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Thermally Conductive,Healable Glass Fiber Cloth Reinforced Polymer Composite based onβ-Hydroxyester Bonds Crosslinked Epoxy with Improved Heat Resistance

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Chinese Journal of Polymer Science 2024年第5期42卷 643-654,I0009页

作者： Fang Chen Xiao-Yan Pang ze-ping Zhang Min-Zhi Rong Ming-Qiu Zhang Key Laboratory for Polymeric Composite and Functional Materials of Ministry of Education GD HPPC LabIGCMESchool of ChemistrySun Yat-sen UniversityGuangzhou510275China Guangdong Provincial Laboratory of Chemistry and Fine Chemical Engineering Jieyang Center Jieyang515200China

To simultaneously endow thermal conductivity,high glass transition temperature(Tg)and healing capability to glass fiber/epoxy(GFREP)composite,dynamic crosslinked epoxy resin bearing reversibleβ-hydroxyl ester bonds was reinforced with boron nitride nanosheets modified glass fiber cloth(GFC@BNNSs).The in-plane heat conduction paths were constructed by electrostatic self-assembly of polyacrylic acid treated GFC and polyethyleneimine decorated ***,the GFC@BNNSs were impregnated with the mixture of lower concentration(3-glycidyloxypropyl)trimethoxysilane grafted BN micron sheets,3,4-epoxycyclohexylmethyl 3,4-epoxycyclohexanecarboxylate and hexahydro-4-methylphthalic anhydride,which accounted for establishing the through-plane heat transport pathways and avoiding serious deterioration of mechanical *** resultant GFREP composite containing less boron nitride particles(17.6 wt%)exhibited superior in-plane(3.2. W·m^(-1)·K^(-1))and through-plane(1.16 W·m^(-1)·K^(-1))thermal conductivities,as well as high Tg of 2.4℃(Tg of the unfilled epoxy=177℃).The reversible transesterification reaction enabled closure of interlaminar cracks within the composite,achieving decent healing efficiencies estimated by means of tensile strength(71.2.),electrical breakdown strength(83.6%)and thermal conductivity(69.1%).The present work overcame the disadvantages of conventional thermally conductive composites,and provided an efficient approach to prolong the life span of thermally conductive GFREP laminate for high-temperature resistant integrated circuit application.

关键词： Thermally conductive composites Boron nitride High-temperature resistance β-Hydroxyl ester bond Healing

S-(1,3-Dioxoisoindolin-2.yl)O,O-diethyl phosphorothioate (SDDP): A practical electrophilic reagent for the phosphorothiolation of electron-rich compounds

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Chinese Chemical Letters 2024年第5期35卷 151-154页

作者： ze-Yuan Ma Mei Xiao Cheng-Kun Li Adedamola Shoberu Jian-ping Zou Key Laboratory of Organic Synthesis of Jiangsu Province College of Chemistry and Chemical EngineeringSoochow UniversitySuzhou 215123China

An efficient synthesis of the electrophilic reagent,S-(1,3-dioxoisoindolin-2.yl)O,O-diethyl phosphorothioate(SDDP)is ***,the synthetic applications of SDDP wherein the transfer of the SP(O)(OEt)_(2. moiety occurs were *** this manner,SDDP underwent facile SP(O)(OEt)_(2. transfer with electron-rich substrates such as ketones,indoles,and thiols to formα-phosphorothiolated ketones,3-phosphorothiolated indoles and S-phosphorothiolated thioethers,respectively.

关键词： Electrophilic reagent Phosphorothiolation Electrophilic substitution

Statistical properties of ideal photons in a two-dimensional dye-filled spherical cap cavity

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Chinese Physics B 2024年第10期33卷 258-268页

作者： ze Cheng School of Physics Huazhong University of Science and TechnologyWuhan 430074China

Within the framework of quantum statistical mechanics,we have proposed an exact analytical solution to the problemof Bose-Einstein condensation(BEC)of harmonically trapped two-dimensional(2.)ideal *** utilize this analyticalsolution to investigate the statistical properties of ideal photons in a 2. dye-filled spherical cap *** resultsof numerical calculation of the analytical solution agree completely with the foregoing experimental results in the BEC ofharmonically trapped 2. ideal *** analytical expressions of the critical temperature and the condensate fractionare derived in the thermodynamic *** is found that the 2. critical photon number is larger than the one-dimensional(1D)critical photon number by two orders of *** spectral radiance of a 2. spherical cap cavity has a sharppeak at the frequency of the cavity cutoff when the photon number exceeds the critical value determined by a temperature.

