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Analytical method of Cr stable isotope and its application to water pollution survey

Chinese Science Bulletin 2010年第7期55卷 664-669页

作者： GAO YongJuan 1,2,3,MA Teng 4,5,LING WenLi 1,2,LIU CunFu 4,5 & LI Li 4,5 1faculty of earth Science,china university of geosciences,wuhan 430074,china 2State Key Laboratory of Geological Processes and Mineral Resources,china university of geosciences,wuhan 430074,china 3 Graduate School,china university of geosciences,wuhan 430074,china 4 Biogeological and Environmental Geology Laboratory of Ministry of Education(china university of geosciences) ,wuhan 430074,china 5 Sino-Hungary Joint Laboratory of Environmental sciences and health,china university of geosciences,wuhan 430074,china faculty of earth Science China University of Geosciences Wuhan China State Key Laboratory of Geological Processes and Mineral Resources China University of Geosciences Wuhan China Graduate School China University of Geosciences Wuhan China Biogeological and Environmental Geology Laboratory of Ministry of Education (china university of geosciences) Wuhan China Sino-Hungary Joint Laboratory of Environmental sciences and health China University of Geosciences Wuhan China

High Cr(VI) concentration is a potential serious risk to environment and ecologic ***,it is essential to effectively monitor Cr contamination in water systems and scientifically evaluate its evolution trend.A new method of in-situ tracer technique by Cr isotopic analysis for quantitatively estimating Cr-contamination and its regional evolution in natural waters as well as a case application are reported in this *** on documented literatures,an experimental procedure for chemical separation and purification of Cr in water samples and its analytical method for Cr isotopic measurement by thermal ionization mass spectrometry(TIMS) are *** samples collected around a chemical factory in Hubei Province were analyzed by this *** samples showδ53Cr values ranging from-1.7‰to 7.3‰and an elevating trend with an increasing in distance from the sampling site to pollution source.A functional correlation following Rayleigh fractionation law was established between sample'sδ53Cr value and its extent of Cr *** study suggests that Cr isotopic analysis is an effective method to reveal the spatial distribution and its evolution trend of Cr contamination in the regional water *** is thus helpful to assessing the self-purifying ability of local water system according to Cr isotopic fractionation.

关键词：铬(VI) 水污染调查稳定同位素应用同位素分析供水系统演变趋势示踪技术

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The Upper Devonian orbital cyclostratigraphy and numerical dating conodont zones from Guangxi,South china

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Science china earth sciences 2005年第1期48卷 32-41页

作者： GONG Yiming, XU Ran, TANG Zhongdao & LI Baohua faculty of earth Science, china university of geosciences, wuhan 430074, china Laboratory of Marine Geology, Tongji university, Shanghai 200092, china faculty of earth Science China University of Geosciences Wuhan China Laboratory of Marine Geology Tongji University Shanghai China

The hierarchically organized laminae, bundles, bundlesets and superbundlesets which correspond to a sub-Milankovitch, obliquity or precession, eccentricity and long eccentricity cyclothems, respectively, have been distinguished from the Upper Devonian Fras-nian-Famennian (F-F) transitional carbonate successions deposited in the carbonate-basin and slope facies of Guangxi, South china. The durations of cyclothems are 8000-10000a, 16667a or 33333a, 100000a and 400000a, respectively. The ratio of eccentricity to precession, eccentricity to obliquity, and long eccentricity to eccentricity is 1 : 6, 1 : 3 and 1 : 4 in the Devonian, respectively. Orbital cyclostratigraphical studies show that the durations of the conodont falsio-valis Zone, transitans Zone, punctate Zone, Lower hassi Zone, Upper hassi Zone, jamieae Zone, Lower rhenana Zone, Upper rhenana Zone, linguiformis Zone, Lower triangularis Zone, Middle triangularis Zone and Upper triangularis Zone are 0.4, 0.4, 0.4, 0.3, 0.4, 0.2, 0.8, 0.6, 0.8, 0.3, 0.3 and 0.3 Ma from bottom to top, respectively, and the duration of the Frasnian is 4.3 Ma. The conodont is the normal marine organism of the latest mass extinction (the latest linguiformis Zone) and the first recovery (including the whole Lower triangularis and Middle triangularis Zone) in the F-F transition. The conodont mass extinction and recovery lasted 200000-100000a and 0.6 Ma, respectively. We consider that average durations of the fossil zones calculated by reported numerical ages divided by fossil zone numbers within a stage or series or system cannot discovery complications and non-uniformity of evolutionary organisms and environments.

关键词： orbital cyclostratigraphy, conodont zone, numerical dating, mass extinction, Devonian, Guangxi, South china.

