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Understand the Temperature Sensing Behavior of Solid-state Polymerized PEDOT Hybrid Based on X-ray Scattering Studies

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Chinese Journal of Polymer Science 2024年第1期42卷 105-112,I0010页

作者： Zhen-Hang He Guang-Feng Liu ze-Kun Zhou Zhen Liu Yi-Shu zeng Peng Zhang School of Materials Science and Engineering Key Laboratory for Polymeric Composite and Functional Materials of Ministry of EducationSun Yat-sen UniversityGuangzhou 510275China Shanghai Advanced Research Institute(Zhangjiang Laboratory) Chinese Academy of SciencesShanghai 201204China

Poly(3,4-ethylenedioxythiophene)(PEDOT) is one of the most successful conductive polymers that recently has been used in wearable sensors for human health monitoring. In this work, we prepared a series of PEDOT hybrids consisting of PEDOT, sodium poly(styrene sulfonate)(PSSNa) and polyethylene oxide(PEO), and their preparation could be scaled-up via an adapted solid-state polymerization process. The resistance of the as-prepared PEDOT:PSS/PEO hybrid shows clear temperature response, i.e., it decreases almost linearly with the temperature increase. To understand this phenomenon, the in situ synchrotron radiation wide-and small-angle X-ray scattering(WAXS/SAXS) characterizations were undertaken to study the temperature-dependent microstructure change of the PEDOT:PSS/PEO hybrid. It demonstrated that PEDOT formed conductive paths in the hybrids, which were not destroyed by the PEO crystallization. As temperature increased, the PEO crystals' melting and the accompanying reorganization of PEDOT chains endowed the hybrid sample temperature responsiveness. Based on these fundamental knowledges, the hybrid materials were used to fabricate flexible wearable sensor that showing temperature sensing performance with an accuracy of 1 ℃. These findings shed lights on the scalable manufacturing of wearable sensors for body temperature monitoring.

关键词： Solid-state polymerization PEDOT hybrid Structure-property correlation X-ray scattering

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On the Innovation,Design,Construction,and Experiments of OMEGA-Based SSPS Prototype:The Sun-Chasing Project

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Engineering 2024年第5期36卷 90-101页

作者： Baoyan Duan Yiqun Zhang Guangda Chen ze Zhao Jianwei Mi Xun Li Lin Yang Xi Li Research Institute on Mechatronics Xidian UniversityXi’an 710071China Research Institute of Antenna Xidian UniversityXi’an 710071China

This study systematically introduces the development of the world’s first full-link and full-system ground demonstration and verification system for the OMEGA space solar power satellite(SSPS).First,the OMEGA 2.0 innovation design was ***,field-coupling theoretical models of sunlight concentration,photoelectric conversion,and transmitting antennas were established,and a systematic optimization design method was ***,a beam waveform optimization methodology considering both a high beam collection efficiency and a circular stepped beam shape was ***,a control strategy was developed to control the condenser pointing toward the sun while maintaining the transmitting antenna toward the ***,a high-efficiency heat radiator design method based on bionics and topology optimization was ***,a method for improving the rectenna array’s reception,rectification,and direct current(DC)power synthesis efficiencies is ***,high-precision measurement technology for high-accuracy beam-pointing control was ***,a smart mechanical structure was designed and ***,the developed SSPS ground demonstration and verification system has the capacity for sun tracking,a high concentration ratio,photoelectric conversion,microwave conversion and emission,microwave reception,and rectification,and thus satisfactory results were obtained.