关键词： rigorous results in statistical mechanics Bose-Einstein condensation 2. photons

Review of the application of in-situ sensing techniques to address the tea growth characteristics from leaf to field

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International Journal of Agricultural and Biological Engineering 2024年第1期17卷 1-11页

作者： Qiong Cao Chunjiang Zhao ze Xu ping Jiang Haibin Yang Xiangyu Meng Guijun Yang Information Technology Research Center Beijing Academy of Agriculture and Forestry SciencesBeijing 100097China College of Machnical and Electrical Engineering Hunan Agricultural UniversityChangsha 410125China Tea Research Institute of Chongqing Academy of Agricultural Sciences Chongqing 400000China

The tea plant is a valuable and evergreen crop that is extensively cultivated in China and many other ***,there is growing research interest in this *** the tea industry,it is crucial to develop rapid and non-invasive methods to evaluate tea plants in their natural *** article provides a comprehensive overview of non-invasive sensing techniques used for in-situ detection of tea *** topics covered include leaf,canopy,and field-level assessments,as well as statistical analysis techniques and characteristics specific to the ***-invasive testing technology is primarily used for monitoring and predicting tea pests and diseases,monitoring quality,and nutrients,determining tenderness and grade,identifying tea plant varieties,automatically detecting,and identifying tea buds,monitoring tea plant growth,and extracting tea garden areas through remote *** also helps to evaluate planting suitability,assess disasters,and estimate ***,the article examines the challenges and prospects of emerging techniques aimed at resolving the in-situ detection problem for tea *** can assist researchers and producers in comprehensively understanding the tea environment,quality characteristics,and growth process,thereby enhancing tea production quality,and fostering tea industry development.

关键词： non-destructive in-situ detection tea plants growth characteristics sensors

Risk evaluation for diabetic retinopathy in Chinese renalbiopsied type 2.diabetes mellitus patients

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International Journal of Ophthalmology(English edition) 2024年第7期17卷 1283-1291页

作者： Shou-Yue Huang Qi-Wei Hu ze-Wei Zhang ping-Yan Shen Qiong Zhang Department of Ophthalmology Ruijin Hospital Affiliated Medical SchoolShanghai Jiao Tong UniversityShanghai 200025China Department of Nephrology Ruijin Hospital Affiliated Medical SchoolShanghai Jiao Tong UniversityShanghai 200025China

AIM:To investigate diabetic retinopathy(DR)prevalence in Chinese renal-biopsied type 2.diabetes mellitus(T2.M)patients with kidney dysfunction,and to further evaluate its relationship with diabetic nephropathy(DN)incidence and the risk factors for DR development in this ***:A total of 84 renal-biopsied T2.M patients were *** and imaging examinations were employed for DR *** information and clinical measures along with renal histopathology were analyzed for comparisons between the DR and non-DR *** factors on DR development were analyzed with multiple logistic ***:DR prevalence was 50%in *** incidences of DN,non-diabetic renal disease(NDRD)and mixed-type pathology were 47.6%,19.0%and 33.3%in the DR group respectively,while 11.9%,83.3%and 4.8%in the non-DR *** blood pressure,ratio of urinary albumin to creatine ratio,urinary albumin,2.-hours urinary protein,the incidence and severity of DN histopathology were found statistically increased in the DR *** logistic regression analysis showed histopathological DN incidence significantly increased the risk of DR development[odds ratio(OR)=2..664,95%confidential interval(CI)5.588 to 83.991,P2.7.611,P2.M patients inexperienced of regular fundus examinations.

关键词： diabetic retinopathy diabetic nephropathy vision threatens renal biopsy vision screening

Controlling the Si/C ratio in SiC matrix based on the modified polymethysilane for C/C-SiC composites with enhanced mechanical properties

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Journal of Advanced Ceramics 2024年第2期13卷 220-236页

作者： Mingdong Liao Xiebo Hu Chenghao Zhong ping Xu Xiaodong Wang ze Zhang Peng Zhou Mingyu Zhang Zhean Su Qizhong Huang National Key Laboratory of Science and Technology on High-Strength Structural Materials Central South UniversityChangsha 410083China

Fabricating SiC matrix with controllable Si/C ratio for C/C-SiC composites via precursor infiltration and pyrolysis is difficult to realize due to the absence of suitable ***,SiC precursors with Si-rich(Si/C=1.2.),nearstoichiometric(Si/C=1.01),and C-rich(Si/C=0.88)pyrolyzed ceramics at 12.0℃ were successfully synthesized by the novel modification of *** structure and ceramization of synthesized SiC precursors were studied,and C/C-SiC composites with similar Si/C ratio in SiC matrix were also *** results revealed that the defects and Young’s modulus of SiC matrix and the thermal residual stress on pyrolytic carbon coated carbon fiber were determined by the Si/C *** a result,the Si/C ratio exerted significant effects on the crack deflection behavior and the mechanical properties of the *** composites with near-stoichiometric SiC matrix showed excellent mechanical properties because of the effective crack deflection and the moderate Young’s modulus of their SiC *** flexural strength,flexural modulus,and compressive strength were 42.±2. MPa,33.41±4.52.GPa,and 393±8 MPa,***,after a heat treatment at 1600℃,the role of carbon fiber toughening was improved and accompanied by a decrease in mechanical properties for all composites,which was attributed to the increased defects in SiC matrix and the damaged interfaces by the thermal residual stress.

