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Dual nanoprecipitation and nanoscale chemical heterogeneity in a secondary hardening steel for ultrahigh strength and large uniform elongation

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Journal of Materials Science & Technology 2024年第18期185卷 245-258页

作者： Shidong Wang Jinhua Wang Shijie Zhang Daixiu Wei Yang Chen Xuequan Rong Wu Gong Stefanus Harjo Xiaochun Liu zengbao jiao Zhigang Yang Gang Sha Chunxu Wang Guang Chen Hao Chen Key Laboratory for Advanced Materials of Ministry of Education School of Materials Science and EngineeringTsinghua UniversityBeijing 100084China School of Materials Science and Engineering/Herbert Gleiter Institute of Nanoscience Nanjing University of Science and TechnologyNanjing 210094China National Key Laboratory of Advanced Casting Technologies MIIT Key Laboratory of Advanced Metallic and Intermetallic Materials TechnologyEngineering Research Center of Materials Behavior and DesignMinistry of EducationNanjing University of Science and TechnologyNanjing 210094China J-PARC Center Japan Atomic Energy AgencyIbaraki 319-1195Japan Institute of Metals College of Materials Science and EngineeringChangsha University of Science&TechnologyChangsha 410114China Department of Mechanical Engineering Research Institute for Advanced ManufacturingThe Hong Kong Polytechnic UniversityHong Kong 999077China Central Iron and Steel Research Institute Beijing 100081China

Nanoprecipitates and nanoscale retained austenite(RA)with suitable stability play crucial roles in deter-mining the yield strength(YS)and ductility of ultrahigh strength steels(UHSSs).However,owing to the kinetics incompatibility between nanoprecipitation and austenite reversion,it is highly challenging to si-multaneously introduce high-density nanoprecipitates and optimized RA in *** this work,through the combination of austenite reversion treatment(ART)and subsequent flash austenitizing(FA),nanoscale chemical heterogeneity was successfully introduced into a low-cost UHSS prior to the aging *** chemical heterogeneity involved the enrichment of Mn and Ni in the austenite *** resulting UHSS exhibited dual-nanoprecipitation of Ni(Al,Mn)and(Mo,Cr)_(2)C and nanoscale austenite stabilized via Mn and Ni *** hard martensitic matrix strengthened by high-density dual-nanoprecipitates con-strains the plastic deformation of soft RA with a relatively low fraction of-15%,and the presence of relatively stable nanoscale RA with adequate Mn and Ni enrichment leads to a marginal loss in YS but keeps a persistent transformation-induced plasticity(TRIP)*** a result,the newly-developed UHSS exhibits an ultrahigh YS of-1.7 GPa,an ultimate tensile strength(UTS)of-1.8 GPa,a large uniform elongation(UE)of-8.5%,and a total elongation(TE)of-13%.The strategy of presetting chemical heterogeneity to introduce proper metastable phases before aging can be extended to other UHSSs and precipitation-hardened alloys.

关键词： Ultrahigh strength steels Dual-nanoprecipitation Austenite stability TRIP effect Phase transformation

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Low-carbon advanced nanostructured steels:Microstructure, mechanical properties, and applications

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Science China Materials 2021年第7期64卷 1580-1597页

作者： Haojie Kong zengbao jiao Jian Lu Chain Tsuan Liu Department of Mechanical Engineering City University of Hong KongHong KongChina Department of Mechanical Engineering&Shenzhen Research Institute The Hong Kong Polytechnic UniversityHong KongChina Department of Materials Science and Engineering City University of Hong KongHong KongChina Center for Advanced Structural Materials Department of Mechanical EngineeringCity University of Hong KongHong KongChina Hong Kong Institute for Advanced Study City University of Hong KongHong KongChina