关键词： OMEGA-SSPS Full-link and full-system Beam collection efficiency Circular stepped beam shape Smart structure Field coupling theoretical model `Beam pointing control

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Leveraging the Empirical Wavelet Transform in Combination with Convolutional LSTM Neural Networks to Enhance the Accuracy of Polar Motion Prediction

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Research in Astronomy and Astrophysics 2024年第9期24卷 214-224页

作者： Xu-Qiao Wang Lan Du Zhong-Kai Zhang ze-Jun Liu Hao Xiang College of Geospatial Information Information Engineering UniversityZhengzhou 450001China Henan Industrial Technology Academy of Spatio-Temporal Big Data Zhengzhou 450046China

High-precision polar motion prediction is of great significance for deep space exploration and satellite *** motion is affected by a variety of excitation factors,and nonlinear prediction methods are more suitable for polar motion *** order to explore the effect of deep learning in polar motion *** paper proposes a combined model based on empirical wavelet transform(EWT),Convolutional Neural Networks(CNN)and Long Short Term Memory(LSTM).By training and forecasting EOP 20C04 data,the effectiveness of the algorithm is verified,and the performance of two forecasting strategies in deep learning for polar motion prediction is *** results indicate that recursive multi-step prediction performs better than direct multi-step prediction for short-term forecasts within 15 days,while direct multi-step prediction is more suitable for medium and long-term *** the 365 days forecast,the mean absolute error of EWT-CNN-LSTM in the X direction and Y direction is 18.25 mas and 15.78 mas,respectively,which is 23.5% and 16.2% higher than the accuracy of Bulletin *** results show that the algorithm has a good effect in medium and long term polar motion prediction.

关键词： data analysis methods:miscellaneous astrometry reference systems Earth

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Learning to bag with a simulation‐free reinforcement learning framework for robots

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IET Cyber-Systems and Robotics 2024年第2期6卷 52-66页

作者： Francisco Munguia-Galeano Jihong Zhu Juan David Hernández ze Ji Cooper Group University of LiverpoolLiverpoolUK School of Physics Engineering and Technology University of YorkYorkUK School of Computer Science and Informatics Cardiff UniversityCardiffUK School of Engineering Cardiff UniversityCardiffUK

Bagging is an essential skill that humans perform in their daily ***,deformable objects,such as bags,are complex for robots to manipulate.A learning-based framework that enables robots to learn bagging is *** novelty of this framework is its ability to learn and perform bagging without relying on *** learning process is accomplished through a reinforcement learning(RL)algorithm introduced and designed to find the best grasping points of the bag based on a set of compact state *** framework utilises a set of primitive actions and represents the task in five *** our experiments,the framework reached 60% and 80% success rates after around 3 h of training in the real world when starting the bagging task from folded and unfolded states,***,the authors test the trained RL model with eight more bags of different sizes to evaluate its generalisability.

关键词： reinforcement learning robot learning robotics

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S-(1,3-Dioxoisoindolin-2-yl)O,O-diethyl phosphorothioate (SDDP): A practical electrophilic reagent for the phosphorothiolation of electron-rich compounds

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Chinese Chemical Letters 2024年第5期35卷 151-154页

作者： ze-Yuan Ma Mei Xiao Cheng-Kun Li Adedamola Shoberu Jian-Ping Zou Key Laboratory of Organic Synthesis of Jiangsu Province College of Chemistry and Chemical EngineeringSoochow UniversitySuzhou 215123China

An efficient synthesis of the electrophilic reagent,S-(1,3-dioxoisoindolin-2-yl)O,O-diethyl phosphorothioate(SDDP)is ***,the synthetic applications of SDDP wherein the transfer of the SP(O)(OEt)_(2) moiety occurs were *** this manner,SDDP underwent facile SP(O)(OEt)_(2) transfer with electron-rich substrates such as ketones,indoles,and thiols to formα-phosphorothiolated ketones,3-phosphorothiolated indoles and S-phosphorothiolated thioethers,respectively.