关键词： SiC precursor Si/C ratio polymethysilane C/C–SiC composites mechanical properties

Single-atom Rh catalysts for efficiently degrading Rhodamine B with high concentration

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Rare Metals 2024年第5期43卷 2331-2338页

作者： Shou-Yao Hu Jian-ping Guan Run-ze Ma Yu Tao Dong-Hao Liu Jia-Xin Gong Yu Xiong Department of Chemistry and Chemical Engineering Central South UniversityChangsha 410083China

Highly concentrated dye wastewater has a serious effect on the quality of natural waters;thus,developing novel catalysts to degrade dyes rapidly and efficiently is of great *** the first time,this study reports an Rh single atom loaded on a nitrogen-doped carbon(SA-Rh/CN)*** catalyst exhibits an excellent processing capacity for high concentrations of Rhodamine B(Rh B),high catalytic activity(95.7% degradation of Rh B in60 min)and excellent stability(93.5% degradation efficiency after 10 stable runs).

关键词： catalyst. catalysts loaded

Keplerate polyoxomolybdate nanoball mediated controllable preparation of metal-doped molybdenum disulfide for electrocatalytic hydrogen evolution in acidic and alkaline media

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Chinese Chemical Letters 2024年第7期35卷 524-528页

作者： ping Wang Ting Wang Ming Xu ze Gao Hongyu Li Bowen Li Yuqi Wang Chaoqun Qu Ming Feng Key Laboratory of Functional Materials Physics and Chemistry of the Ministry of Education Jilin Normal UniversityChangchun 130103China School of Science Changchun University of Science and TechnologyChangchun 130022China

Rationally designed novel cost-effective hydrogen evolution reaction(HER)electrocatalysts with controlled surface composition and advanced structural superiority is extremely critical to optimize the HER ***(POMs)with structural diversity and adjustable element compositions represent a promising precursor for rational design and preparation of HER ***,a series of transition metal-doped MoS_(2.materials with different surface engineered structures(Fe,Cr,V doping and S vacancies)(M-MoS_(2./CC,M=Fe,Cr and V)were fabricated by a simple hydrothermalvulcanization strategy using Keplerate polyoxomolybdate nanoball({Mo_(72.Fe_(30)},{Mo_(72.Cr_(30)},{Mo_(72.V_(30)},{Mo_(132.})as *** enlarged interlayer spacing as well as the integration of homogeneous transition metal doping and abundant sulfur vacancies endows prepared M-MoS_(2./CC with superior HER electrocatalytic performance and excellent long-term working stability in both acidic and alkaline *** optimized Fe-MoS_(2./CC afford current densities of 10 and 50 mA/cm^(2.at overpotentials of 188/2.2.mV and 194/394 mV in 0.5 mol/L H_(2.SO_(4)and 1.0 mol/L KOH aqueous solution,respectively,outperforming most of reported typical transition metal sulfide-based *** work represents an important breakthrough for POMs-mediated highly efficient transition metal sulfide-based HER electrocatalysts with wide range pH activity and may provide new options for the rational design of promising HER electrocatalysts and beyond.

关键词： Polyoxometalate Electrocatalytic Hydrogen evolution reaction Doping MoS_(2.

Robustness of the octupole collectivity in 144Ba within the cranking covariant density functional theory in 3D lattice

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Nuclear Science and Techniques 2024年第8期35卷 124-131页

作者： ze‑Kai Li Yuan‑Yuan Wang Mathematics and Physics Department North China Electric Power UniversityBeijing 102206China Hebei Key Laboratory of Physics and Energy Technology North China Electric Power UniversityBaoding 071000China

The octupole deformation and collectivity in octupole double-magic nucleus 144Ba are investigated using the Cranking covariant density functional theory in a three-dimensional lattice *** reduced B(E3)transition probability is implemented for the first time in semiclassical approximation based on the microscopically calculated electric octupole *** available data,including the I-ωrelation and electric transitional probabilities B(E2.and B(E3)are well ***,it is shown that the ground state of 144Ba exhibits axial octupole and quadrupole deformations that persist up to high spins(I≈2.h).

关键词： Octupole collectivity Cranking covariant density functional theory Rotational spectrum Electric transitional probabilities