Low-carbon advanced nanostructured steels have been developed for various structural engineering applications, including bridges, automobiles, and other strength-critical applications such as the reactor pressure vessels in nuclear power stations. The mechanical performances and applications of these steels are strongly dependent on their microstructural features. By controlling the size,number density, distribution, and types of precipitates, it is possible to produce nanostructured steels with a tensile strength reaching as high as 2 GPa while keeping a decent tensile elongation above 10% and a reduction of area as high as 40%. Besides, through a careful control of strength contributions from multiple strengthening mechanisms, the nanostructured steels with superior strengths and low-temperature impact toughness can be obtained by avoiding the temper embrittlement regime. With appropriate Mn additions, these nanostructured steels can achieve a triple enhancement in ductility(total tensile elongation, TE of ~30%) at no expense of strengths(yield strength, YS of ~1100 to 1300 MPa, ultimate tensile strength, UTS of ~1300 to 1400 MPa). More importantly, these steels demonstrate good fabricability and weldability. In this paper, the microstructure-property relationships of these advanced nanostructured steels are comprehensively reviewed. In addition, the current limitations and future development of these nanostructured steels are carefully discussed and outlined.

关键词： heterogeneous nano-precipitates strength-ductility paradox embrittlement dislocation interactions

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通过介导相分离制备的纳米结构W-Cu基复合材料的性能

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Engineering 2023年第7期26卷 173-184,I0007页

作者：侯超吕皓赵治 Xintao Huang 韩铁龙 Junhua Luan zengbao jiao 宋晓艳 Zuoren Nie Key Laboratory of Advanced Functional Materials Ministry of EducationFaculty of Materials and ManufacturingBeijing University of TechnologyBeijing 100124China Department of Materials Science and Engineering City University of Hong KongHong Kong 999077China Department of Mechanical Engineering The Hong Kong Polytechnic UniversityHong Kong 999077China

The challenge of fabricating nanostructured W–Cu composites by powder metallurgy has been solved by means of modulated phase separation.A hierarchically nanostructured(HN)W–Cu composite was prepared using intermediary Al through sluggish asynchronous phase *** addition to a dual network composed of a Cu phase and the W–Cu nanostructure,dense Al-containing nanoprecipitates with a body-centered cubic(bcc)structure are distributed in the W *** with a pristine W/Cu interface,the newly formed W/Cu interfaces modulated by Al and the coherent W/Al-containing particle interfaces possess lower energy and enhanced bonding strength due to efficient electron transfer and strong coupling *** a large number of stable heterogeneous interfaces and a“selflocking”geometry,the HN W–Cu composite exhibits excellent resistance against plastic *** combination of the presented composite’s hardness and compressive strength outperforms all other sintered W–Cu composites with the same Cu *** a reciprocating sliding load,the reactive Al prevents excessive *** excellent synergy of the hardness and toughness of the friction-induced surface endows the HN composite with high abrasion *** study provides a new strategy to modulate the structure and energy state of interfaces in metallic composites containing immiscible components in order to achieve high mechanical performance.

关键词： Immiscible-component composite Phase separation Nanostructure Mechanical properties Interface modulation

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Single-element amorphous palladium nanoparticles formed via phase separation

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Nano Research 2022年第6期15卷 5575-5580页

作者： Dong Sheng He Yi Huang Benjamin D.Myers Dieter Isheim Xinyu Fan Guang-Jie Xia Yunsheng Deng Lin Xie Shaobo Han Yang Qiu Yang-Gang Wang Junhua Luan zengbao jiao Li Huang Vinayak P.Dravid Jiaqing He Pico Center and Department of Physics Southern University of Science and TechnologyShenzhen 518055China Department of Materials Science and Engineering Northwestern UniversityEvanstonIL 60208USA Department of Chemistry and Guangdong Provincial Key Laboratory of Catalytic Chemistry Southern University of Science and TechnologyShenzhen 518055China Department of Materials Science and Engineering Southern University of Science and TechnologyShenzhen 518055China Department of Materials Science and Engineering City University of Hong KongHong KongChina Department of Mechanical Engineering The Hong Kong Polytechnic UniversityHong KongChina

Physically vitrifying amorphous single-element metal requires ultrahigh cooling rates,which are still unachievable for most of the closest-packed ***,we report a facile chemical synthetic strategy for single-element amorphous palladium nanoparticles with a purity of 99.35 at.%±0.23 at.%from palladium–silicon liquid ***-situ transmission electron microscopy directly detected the solidification of palladium and the separation of *** hydrogen absorption experiment showed that the amorphous palladium expanded little upon hydrogen uptake,exhibiting a great potential application for hydrogen *** results provide insight into the formation of amorphous metal at nanoscale.