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A High Precision Forecasting Model and Its Constructing Method for Vein Type Gold Deposits

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Journal of china university of geosciences 2001年第2期12卷 100-107页

作者： zhang Jun faculty of earth Resources, china university of geosciences, wuhan 430074 faculty of earth Resources China University of Geosciences

A high precision forecasting and prospecting model incorporating the “field theory field structure analysis field simulation”, a temporal and spatial structural framework reflecting local extremely fine structures, is established to make an effective extraction and an integrated analysis of multivariate forecasting information. This model can best show not only the coupling between metallogenic anomalous structure, mineralized structure and information structure, but also the extraction, optimization, matching and summarization of key forecasting information. The technological keys to this model are the fine structural analysis of geological and geophysical and geochemical anomalous fields and metallogenic fields, and the establishment of occurrence patterns for the spatial location of orebodies.

关键词： high precision forecasting model anomalous structure mineralized structure orebody location.

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Zircon geochronology and geochemistry of mafic xenoliths from Liaoning kimberlites:Track the early evolution of the lower crust,North china Craton

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Science china earth sciences 2004年第11期47卷 961-972页

作者： ZheNG Jianping1,YU Chunmei1,LU Fengxiang1 & LI Huimin2.1.faculty of earth sciences,china university of geosciences,wuhan 430074,china 2.Tianjin Institute of Geology and Mineral Resources,Tianjin 300170,china faculty of earth sciences China University of Geosciences Wuhan China Tianjin Institute of Geology and Mineral Resources Tianjin China

Mafic xenoliths from Paleozoic Fuxian kimberlites (Liaoning Province) mainly in- clude garnet granulite, with minor pyroxene amphibolite, meta-gabbro and pyroxene syenite. The SiO2 contents of the xenoliths are from 47.3 wt% to 49.9 wt%. The granulites are mainly coarse-medium grained and reasonably with well-developed granoblastic (mostly polygonal) texture, contain the assemblage of garnet + plagioclase + pyroxene + K-feldspar ±phlogopite. The mineral assemblage of the amphibolites is plagioclase + pyroxene + amphibole ±K-feldspar, with the equilibrium temperature and pressure conditions of 744—821℃ and 0.76—0.88 GPa. The granulites are regarded as derivation from the lower crust depth (more than 29 km), below the amphibolites. Garnet granulites compositionally correspond to sub-alkalic basalt, and have wide ranges of Ni abundance (133—840 ppm), and Nb/Y (0.12.1.85), Nb/U (3.51—53.86) and Ta/U (0.38—2.48). The amphibolite and the syenite correspond to alkalic basalt. The Fuxian ma- fic xenoliths are regarded as the metamorphic product of the underplated magmas (including fractional crystallization or not) experienced the contamination with the pre-existed crustal com- ponents, and partly effected by kimberlitic magmas. The concordant ages of zircons for the gab- bro (2.10—2580 Ma) and the near-concordant upper intercept ages of zircons for the garnet granulite and pyroxene amphibolite (2578—2538 Ma) indicate that they are currently known as the oldest deep-seated xenoliths from the lower crust of the North china Craton. These ages recorded the formation of the united Eastern Block of the North china Craton, That is, Neoar- chean (2.6—2.5 Ga) is an important continental crustal growth period of the North china Craton. The lower intercept age of the garnet granulite (1853 Ma) recorded an important tectonic thermal event in Paleoproterozoic. This event was probably related to collision of the East and West block, and resulted in the final assembly of the North china

关键词： mafic xenolith, petrochemistry, zircon geochronology, petrogenesis, lower crustal evolution, North china Craton.

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New stylophorans(Echinodermata) from the Upper Cambrian of Guangxi,South china

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Science china earth sciences 2008年第2期51卷 181-186页

作者： HAN NaiRen1 & CheN GuiYing1,2.1 Department of Resources and Environmental Engineering, Guilin university of Technology, Gulin 541004, china 2 faculty of earth sciences, china university of Geoscience, wuhan 430074, china Department of Resources and Environmental Engineering Guilin University of Technology Gulin China faculty of earth sciences China University of Geoscience Wuhan China

This paper describes for the first time the cornute stylophorans (Echinodermata) in china. The new material came from the Guole Formation of the Furongian (Late Cambrian) in the Guole area of Jingxi, Guangxi Province, South china. These new cornute specimens are preserved in situ and found along with well-preserved trilobites and brachiopods. One new species, Phyllocystis jingxiensis sp. nov., is proposed to accommodate these unusual materials. The new species is defined by the small, heart-shaped theca with the frame composed of ten narrow, smooth and thick marginal plates, three adoral plates and distinctive zygal and aulacophore. Both supracentrals and infracentrals are polygonal-outlined. The marginal plate M1' on the inferior face extends posteriorly to form zygal that possesses a broadened proximal end and the proximal portion joining with the conjunction between M4 and M5 on the inferior face. Aulacophore comprises ten segments at its proximal part and is conical at the middle part (named stylocone). Its distal portion is rather long and bears conspicuous ambulacrum grooves. Tectals are horizontally arranged on superior face and obliquely arranged on inferior face. Both cothurnopore and anal pyramid are vaguely seen on the right anterior corner and the extremity of theca's superior face.

