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Mechanical properties and thermal deformation behavior of low-cost titanium matrix composites prepared by a structure-optimized Y_(2)O_(3) crucible

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Journal of Iron and Steel Research(International) 2024年第3期31卷 738-751页

作者： Qian Dang Gang Huang Ye wang Chi Zhang Guo-huai Liu zhao-dong wang The State Key Laboratory of Rolling and Automation Northeastern UniversityShenyang 110819LiaoningChina School of Materials Science and Chemical Engineering Harbin University of Science and TechnologyHarbin 150004HeilongjiangChina School of Materials Science and Engineering Shenyang University of TechnologyShenyang 110870LiaoningChina

A porous yttrium oxide crucible with both thermal shock resistance and erosion resistance was developed by structural *** structure-optimized yttrium oxide crucible was proved to be suitable for melting highly reactive titanium ***-cost(TiB+Y2O_(3))-reinforced titanium matrix composites were prepared by vacuum induction melting using the prepared *** thermal deformation behavior and microstructure evolution of(TiB+Y2O_(3))-reinforced tita-nium matrix composites were investigated at deformation temperatures of 900-1100℃with strain rates of 0.001-1 *** results showed that the prepared yttrium oxide crucible had both thermal shock and erosion resistance,the low-cost titanium matrix composites could be prepared by the developed yttrium oxide crucibles which were homogeneous in composition and highly sensitive to strain rate and deformation temperature,and the peak and theological stresses decreased with increasing deformation temperature or decreasing strain *** addition,the average thermal deformation activation energy of the composites was calculated to be 574.6 kJ/mol by establishing the Arrhenius constitutive equation in consideration of the strain variables,and the fitting goodness between the predicted stress value and the measured value was 97.624%.The calculated analysis of the hot processing map showed that the best stable thermal deformation zone was located in the deformation temperature range of 1000-1100℃and strain rate range of 0.001-0.01 s^(-1),where the peak dissipation coefficient wasη=71%.In this zone,the deformation of the reinforcement and matrix was harmonious,the reinforcement was less likely to fracture,dynamic recrystallization occurred more fully and the alloy exhibited near steady rheological characteristics.

关键词： Yttrium oxide crucible Titanium matrix composite Thermal deformation behavior Constitutive equation Hot processing map Microstructure evolution

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Synergistic effects of multiscale TiC and dual-phase structure on tensile properties of particle-reinforced steel

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Journal of Iron and Steel Research(International) 2024年第5期31卷 1232-1245页

作者： Ye Jia Xiang-tao Deng Qi wang Cheng-ru Li Hao Wu zhao-dong wang State Key Laboratory of Rolling and Automation Northeastern UniversityShenyang110819LiaoningChina

The conventional melting methods were used to obtain in situ TiC particle-reinforced dual-phase steel,followed by hot rolling and heat treatment *** aim was to investigate the effect of TiC particles on the fracture behavior of dual-phase steel at different annealing temperatures,by analyzing the microstructure and tensile behavior of the multiscale TiC particle-reinforced dual-phase *** results showed that TiC particles precipitated in the as-cast microstructure of dual-phase steel were distributed along the grain *** hot rolling,the grain boundary-like morphology of the micron-sized TiC particles was disrupted,and the particles became more refined and evenly distributed in the *** tensile tests revealed that the strength of the TiC particle-reinforced dual-phase steel increased with increasing martensite content,while the elongation *** results were similar to those of conventional *** addition of 1 vol.%multiscale TiC particles improved the strength of the dual-phase steel but did not affect elongation of the *** and holes were primarily concentrated around the TiC particles rather than at the interface of martensite and *** main causes of crack sprouting were TiC particle interface cracking and TiC particle internal ***,the study demonstrated the potential of multiscale TiC particle-reinforced dual-phase steel as a strong and tough *** refined distribution of TiC particles in the matrix improved the strength of the material without compromising its *** results also highlighted the importance of careful selection of reinforcement particles to avoid detrimental effects on the fracture behavior of the material.

