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Progress in the Research and Manufacture of GH4169 Alloy

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Journal of Iron and Steel Research International 2015年第8期22卷 657-663页

作者： Jin-hui DU Xu-dong LU Qun DENG zhong-nan bi Beijing Key laboratory of Advanced High Temperature Materials Central Iron and Steel Research Institute

GH4169 alloy has been widely used in fields such as aviation, aerospace, and petrochemical, because of its excellent combination of mechanical and processing properties. These properties include good high-temperature strength, excellent creep and fatigue resistance, and good processing and welding performance. The requirement for high performance, high reliability, and long service life of modem engines has led to the incentive to develop GH4169 alloys with improved performance, such as increased temperature-bearing capacity, improved creep endurance, and better fatigue resistance. Advances during the past thirty years in ba- sic research and industrial technology related to GH4169 alloy were systematically summarized, including advances in alloy modi- fication, melting process optimization, and hot deformation technology.

关键词： GH4169 triple-melt cogging radial forging isothermal forging

Interaction between γ'precipitate distribution and microstructure homogeneity during hot deformation in a Ni-based superalloy

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Journal of Iron and Steel Research International 2023年第11期30卷 2301-2317页

作者： Cheng-yu Wang Teng An Yu Gu zhong-nan bi Jin-hui Du Jing-long Qu Beijing Key Laboratory of Advanced High Temperature Materials Central Iron&Steel Research InstituteBeijing100081China Beijing GAONA Materials&Technology Co. Ltd.Beijing100081China

The inhomogeneous microstructure of the Ni-based superalloys used for turbine disks was an intolerable defect for the mechanical *** effects of the distribution ofγ'precipitate,forging temperature,and strain level on the microstructure evolution of GH4730 alloy were investigated by EBSD during hot *** results showed that the heterogeneous factor peaked at the transition temperature from the single-phase to the double-phase *** coupling effect of heat and stress led to the heterogeneous precipitation and distribution ofγ'phase during the transition region,which was the main reason for the formation of inhomogeneous *** coherentγ'phases of approximately 0.3μm were diffusely distributed inside the large grains,increasing the grain strength,making recrystallization refinement difficult,and thus forming large unrecrystallized *** incoherentγ'phases with a size of approximately 1.1μm located at the grain boundaries and pinned the grain boundaries,and thus the accumulated strain at the grain boundaries caused the occurrence of discontinuous dynamic recrystallization and promoted continuous refinement of the *** microstructure evolution of new Ni-based superalloys during hot forging was focused,and the formation mechanism of inhomogeneous microstructure and control measures was explained.A theoretical basis for improving the microstructure homogeneity of the new cast and wrought superalloys was provided.

关键词： GH4730 alloy Hot deformation γ′phase Heterogeneous factor Microstructure homogeneity

Mechanism of α-Cr precipitation and crystallographic relationships between α-Cr and δ phases in Inconel 718 alloy after long-time thermal exposure

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International Journal of Minerals,Metallurgy and Materials 2010年第3期17卷 312-317页

作者： zhong-nan bi Jian-xin Dong Mai-cang Zhang Lei Zheng Xi-shan Xie School of Materials Science and Engineering University of Science and Technology Beijing Beijing 100083 China

To study the precipitation mechanism of α-Cr phase in Inconel 718 alloy, the samples after long-time aging at 650 and 677℃ were examined by microstructural observations and chemical phase analysis methods. Combining the thermodynamics and kinetics calculation results, α-Cr always precipitates in the vicinity of δ phase, because δ phase rejects Cr into the γ-matrix when growing. The selected area diffraction patterns confirm that the crystallographic relationships of α-Cr with 6 phase are （010）d/（1- 10）*** and [100]d/If 11 ]α-Cr- A graphic model is also presented to show the crystallographic relation between α-Cr and δ phases.

关键词： Inconel 718 precipitation mechanism crystallography thermodynamics kinetics

Machine learning study on time-temperature-transformation diagram of carbon and low-alloy steel

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Journal of Iron and Steel Research International 2023年第5期30卷 1032-1041页

作者： Xiao-ya Huang biao Zhang Qiang Tian Hong-hui Wu bin Gan zhong-nan bi Wei-hua Xue Asad Ullah Hao Wang School of Materials Science and Engineering University of Science and Technology BeijingBeijing 100083China School of Materials Science and Engineering Beihang UniversityBeijing 100191China High Temperature Materials Research Division Central Iron and Steel Research InstituteBeijing 100081China Beijing Advanced Innovation Center for Materials Genome Engineering Collaborative Innovation Center of Steel TechnologyUniversity of Science and Technology BeijingBeijing 100083China Beijing Key Laboratory of Advanced High Temperature Materials Central Iron and Steel Research InstituteBeijing 100081China School of Materials Science and Engineering Liaoning Technical UniversityFuxin 123099LiaoningChina Department of Mathematical Sciences Karakoram International UniversityGilgit-Baltistan 15100Pakistan