关键词： Pd single-element metallic glass nanoparticle phase separation undercooling

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通过介导相分离制备的纳米结构W-Cu基复合材料的性能（英文）

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Engineering 2023年第7期 173-184页

作者：侯超吕皓赵治 Xintao Huang 韩铁龙 Junhua Luan zengbao jiao 宋晓艳 Zuoren Nie Key Laboratory of Advanced Functional Materials Ministry of Education Faculty of Materials and Manufacturing Beijing University of Technology Department of Materials Science and Engineering City University of Hong Kong Department of Mechanical Engineering The Hong Kong Polytechnic University

The challenge of fabricating nanostructured W–Cu composites by powder metallurgy has been solved by means of modulated phase separation. A hierarchically nanostructured(HN) W–Cu composite was prepared using intermediary Al through sluggish asynchronous phase separation. In addition to a dual network composed of a Cu phase and the W–Cu nanostructure, dense Al-containing nanoprecipitates with a body-centered cubic(bcc) structure are distributed in the W matrix. Compared with a pristine W/Cu interface, the newly formed W/Cu interfaces modulated by Al and the coherent W/Al-containing particle interfaces possess lower energy and enhanced bonding strength due to efficient electron transfer and strong coupling interactions. With a large number of stable heterogeneous interfaces and a “self-locking” geometry, the HN W–Cu composite exhibits excellent resistance against plastic *** combination of the presented composite’s hardness and compressive strength outperforms all other sintered W–Cu composites with the same Cu content. Under a reciprocating sliding load, the reactive Al prevents excessive oxidation. The excellent synergy of the hardness and toughness of the friction-induced surface endows the HN composite with high abrasion resistance. This study provides a new strategy to modulate the structure and energy state of interfaces in metallic composites containing immiscible components in order to achieve high mechanical performance.

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The autophagy-lysosome pathway:a potential target in the chemical and gene therapeutic strategies for Parkinson’s disease

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Neural Regeneration Research 2025年第1期20卷 139-158页

作者： Fengjuan jiao Lingyan Meng Kang Du Xuezhi Li School of Mental Health Jining Medical UniversityJiningShandong ProvinceChina Shandong Collaborative Innovation Center for Diagnosis Treatment and Behavioral Interventions of Mental DisordersInstitute of Mental HealthJining Medical UniversityJiningShandong ProvinceChina

Parkinson’s disease is a common neurodegenerative disease with movement disorders associated with the intracytoplasmic deposition of aggregate proteins such asα-synuclein in *** one of the major intracellular degradation pathways,the autophagy-lysosome pathway plays an important role in eliminating these *** evidence has shown that upregulation of the autophagy-lysosome pathway may contribute to the clearance ofα-synuclein aggregates and protect against degeneration of dopaminergic neurons in Parkinson’s ***,multiple genes associated with the pathogenesis of Parkinson’s disease are intimately linked to alterations in the autophagy-lysosome ***,this pathway appears to be a promising therapeutic target for treatment of Parkinson’s *** this review,we briefly introduce the machinery of ***,we provide a description of the effects of Parkinson’s disease–related genes on the autophagy-lysosome ***,we highlight the potential chemical and genetic therapeutic strategies targeting the autophagy–lysosome pathway and their applications in Parkinson’s disease.