关键词： TiC particle Dual-phase structure TiC-reinforced dual-phase steel Tension Fracture behavior

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Atomic-Scale Insights into Damage Mechanisms of GGr15 Bearing Steel Under Cyclic Shear Fatigue

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Acta Metallurgica Sinica(English Letters) 2024年第7期37卷 1265-1278页

作者： Qiao-Sheng Xia dong-Peng Hua Qing Zhou Ye-Ran Shi Xiang-Tao Deng Kai-Ju Lu Hai-Feng wang Xiu-Bing Liang zhao-dong wang State Key Laboratory of Solidification Processing Center of Advanced Lubrication and Seal MaterialsNorthwestern Polytechnical UniversityXi’an710072China State Key Laboratory of Rolling and Automation Northeastern UniversityShenyang110819China Defense Innovation Institute Academy of Military ScienceBeijing100071China

Alternating shear stress is a critical factor in the accumulation of damage during rolling contact fatigue,severely limiting the service life of ***,the specific mechanisms responsible for the cyclic shear fatigue damage in bearing steel have not been fully *** the mechanical response and microstructural evolution of a model GGr15 bearing steel under cyclic shear loading are investigated through the implementation of molecular dynamics *** samples undergo 30 cycles under three different loading conditions with strains of 6.2%,9.2%,and 12.2%,*** findings indicate that severe cyclic shear deformation results in early cyclic softening and significant accumulation of plastic damage in the bearing ***,samples subjected to higher strain-controlled loading exhibit higher plastic strain energy and shorter fatigue ***,strain localization is identified as the predominant damage mechanism in cyclic shear fatigue of the bearing steel,which accumulates and ultimately results in fatigue ***,simulation results also revealed the microstructural reasons for the strain localization(e.g.,BCC phase transformation into FCC and HCP phase),which well explained the formation of white etching *** study provides fresh atomic-scale insights into the mechanisms of cyclic shear fatigue damage in bearing steels.

关键词： Cyclic shear fatigue Molecular dynamic simulation Bearing steels Plastic damage accumulation

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Solidification microstructure of Ti-43Al alloy by twin-roll strip casting

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China Foundry 2023年第2期20卷 99-107页

作者： Yang Chen Guo-huai Liu Ye wang zhao-dong wang State Key Laboratory of Rolling and Automation Northeastern UniversityShenyang 110819China College of Material Science and Chemical Engineering Harbin University of Science and TechnologyHarbin 150080China

As a near-net-shape technology,the twin-roll strip casting(TRC)process can be considered to apply to the fabrication of TiAl alloy ***,the control of the grain distribution is very important in strip casting because the mechanical properties of strips are directly determined by the solidification microstructure.A three-dimensional(3D)cellular automation finite-element(CAFE)model based on ProCAST software was established to simulate the solidification microstructure of Ti-43Al ***,the influence of casting temperature and the maximum nucleation density(nmax)on the solidification microstructure was investigated in *** simulation results provide a good explanation and prediction for the solidification microstructure in the molten pool before leaving the kissing *** and simulated microstructure show the common textureorientation in the columnar grains ***,the microstructure evolution of the Ti-43Al alloy was analyzed and the solidification phase transformation path during the TSC process was determined,i.e.,L→L+β→β→β+α→α+γ+β/B2 phase under a faster cooling rate and L→L+β→β→β+α→γ+lamellar(α_(2)+γ)+β/B2 phase under a slower cooling rate.

关键词： TiAl alloy simulation microstructure strip casting solidification

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Optimization of investment casting process for K477 superalloy aero-engine turbine nozzle by simulation and experiment

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China Foundry 2022年第4期19卷 351-358页

作者： Xin Hao Guo-huai Liu Ye wang Shi-ping Wu zhao-dong wang AECC South Industry Company Limited Zhuzhou 412002HunanChina State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi'an 710072China State Key Laboratory of Rolling and Automation Northeastern UniversityShenyang 110819China School of Materials Science and Chemical Engineering Harbin University of Science and TechnologyHarbin 150001China School of Materials Science and Engineering Harbin Institute of TechnologyHarbin 150001China

In order to reduce the shrinkage porosity of nickel-based superalloy castings in the investment casting process,the effects of different gating systems on mold filling,solidification process,and prediction of shrinkage porosity of aero-engine turbine nozzle castings were investigated by simulation and experimental *** show that the design of the vertical runner would cause greater turbulence of the melt in the riser during the mold filling process,and the outer runner is not *** the decrease in number of runners,the hot spot moves down towards the casting,and the shrinkage and porosity defects are formed in the casting below the *** the original designs,a certain tendency of shrinkage and porosity defect is found in the vanes,inner rings,and outer rings of the castings by both simulation prediction and ***,based on the processing optimization,the aero-engine turbine nozzle casting with no shrinkage and porosity defects is obtained.