Time-temperature-transformation(TTT)diagram plays a critical role in designing appropriate heat treatment process of steels by describing the relationship among holding time,temperature,and quantities of phase *** predictions for TTT diagrams of new steel rapidly and accurately is therefore of much practical importance,especially for costly and time-consuming experimental ***,TTT diagrams for carbon and low-alloy steels were predicted using machine learning *** commonly used machine learning(ML)algorithms,backpropagation artificial neural network(BP network),LibSVM,k-nearest neighbor,Bagging,and Random tree,were adopted to select appropriate models for the *** results illustrate that Bagging is the optimal model for the prediction of pearlite transformation and bainite transformation,and BP network is the optimal model for martensite ***,the ML framework composed of Bagging and BP network models was applied to predict the entire TTT ***,the ML models show superior performance on the prediction of testing samples than the commercial software JMatPro.

关键词： Time-temperature-transformation diagram Carbon steel Low-alloy steel Machine learning Prediction framework

Multi-dimensional bi@C electrocatalyst for Cr3+/Cr2+ redox reaction boosting high-performance iron-chromium flow batteries

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Science China Chemistry 2025年

作者： Min Wu Mingjun nan Shumin Liu Caihe zhong Lin Qiao Huamin Zhang Xiangkun Ma Department of Materials Science and Engineering Dalian Maritime University Division of Energy Storage Dalian National Laboratory for Clean Energy Dalian Institute of Chemical Physics Chinese Academy of Sciences

With the increasing demand for energy storage technology, iron-chromium flow batteries（ICFBs） have been widely concerned because of their price advantage. However, the low electrochemical activity of Cr3+/Cr2+redox couples and the side hydrogen evolution reaction limit the industrial application of ICFBs. A multi-dimensional bi/carbon composite electrocatalyst（bi@C）for ICFB is designed and prepared to improve the electrochemical activity of Cr3+/Cr2+redox couples. Benefiting by using the bimetal organic framework（bi-MOF） with solid matrix as precursors, bi nanospheres are highly dispersed on the bi@C electrocatalyst that effectively enhances the electrochemical activity. The special morphology of bi@C electrocatalyst helps the transfer of electrons and ions, significantly reducing the polarization of battery. Herein, the 3D porous carbon frames accelerate mass transfer, and the 2D carbon nanobelts and carbon layer coating on 0D bi nanospheres improve the conductivity of bi nanospheres. Therefore, the ICFB with multi-dimensional bi@C electrocatalyst exhibits coulombic efficiency of 98.10% and energy efficiency of 79.14% at 140 mA cm-2, which is higher than ICFBs with commercial graphite carbon electrocatalyst and with heat treatment carbon felt. This work provides a simple and economical method to fabricate a high-performance multidimensional bi@C electrocatalyst for Cr3+/Cr2+redox couples, boosting the development of ICFBs.

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Modular assembly of Co4-thiacalix[4]arene units and Keggin-type SiW12O40 for visible-light photothermal conversion

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Tungsten 2025年第1期7卷 112-119页

作者： Jia-Hui Li Qing Zhao Dong-Ao Mao Kun Zhou Bao-Kuan Chen Yan-Feng bi School of Petrochemical Engineering Liaoning Petrochemical University

The construction of metal-organic coordination clusters（MCCs） using modular secondary building units is an important method for preparing functional *** this study,two new MCCs modularly assembled from Keggin-type {SiW12O40}H4TC4A=p-tert-Butylthiacalix[4]arene(SiW12) units and thiacalixarene-supported Co4-thiacalix[4]arene(Co4-TC4A polynuclear second-building units（PSBUs,H4TC4A=p-tert-Butylthiacalix[4]arene） are *** two MCCs,abbreviated as Co4-SiW12and Co8-SiW12,were structurally characterized by single-crystal X-ray *** Co4-SiW12is a supramolecular structure involving cation-anion interactions between Co4-TC4A PSBUs and ***8-SiW12features "barbell-like" shapes with two Co4-TC4A coordinatively linked to a Keggin-type SiW12unit on opposite via W-O_t-Co *** coordination of Co4-TC4A to SiW12in Co8-SiW12resulted in significantly improved photothermal conversion performances compared with Co4-SiW12and pure SiW12or ***-gap determination and photophysical analysis combined with density functional theory calculations indicated the binding mode between Co4-TC4A PSBUs and SiW12,which considerably influences the way of electron transport and the conversion ability of visible light to heat.