关键词： autophagy chemical therapy gene therapy Parkinson’s disease α-synuclein

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Advances in the Development of Gradient Scaffolds Made of Nano-Micromaterials for Musculoskeletal Tissue Regeneration

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NANO-MICRO LETTERS 2025年第1期17卷 1-46页

作者： Fang, Lei Lin, Xiaoqi Xu, Ruian Liu, Lu Zhang, Yu Tian, Feng Li, jiao jiao Xue, Jiajia Beijing Univ Chem Technol Beijing Lab Biomed Mat Beijing 100029 Peoples R China Beijing Univ Chem Technol State Key Lab Organ Inorgan Composites Beijing 100029 Peoples R China Univ Technol Sydney Fac Engn & IT Sch Biomed Engn Sydney NSW 2007 Australia

This review highlights the gradient variations in the structural composition of musculoskeletal tissues and comprehensively examines recent progress in the fabrication and application of biomimetic gradient scaffolds for musculoskeletal *** challenges and prospects of gradient scaffolds for clinical application are discussed. The intricate hierarchical structure of musculoskeletal tissues, including bone and interface tissues, necessitates the use of complex scaffold designs and material structures to serve as tissue-engineered substitutes. This has led to growing interest in the development of gradient bone scaffolds with hierarchical structures mimicking the extracellular matrix of native tissues to achieve improved therapeutic outcomes. Building on the anatomical characteristics of bone and interfacial tissues, this review provides a summary of current strategies used to design and fabricate biomimetic gradient scaffolds for repairing musculoskeletal tissues, specifically focusing on methods used to construct compositional and structural gradients within the scaffolds. The latest applications of gradient scaffolds for the regeneration of bone, osteochondral, and tendon-to-bone interfaces are presented. Furthermore, the current progress of testing gradient scaffolds in physiologically relevant animal models of skeletal repair is discussed, as well as the challenges and prospects of moving these scaffolds into clinical application for treating musculoskeletal injuries.

关键词： Gradient scaffolds Musculoskeletal tissues Advanced manufacturing Biomaterials Tissue regeneration

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High-energy-density lithium manganese iron phosphate for lithium-ion batteries: Progresses, challenges, and prospects

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Journal of Energy Chemistry 2025年第1期100卷 1-17页

作者： Bokun Zhang Xiaoyun Wang Shuai Wang Yan Li Libo Chen Handong jiao Zhijing Yu Jiguo Tu State Key Laboratory of Advanced Metallurgy University of Science and Technology Beijing Research Institute for Intelligent Wearable Systems The Hong Kong Polytechnic University Institute of Advanced Structure Technology Beijing Institute of Technology

The soaring demand for smart portable electronics and electric vehicles is propelling the advancements in high-energy–density lithium-ion *** manganese iron phosphate (LiMnxFe1-xPO4) has garnered significant attention as a promising positive electrode material for lithium-ion batteries due to its advantages of low cost,high safety,long cycle life,high voltage,good high-temperature performance,and high energy *** LiMnxFe1-xPO4has made significant breakthroughs in the past few decades,there are still facing great challenges in poor electronic conductivity and Li-ion diffusion,manganese dissolution affecting battery cycling performance,as well as low tap *** review systematically summarizes the reaction mechanisms,various synthesis methods,and electrochemical properties of LiMnxFe1-xPO4to analyze reaction processes accurately and guide material ***,the main challenges currently faced are concluded,and the corresponding various modification strategies are discussed to enhance the reaction kinetics and electrochemical performance of LiMnxFe1-xPO4,including multi-scale particle regulation,heteroatom doping,surface coating,as well as microscopic morphology ***,in view of the current research challenges faced by intrinsic reaction processes,kinetics,and energy storage applications,the promising research directions are *** importantly,it is expected to provide key insights into the development of high-performance and stable LiMnxFe1-xPO4materials,to achieve practical energy storage requirements.

