychkov A.V.Yeremin O.Dorvaux B.Gall K.Kessaci K.Hauschild A.Lopez-martens Joint Institute for nuclear research Dubna141980Russia Dubna State University Dubna141982Russia Institute of nuclear Physics Almaty050032Kazakhstan L.n.Gumilyov Eurasian national University Astana010008Kazakhstan Kazan Federal University Kazan420008Russia Universitéde Strasbourg CNRSStrasbourg67000France IJCLab IN2P3-CNRSUniversitéParis-SaclayOrsay91400France

The complete-fusion reaction^(204)Pb(^(48)Ca,2n)^(250)no was used to study two activities of^(250)no with distinct half-lives.A total of 1357 events were observed in the SFinx neutron detection *** average n.mber of neutrons emitted per spontaneous fission of^(250)no was determined to be(4.1±0.1).The unusually symmetrical shape of the prompt neutron.multiplicity distribution was restored and presented for the first *** tests were performed to compare the prompt neutron.multiplicity distributions associated with the ground state and K-isomer state decays.

关键词： spontaneous fission prompt neutrons actinide