关键词： Modular construction Photothermal conversion Polyoxometalate Thiacalixarene

Robust interface and excellent as-built mechanical properties of Ti–6Al–4V fabricated through laser-aided additive manufacturing with powder and wire

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International Journal of Minerals,Metallurgy and Materials 2025年第1期32卷 154-168页

作者： Fei Weng Guijun bi Youxiang Chew Shang Sui Chaolin Tan Zhenglin Du Jinlong Su Fern Lan Ng Key Laboratory for Liquid-Solid Structural Evolution and Processing of Materials Ministry of EducationShandong Engineering&Technology Research Center for Superhard MaterialSchool of Materials Science and EngineeringShandong UniversityJinan 250061China Institute of Intelligent Manufacturing Guangdong Academy of SciencesGuangzhou 510095China Singapore Institute of Manufacturing Technology 5 Cleantech Loop636732Singapore

The feasibility of manufacturing Ti-6Al-4V samples through a combination of laser-aided additive manufacturing with powder(LAAM_(p))and wire(LAAM_(w))was explored.A process study was first conducted to successfully circumvent defects in Ti-6Al-4V deposits for LAAM_(p) and LAAM_(w),*** the optimized process parameters,robust interfaces were achieved between powder/wire deposits and the forged substrate,as well as between powder and wire *** characterization results revealed the epitaxial prior β grains in the deposited Ti-6Al-4V,wherein the powder deposit was dominated by a finerα′microstructure and the wire deposit was characterized by lamellar α *** mechanisms of microstructure formation and correlation with mechanical behavior were analyzed and *** mechanical properties of the interfacial samples can meet the requirements of the relevant Aerospace Material Specifications(AMS 6932)even without post heat *** fracture occurred within the interfacial area,further suggesting the robust *** findings of this study highlighted the feasibility of combining LAAM_(p) and LAAM_(w) in the direct manufacturing of Ti-6Al-4V parts in accordance with the required dimensional resolution and deposition rate,together with sound strength and ductility balance in the as-built condition.

关键词： laser-aided additive manufacturing powder deposition wire deposition interfacial characteristic mechanical behavior

Photosynthetic reaction pathways of natural and artificial systems

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Science China Chemistry 2025年

作者： Shixing Lei Liting bi Lingxuan Chen Zhanting Li Jia Tian State Key Laboratory of Organometallic Chemistry and Shanghai Hong Kong Joint Laboratory in Chemical Synthesis Shanghai Institute of Organic Chemistry University of Chinese Academy of Sciences Chinese Academy of Sciences

Photosynthesis converts solar energy into chemical energy through highly coordinated photosynthetic *** by natural systems,artificial photosynthesis aims to develop an efficient,sustainable,and cost-effective pathway for solar-tochemical *** review examines natural photosynthetic pathways,including retinal/rhodopsin-,bacteriochlorophyll-,and chlorophyll-based systems,highlighting their key components and ***,we outline reaction pathways in artificial photosynthetic systems constructed via heterogeneous,homogeneous,self-assembly,and semi-artificial strategies,focusing on water splitting,carbon fixation,and nitrogen ***,we offer insights into future directions for artificial photosynthesis,emphasizing the importance of using self-assembly strategies and the potential of using primitive phototrophic microorganisms as models.

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Cortico-striatal gamma oscillations are modulated by dopamine D3 receptors in dyskinetic rats

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Neural Regeneration Research 2025年第4期20卷 1164-1177页

作者： Pengfei Wang Yuewei bi Min Li Jiazhi Chen Zhuyong Wang Huantao Wen Ming Zhou Minjie Luo Wangming Zhang Neurosurgery Center Department of Pediatric NeurosurgeryGuangdong Provincial Key Laboratory on Brain Function Repair and RegenerationZhujiang HospitalSouthern Medical UniversityGuangzhouGuangdong ProvinceChina

Long-term levodopa administration can lead to the development of levodopa-induced *** oscillations are a widely recognized hallmark of abnormal neural electrical activity in levodopa-induced ***,studies have reported increased oscillation power in cases of levodopa-induced ***,little is known about how the other electrophysiological parameters of gamma oscillations are altered in levodopa-induced ***,the role of the dopamine D3 receptor,which is implicated in levodopa-induced dyskinesia,in movement disorder-related changes in neural oscillations is *** found that the cortico-striatal functional connectivity of beta oscillations was enhanced in a model of Parkinson’s ***,levodopa application enhanced cortical gamma oscillations in cortico-striatal projections and cortical gamma aperiodic components,as well as bidirectional primary motor cortex(M1)↔dorsolateral striatum gamma *** of PD128907(a selective dopamine D3 receptor agonist)induced dyskinesia and excessive gamma oscillations with a bidirectional M1↔dorsolateral striatum ***,administration of PG01037(a selective dopamine D3 receptor antagonist)attenuated dyskinesia,suppressed gamma oscillations and cortical gamma aperiodic components,and decreased gamma causality in the M1→dorsolateral striatum *** findings suggest that the dopamine D3 receptor plays a role in dyskinesia-related oscillatory activity,and that it has potential as a therapeutic target for levodopa-induced dyskinesia.

关键词： aperiodic components dopamine D3 receptor dorsolateral striatum functional connectivity gamma oscillations levodopa-induced-dyskinesia local field potentials neuromodulation Parkinson’s disease primary motor cortex