关键词： Phyllocystis Stylophora Echinodermata Cambrian Guangxi South china

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^(40)Ar-^(39)Ar and U-Pb ages of metadiorite from the East Kunlun Orogenic Belt: Evidence for Early-Paleozoic magmatic zone and excess argon in amphibole minerals

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Chinese Science Bulletin 2001年第4期46卷 330-333页

作者： CheN Nengsong, SUN Min, zhang Kexin & ZHU Yunhaifaculty of earth sciences, china university of geosciences, wuhan 430074, china Department of earth sciences, The university of Hong Kong, Hong Kong SAR, china faculty of earth sciences China University of Geosciences Wuhan China Department of earth sciences The University of Hong Kong Hong Kong SAR China

Single-grain zircon U-Pb and amphibole 40Ar-39Ar dating have been conducted on a deformed and metamorphosed diorite in the East Kunlun Orogenic Belt, which intruded into the middle Proterozoic Kuhai Group exposed in the south of Xiangride region, Dulan County, NW Qinghai Province. The zircon gives a concordant U-Pb age of (446.5±9.1) Ma. The amphibole yields Ar plateau age of (488.0±1.2) Ma and an isochronal age of (488.9±5.6) Ma. Age results of both stepwise released Ar and conventional K-Ar analysis are remarkably higher than that of zircon U-Pb, suggesting that the amphibole contains excess argon and the amphibole plateau age cannot be taken as the timing of metamorphism or deformation. The zircon age is interpreted to be crystallization age of the diorite pluton, which suggests that an Early-Paleozoic magmatic zone indeed existed in the East Kunlun Orogenic Belt stretching along the region south to the Golmud, Normuhong and Xiangride.

关键词： East Kunlun Orogenic Belt metadiorite geochronology excess argon.

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Mass and Energy Transportation in Ore-Forming Processes of Sulfide Deposits in Tongling District

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Journal of earth Science 1999年第4期18卷 299-304页

作者： Cen Kuang Yu Chongwen(faculty of earth sciences, china university of geosciences, wuhan 430074) faculty of earth sciences China University of GeosciencesWuhan 430074

Based on dynamics of heat conduction, fluid flow caused by heating and chemical material transport induced by fluid flow, temperature and stream fields of fluid flow in ore-forming processes of Cu-Au sulfide in the Tongling district deposits was modeled and analyzed. It is shown that: (1) Mass and energy flow caused by fluid flow is key problem of kythrothermal ore-forming processes; the heating from magma intruded is basic power for driving fluid flow. (2) occurrence of pluton, different chemical property and porosity of wall rocks and infiltration restrict the specifically field of precipitation for ore-forming ***, the dissolution and precipitation field for ore-forming material in deposit can be forecasted. (3) Iron and sulfur material comes mostly from sandstone formation of Wutong Group, which contains pyrite and high porosity. The cataclastic dolomite interlayered in sandstone and limestone is a favorable place for ore accumulating. The difference of chemical property between sandstone and dolomite forms a favorable interface for ore-forming processes.

关键词： heat conduction mass transportation fluid path-line streamline

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Principle and Technique of Calculating Seismic Velocities from Lattice Preferred Orientation (LPO) Data of Minerals

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Journal of earth Science 1998年第2期17卷 60-66页

作者： Guan Xiaoping Department of Applied Geophysics, china university of geosciences, wuhan 430074 Jin Shuyan faculty of earth sciences, china university of geosciences, wuhan 430074

Deducing seismic velocity anisotropy from LPO (lattice preferred orientation) data of deformed rock samples, a significant link between geology and seismology in geoscience researches, has extensive and promising application. In this paper, the principle and programming technique are highlighted to illustrate the comprehensive automatization procedure. In computer algorithm, two aspects of the programs commonly used in the world are improved: (1) the addition of a pre processing subroutine makes the straightforward calculation realizable from universal stage readings to geographic azimuths and thus to solution of all crystal axes, even for non orthorhombic a and c axes in monoclinic systems. (2) the simplification and perfection of programming can be implemented in the light of Visual Basic (VB) resource. The algorithm has been verified with results from practical data of omphacite samples.

关键词： omphacite fabric seismic velocity anisotropy contouring.