关键词： nickel-based superalloy investment casting shrinkage porosity simulation optimization

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Tracking lithiation with transmission electron microscopy

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Science China Chemistry 2024年第1期67卷 291-311页

作者： Xincheng Lei Jianxiong zhao Jiayi wang dong Su Beijing National Laboratory for Condensed Matter Physics Institute of PhysicsChinese Academy of SciencesBeijing 100190China South China Academy of Advanced Optoelectronics&International Academy of Optoelectronics at zhaoqing South China Normal UniversityGuangzhou 510006China

Li-ion batteries(LIBs)have dominated energy-storage techniques for portable electronic devices and electric cars,and are expanding their territory into the large-scale energy *** energy storage of LIBs is realized by the reversible shuttle of lithium ions between *** is essential to track the lithium diffusion and obtain a profound insight into the lithiation mechanism during the work cycle of *** electron microscopy(TEM)is a powerful tool for the structural characterization,which can provide the information about the lithiation at the atomic *** this review,we summarize the research frontiers of TEM applications on *** introduce the techniques for the direct observation of Li species in LIB-related ***,the application of cryo-TEM is ***,in-situ TEM technique is further discussed since it shows great advantages in studying the dynamical structure changes of *** perspectives and strategies in this review offer feasible guidance for researchers to further improve the performance of LIBs.

关键词： lithium-ion battery electrode materials transmission electron microscopy cryo-TEM in-situ TEM

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Effect of competitive crystal growth on microstructural characteristics of directionally solidified nickel-based single crystal superalloy

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China Foundry 2022年第2期19卷 109-116页

作者： Mang Xu Xiao-qi Geng Xiang-long Zhang Guo-huai Liu Ye wang zhao-dong wang Jing-jie Guo State Key Laboratory of Rolling and Automation Northeastern UniversityShenyang 110819China School of Materials Science and Engineering Harbin University of Science and TechnologyHarbin 150040China School of Materials Science and Engineering Harbin Institute of TechnologyHarbin 150001China

Directionally solidified single crystal superalloy test bars were prepared by the spiral grain selection *** microstructural evolution and orientation characteristics of the starter block and spiral part were studied,and the influence of the competitive growth of crystals on the microstructural characteristics was *** results show that the divergent grain groups,with small size and randomly oriented grains,appear at the bottom of the start block due to the chilling effect,which is an important area for competitive *** the height of the starter block increases,the primary dendrite spacing increases,and the grain density decreases;furthermore,the proportion of grains with an orientation deflection angle less than 10°gradually ***texture gradually becomes stronger as the height of the starter block increases,which indicates that the competitive growth of crystals gradually *** the initial stage of the crystal selection in the spiral part,the obstacle of adjacent grains and spiral passage is the main working *** grains located at the inner side of the front edge of the spiral passage have the growth *** single crystal screening process is achieved at about two-thirds of the spiral height,and the single crystal with the orientation deviation angle of 6.7°from the casting axis is prepared.

关键词： directional solidification Ni-based superalloy microstructural evolution spiral grain selector single crystal

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Roles of nanoscale precipitates and metastable austenite in determining strength and toughness of high-strength Nb-bearing steel

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Journal of Iron and Steel Research(International) 2022年第10期29卷 1646-1658页

作者： Qi-bin Ye Cheng Zhou Jun Hu Xiao-lan Gong Yong Tian Xiu-hua Gao zhao-dong wang State Key Laboratory of Rolling and Automation Northeastern UniversityShenyang110819LiaoningChina

The effects of tempering temperature on the microstructure and mechanical properties of high-strength structural steel containing niobium were investigated to examine the roles of nanoscale precipitates and metastable austenite in determining the yield strength and *** hot-rolling and quenching,three experimental steels were tempered at 590,630,and 670℃.During tempering,nanoscale Nb(C,N)precipitates were formed with the recovery of quenched *** average diameters of Nb(C,N)precipitates increased from 5.4 to 8.2 nm as the tempering temperature was ***,reversed austenite with a volume fraction of 9%was formed at tempering temperatures up to 670℃.The yield strengths of steel containing tempered martensite tempered at 590 and 630℃ were 965 and 831 MPa,and the tensile strengths were 998 and 879 MPa,***,the steel comprising reversed austenite and tempered martensite tempered at 670℃ showed continuous yielding behavior,affording yield and tensile strengths of 610 and 889 MPa,*** impact energy increased from 105 to 260 J at−60℃ with increasing tempering *** austenite improves low-temperature toughness by significantly increasing the crack propagation energy.