关键词： Electrophilic reagent Phosphorothiolation Electrophilic substitution

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Comparative study on interaction between rare earth oxide refractories and rare earth treated steel

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Journal of Iron and Steel Research International 2024年第6期31卷 1493-1501页

作者： ze Meng Guang-qiang Li Cheng Yuan Yi-jiang Zhao Qing Zheng Bin zeng Yu Liu The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan430081HubeiChina Key Laboratory for Ferrous Metallurgy and Resources Utilization of Ministry of Education Wuhan University of Science and TechnologyWuhan430081HubeiChina Hubei Provincial Key Laboratory for New Processes of Ironmaking and Steelmaking Wuhan University of Science and TechnologyWuhan430081HubeiChina Technical Center Lianyuan Iron and Steel Co.Ltd.Loudi417009HunanChina

Refractories have an important effect on the cleanliness of molten *** interaction between CeAlO_(3) refractories and Ce treated steel was explored and compared with that between Al_(2)O_(3) refractories and Ce treated *** results show that the Ce content in steel decreases sharply after contact with Al_(2)O_(3) refractories and the pick-up of dissolved Al *** with the test of Al_(2)O_(3) refractories,the loss of Ce content is less in the test of CeAlO_(3) refractory,and the total oxygen content and dissolved Al content in steel increase *** dense and continuous Ce_(2)O_(2)S interface layer is observed at the CeAlO_(3) refractories/steel interface,which can serve as the metallurgical isolation layer and hinder the further interaction between refractories and ***,the higher steel cleanliness and less penetration of refractories by molten steel are obtained in the test of CeAlO_(3) *** CeAlO_(3) refractories show a promising prospect in the production of clean Ce treated steel.

关键词： CeAlO_(3)refractory Steel Cleanliness Interaction Rare earth

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Uniform lithium deposition induced by copper phthalocyanine additive for durable lithium anode in lithium-sulfur batteries

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Chinese Chemical Letters 2024年第5期35卷 447-452页

作者： Ting Hu Yuxuan Guo Yixuan Meng ze Zhang Ji Yu Jianxin Cai Zhenyu Yang Key Laboratory of Jiangxi Province for Environment and Energy Catalysis School of Chemistry and Chemical EngineeringNanchang UniversityNanchang 330031China

Copper phthalocyanine(CuPc)is adopted as an electrolyte additive to stabilize lithium anode for lithiumsulfur(Li-S)*** with a planar molecular structure and lithiophilic N-containing group,is likely to be adsorbed on the surface of Li anode to form a coating layer,which can restrict the direct contact between Li anode and solvents,and guide the uniform deposition of Li^(+)*** Li||Li symmetric cells demonstrate a stable cycle performance,and Li||Cu cells show high Coulombic *** Li-S batteries,the formed stable solid-electrolyte interface(SEI)film containing copper sulfides can protect Li anode from the polysulfide corrosion and side reactions with the electrolyte,leading to the compact and smooth surface morphology of Li ***,the Li-S batteries with CuPc additive deliver much higher capacity,better cycle performance and rate capability as compared to the one without CuPc additive.

关键词： Copper phthalocyanine Electrolyte additive Stable SEI film Stabilized Li anode Lithium-sulfur batteries

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Application of a concrete thermal pile in cooling the warming permafrost under climate change

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Advances in Climate Change Research 2024年第1期15卷 170-183页

作者： Yun-Hu SHANG Fu-Jun NIU Guo-Yu LI Jian-Hong FANG ze-Yong GAO State Key Laboratory of Frozen Soil Engineering Northwest Institute of Eco-Environment and ResourcesChinese Academy of SciencesLanzhou 730000China Da Xing'anling Observation and Research Station of Frozen-Ground Engineering and Environment Northwest Institute of Eco-Environment and ResourcesChinese Academy of SciencesJagdaqi 165000China Qinghai Research Institute of Transportation Xining 810008China