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Indian Ocean-MORB-type isotopic signature of Yushigou ophiolite in North Qilian Mountains and its implications

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Science china earth sciences 2006年第6期49卷 561-572页

作者： HOU Qingye1,2, ZHAO Zhidan1,2, zhang Hongfei3, zhang Benren3 & CheN Yuelong2.1. State Key Laboratory of Geological Processes and Mineral Resources, china university of geosciences, Beijing 100083, china 2. School of earth Science and Mineral Resources, china university of geosciences, Beijing 100083, china 3. faculty of earth sciences, china university of geosciences, wuhan 430074, china State Key Laboratory of Geological Processes and Mineral Resources China University of Geosciences Beijing China School of earth Science and Mineral Resources China University of Geosciences Beijing China faculty of earth sciences China University of Geosciences Wuhan China

In order to explore the disputed issue concerning the tectonic affinity ofthe ancient ocean mantle of North Qilian Mountains (NQM), geochemical and Sr, Nd, Pb isotopiccompositions of pillow basalts of the Yushigou Ophiolite (YSGO) suite from NQM have been analyzedsystematically. The pillow basalts exhibit tholeiitic characteristics, with flatchondrite-normalized REE patterns ((La/Yb)_N = 0.98—1.27). They display no Nb, Ta, Zr, Hf negativeanomalies, and show MORB features in 2Nb-Zr/4-Y and Ti/100-Zr-YX3 tectonic discrimination *** results indicate that the Yushigou ophiolite is most likely to be formed in a mid-ocean ridgeor mature back-arc basin. Their isotopic data show a relatively broad and enriched ^(87)Sr/^(86)Sr(0.70509 — 0.70700), restricted ^(143)Nd/^(144)Nd (0.512955-0.512978). Pb isotopes are in the rangeof ^(206)Pb/^(204)Pb (18.054-20.562), ^(207)Pb/^(204)Pb (15.537-15.743) and ^(208)Pb/^(204)Pb(38.068-38.530). These isotopic data imply that the basalts originated from the depleted mantle(DMM), with the involvement of enriched mantle components (mainly EMII). Geochemical comparisonsbetween the basalts in YSGO and the MORB-type basalts of ophiolite suites occurring in the knownancient Tethyan tectonic domain indicate that the ancient oceanic mantle represented by YSGO suiteforming in early Paleozoic in the North Qilian Moutains is very similar to the Tethyan mantle inboth trace elements and isotopic compositions. The North Qilian Mountains should be a part of theTethyan tectonic domain in early Paleozoic. This further implies that the Tethyan tectonic domaincan be deduced to early Paleozoic in the study area, which will be helpful to discussing thetectonic affinity and evolution of the North Qilian Mountains.

关键词： geochemistry, Indian Ocean-MORB-type isotopic signatures, Tethyan tectonic domain, Yushigou ophiolite, North Qilian Mountains.

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earthquake-controlled event deposits and its tectonic significance from the Middle Permian Wandrawandian Siltstone in the Sydney Basin, Australia

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Science china earth sciences 2005年第9期48卷 1337-1346页

作者： DU Yuansheng1, G. R. Shi1,2 & GONG Yiming1 1. faculty of earth sciences, china university of geosciences, wuhan 430074, china 2. School of Ecology and Environment, Deakin university, Victoria 3125, Australia faculty of earth sciences China University of Geosciences Wuhan China School of Ecology and Environment Deakin University Victoria Australia

The Sydney-Bowen basin in eastern Australia is an elongate back arc-converted foreland basin system situated between the Lachlan Fold Belt in the west and the New England Fold Belt in the east. The Middle Permian Wandrawandian Siltstone at Warden head near Ulla- dulla in the southern Sydney Basin is dominated by fossiliferous siltstone and mudstone, with a large amount of dropstones and minor pebbly sandstone beds. Two general types of deposits are recognized from the siltstone unit in view of the timing and mechanism of formation. One is rep- resented by the primary deposits from offshore to subtidal environments with abundant drop- stones of glacial marine origin. The second type is distinguished by secondary, soft-sediment deformational deposits and structures, and comprises three layers of mudstone dykes of seismic origin. In the latter type, metre scale, laterally extensive syn-depositional slump deformation structures occur in the middle part of the Wandrawandian Siltstone. The deformation structures vary in morphology and pattern, including large-scale complex-type folds, flexural stratification, concave-up structures, faulting of small displacements accompanied by folding and brecciation. The slumps and associated syn-sedimentary structures are attributed to penecontemporaneous deformations of soft sediments (mostly silty mud) formed as a result of mass movement of un- consolidated and/or semi-consolidated substrate following an earthquake event. The occurrence of the earthquake event deposits supports the current view that the Sydney Basin was located in a back-arc setting near the New England magmatic arc on an active continental margin during the Middle Permian.

关键词： Permian, seismites, earthquake, tectonics, Sydney Basin, Australia.

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