关键词： High-strength structural steel Tempering Nanoscale precipitate Metastable austenite Mechanical property

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Influence of cooling rate on phase transformation and precipitation behavior of Ti-bearing steel in continuous cooling process

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Journal of Iron and Steel Research(International) 2022年第1期29卷 165-174页

作者： Xiao-lin Li Chi Jin Hao-zhe Li Xiao-xiao Hao Yi He Xiang-tao Deng zhao-dong wang State Key Laboratory of Solidification Processing Center of Advanced Lubrication and Seal MaterialsNorthwestern Polytechnical UniversityXi’an 710072ShaanxiChina State Key Laboratory of Rolling and Automation Northeastern UniversityShenyang 110819LiaoningChina

The influence of cooling rate on microstructural evolution and precipitation behavior in Ti,Ti–Nb and Ti-Mo low-carbon steels during the continuous cooling process was studied by dilatometer method,optical microscopy,and transmission electron *** results indicated that austenite transformation temperature decreased with the increasing cooling rate in three *** addition of Nb and Mo promoted bainite and martensite transformation and improved the hardenability of *** addition,precipitates formed in deformed austenite and ferrite can be observed *** in the austenite non-recrystallization zone can introduce a large number of deformation bands,and then,the precipitates preferentially nucleated in these deformation *** the following process,randomly distributed precipitates and interphase precipitates will be formed in *** precipitates formed in deformed austenite obey Kurdjumov-Sachs orientation relationship with the matrix,while the precipitates formed in ferrite obey Baker-Nutting orientation relationship with the *** addition of Nb and Mo in Ti-bearing steels decreased the precipitates size and increased the number density of precipitates and then improved the precipitation *** the effect of Mo addition is more obvious than that of Nb addition.

关键词： Ti-microalloyed steel Continuous cooling transformation Precipitation behavior Precipitate-free zone Orientation relationship

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Superhydrophilic nickel hydroxide ultrathin nanosheets enable high-performance asymmetric supercapacitors

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Rare Metals 2024年第1期43卷 138-147页

作者： Yi-Ran wang Fei Zhang Jian-Min Gu Xiao-Yu zhao Ran zhao Xing wang Tian-Hui Wu Jing wang Ji-dong wang De-Song wang State Key Laboratory of Metastable Materials Science and Technology(MMST) Hebei Key Laboratory of Applied ChemistryYanshan UniversityQinhuangdao 066004China Department of Food and Pharmaceutical Engineering Suihua UniversitySuihua 152000China School of Chemical Science and Engineering Tongji UniversityShanghai 200092China School of Sciences Hebei University of Science and TechnologyShijiazhuang 050018China

Superhydrophilic surfaces have been applied for supercapacitor;however,during energy storage reaction,how the wettability affects the process of electrochemical reaction specifically is still ***,we demonstrate superhydrophilic surface for promotion of electrochemical reactions by liquid affinity and further explain the mechanism,where the transition of the wettability state caused by the change in surface free energy is the main reason for the obvious increase in specific *** citric acid assistance strategy,an intrinsically hydrophobic Ni(OH)_(2)thick nanosheets(HNHTNs,16 nm)can be transitioned into superhydrophilic Ni(OH)_(2)ultrathin nanosheets(SNHUNs,6.8 nm),where the water contact angle was 0°and the surface free energy increased from 8.6to 65.8 mN·m^(-1),implying *** with HNHTNs,the specific capacitance of SNHUNs is doubled:from 1230 F·g^(-1)(HNHTNs)to 2350 F·g^(-1)(2A·g^(-1))and,even at 20 A·g^(-1),from 833 F·g^(-1)(HNHTNs)to 1670 F·g^(-1).The asymmetric capacitors assembled by SNHUNs and activated carbon show 52.44 Wh·kg^(-1)at 160W·kg^(-1)and excellent stability with~90%retention after5000 cycles(~80%retention after 9500 cycles).The promotion of electrochemical performances is ascribed to the change of surface wettability caused by surface free energy,which greatly increase affinity of electrode to the surrounding liquid environment to reduce the interface resistance and optimize the electron transport path.

关键词： Asymmetric supercapacitor Superhydrophilic interface Transition metal hydroxides Ultrathin nanosheets High specific capacitance

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