Permafrost degradation caused by climate warming is posing a serious threat to the stability of cast-in-place pile foundations in warm permafrost *** cold energy can be effectively utilized by two-phase closed thermosyphons(TPCTs)to cool the ***,we installed TPCTs in a cast-in-place pile foundation to create a unique structure called a thermal pile,which effectively utilizes the TPCTs to regulate ground *** we conducted a case study and numerical simulation to exhibit the cooling performance,and optimize the structure of the thermal *** purpose of this study is to promote the application of thermal piles in unstable permafrost *** on the findings,the thermal pile operated for approximately 53%of the entire year and effectively reduced the deep ground temperature at a rate of at least-0.1℃per ***,it successfully raised the permafrost table that is 0.35 m shallower than the natural ground *** characteristics prove highly beneficial in mitigating the adverse effects of permafrost degradation and enhancing infrastructure *** the length of the condenser section and the diameter of the TPCT in a suitable manner can effectively enhance the cooling capability of the thermal pile and ensure the long-term mechanical stability of the pile foundation even under climate warming.

关键词： Heat transfer Cold energy Warm permafrost Two-phase closed thermosyphons Cast-in-place pile foundation

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Comment on“Robotic surgery and liver transplantation:A single-center experience of 501 robotic donor hepatectomies”

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Hepatobiliary & Pancreatic Diseases International 2024年第1期23卷 109-110页

作者： Xiang-Yan Liu Yun-Yang Xu ze Xiang Shu-Sen Zheng Shulan(Hangzhou)Hospital Affiliated to Zhejiang Shuren University Shulan International Medical College Hangzhou 310015China Zhejiang University School of Medicine Hangzhou 310009China

To the Editor:We read with great interest the article by Schulze et ***“Robotic surgery and liver transplantation:A single-center experience of 501 robotic donor hepatectomies”[1].It is the first single-center report including over 500 fully robotic donor *** the donors,the overall complication rate was 6.4%(n=32).Postoperative self-limiting bleeding(0.4%)and bile leakage from the resection plane(1.8%)were rare.

关键词： robotic Robotic center

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Effect of nucleating agents on the electrical properties of cross-linked polyethylene under tensile stress

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High Voltage 2024年第2期9卷 429-439页

作者： Yunqi Xing Jiahao Liu Jingang Su Junwei Zha Guochang Li ze Guo Xiaozhen Zhao Mengjia Feng State Key Laboratory of Reliability and Intelligence of Electrical Equipment Hebei University of TechnologyTianjinChina Electric Power Research Institute of State Grid Hebei Electric Power Supply Co. Ltd.ShijiazhuangChina Beijing Advanced Innovation Center for Materials Genome Engineering School of Chemistry and Biological EngineeringUniversity of Science&Technology BeijingBeijingChina Institute of Advanced Electrical Materials Qingdao University of Science and TechnologyQingdaoChina

During the operation of high-voltage cables,external stress and residual stress can affect the aggregated structure of insulating materials and lead to significant deterioration in their electrical *** investigate the evolution characteristics of the electrical properties of cross-linked polyethylene(XLPE)under mechanical stress,this paper ex-plains the relationship between the aggregated structure of XLPE and its electrical properties and proposes a method for improving insulation performance under me-chanical *** results show that metallocene polyethylene used as a nucleating agent can promote crystallisation through heterogeneous nucleation and increase Young's modulus by non-uniform nucleation,increasing crystallinity and reducing interplanar spacing,resulting in more complete crystal forms and reduced damage to the aggregated structure during the tensile *** nucleating agent modification,the XLPE crystallisation becomes more uniform,and interfacial adhesion forces *** weakened interface damage process between the amorphous and crystalline regions under tensile stress effectively inhibits the process of molecular chain polarisation turning and reduces trap *** modified XLPE crystal structure shows a tendency towards densification and enhanced molecular chain interactions,which can reduce the damage to the aggregated structure under tensile stress,while the reduced free volume inside the material and the shortened average free path of carriers can weaken the damage of high-energy electrons to molecular chains,thereby inhibiting the process of electrical tree *** results show that nucleating agents have great potential for maintaining the stable operation of XLPE cables under mechanical stress.

关键词： stress electrical damage

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