关键词： Lithium manganese iron phosphate High energy density Lithium-ion batteries Reaction mechanism Tap density

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SensFL:Privacy-Preserving Vertical Federated Learning with Sensitive Regularization

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Computer Modeling in Engineering & Sciences 2025年第1期142卷 385-404页

作者： Chongzhen Zhang Zhichen Liu Xiangrui Xu Fuqiang Hu jiao Dai Baigen Cai Wei Wang School of Automation and Intelligence Beijing Jiaotong UniversityBeijing100044China Shuohuang Railway Development Co. Ltd.National Energy GroupCangzhou062350China Beijing Key Laboratory of Security and Privacy in Intelligent Transportation School of Computer Science and TechnologyBeijing Jiaotong UniversityBeijing100044China

In the realm of Intelligent Railway Transportation Systems,effective multi-party collaboration is crucial due to concerns over privacy and data *** Federated Learning(VFL)has emerged as a promising approach to facilitate such collaboration,allowing diverse entities to collectively enhance machine learning models without the need to share sensitive training ***,existing works have highlighted VFL’s susceptibility to privacy inference attacks,where an honest but curious server could potentially reconstruct a client’s raw data from embeddings uploaded by the *** vulnerability poses a significant threat to VFL-based intelligent railway transportation *** this paper,we introduce SensFL,a novel privacy-enhancing method to against privacy inference attacks in ***,SensFL integrates regularization of the sensitivity of embeddings to the original data into the model training process,effectively limiting the information contained in shared *** reducing the sensitivity of embeddings to the original data,SensFL can effectively resist reverse privacy attacks and prevent the reconstruction of the original data from the *** experiments were conducted on four distinct datasets and three different models to demonstrate the efficacy of *** results show that SensFL can effectively mitigate privacy inference attacks while maintaining the accuracy of the primary learning *** results underscore SensFL’s potential to advance privacy protection technologies within VFL-based intelligent railway systems,addressing critical security concerns in collaborative learning environments.

关键词： Vertical federated learning privacy defenses

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Pathogenesis, diagnosis, and treatment of epilepsy: electromagnetic stimulation-mediated neuromodulation therapy and new technologies

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Neural Regeneration Research 2025年第4期20卷 917-935页

作者： Dian jiao Lai Xu Zhen Gu Hua Yan Dingding Shen Xiaosong Gu Academy of Medical Engineering and Translational Medicine Tianjin UniversityTianjinChina Key Laboratory of Advanced Drug Delivery Systems of Zhejiang Province College of Pharmaceutical SciencesZhejiang UniversityHangzhouZhejiang ProvinceChina Affiliated Hospital of Nantong University NantongJiangsu ProvinceChina

Epilepsy is a severe,relapsing,and multifactorial neurological *** regarding the accurate diagnosis,prognosis,and in-depth pathogenesis are crucial for the precise and effective treatment of *** pathogenesis of epilepsy is complex and involves alterations in variables such as gene expression,protein expression,ion channel activity,energy metabolites,and gut microbiota *** results are lacking for conventional treatments for *** resection of lesions,drug therapy,and non-drug interventions are mainly used in clinical practice to treat pain associated with ***-pharmacological treatments,such as a ketogenic diet,gene therapy for nerve regeneration,and neural regulation,are currently areas of research *** review provides a comprehensive overview of the pathogenesis,diagnostic methods,and treatments of *** also elaborates on the theoretical basis,treatment modes,and effects of invasive nerve stimulation in neurotherapy,including percutaneous vagus nerve stimulation,deep brain electrical stimulation,repetitive nerve electrical stimulation,in addition to non-invasive transcranial magnetic stimulation and transcranial direct current *** studies have shown that electromagnetic stimulation-mediated neuromodulation therapy can markedly improve neurological function and reduce the frequency of epileptic ***,many new technologies for the diagnosis and treatment of epilepsy are being ***,current research is mainly focused on analyzing patients’clinical manifestations and exploring relevant diagnostic and treatment methods to study the pathogenesis at a molecular level,which has led to a lack of consensus regarding the mechanisms related to the disease.

关键词： diagnosis drug treatment electroencephalography epilepsy monitoring epilepsy nerve regeneration neurostimulation non-drug interventions pathogenesis prediction

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