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Fabrication of Humidity Sensors Based on Laser Scribed Graphene Oxide/SnO Composite Layers

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Chinese Journal of Structural Chemistry 2020年第11期39卷 1949-1957页

作者： LI xin FENG Wen-Dou zhang xiang-xin WANG Wei CHEN Su-Jing zhang Yi-Ning College of Chemistry and Materials Science Fujian Normal UniversityFuzhou 350007China Key Laboratory of Optoelectronic Materials Chemistry and Physics Fujian Institute of Research on the Structure of MatterChinese Academy of SciencesFuzhou 350002China

Humidity sensors have been widely applied to detect environment humidity in various fields. However, most of humidity sensors cannot provide performance needed for high sensitivity and fast response. We report one type of capacitive-type humidity sensors composed of laser-scribed graphene(LSG) as sensing electrodes and graphene oxide/tin dioxide(GO/SnO2) as a sensing layer. The LSG is reduced graphene oxide(rGO) electrodes resulted from selective reducing of GO within a GO/SnO2 composite layer by laser scribing method, and the sensing layer is the un-scribed GO/SnO2 composite. The sensor fabrication is a one-step process which is facile and cost-efficient. When a mass ratio of GO:SnO2 in the composite reaches 1:1, the humidity sensor(named as LSG-GS1) has the best properties than other ratios, which exhibits high sensitivity in the range of 11%~97% relative humidity(RH). In addition, the LSG-GS1 also has very quick response/recovery time(20 s for adsorption and 18 s for desorption) when RH changes from 23% to 84%, and very good stability after monitoring for 41 days. Such excellent performances of the humidity sensor can be attributed to synergistic effect of SnO2 and GO within the composite layer.

关键词： humidity sensor tin dioxide graphene laser scribed

Preparation of β-Cyclodextrin Modified FusedSilica Capillary and Its Application inCapillary Electrophoresis Enantiom eric Separation

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Chemical Research in Chinese Universities 1999年第3期15卷 232-237页

作者： zhang xin-xiang HONG Feng BAI Jing CHANG Wen-bao CI Yun-xiang College of Chemistry Peking UniversityBeijing 100871P.R.China

A simple type of chiral selector immobilized capillaries was prepared and applied to the separation of some enantiomers by capillary electrophoresis(CE) without chiral selective reagents in a buffer solution. β Cyclodextrin (CD) was bonded to the inner wall of fused silica capillary with the aid of 3 (2 cyclooxypropoxyl) propyl trimethoxy silane or 3 aminopropyltriethoxyl silane as bridge. The synthesis conditions such as reaction temperature, reaction ratios, solvents were optimized. The stability and reproducibility of the CD modified capillaries were studied under different operation conditions. It is satisfactory to apply the capillary to the chiral separation of d,l adrenaline and the atracurium besilate diastereoisomers under the optimized conditions.

关键词： U-cyclodextrin-immobilized capillary Capillary electrophoresis Enantiomeric separation

Determination　of　Trace　Amounts　of　Cobalt　and　Copper　by　High　Performance　Liquid　Chromatography　with　Indigo　Carmine　Chemiluminescence　Detection

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Chemical Research in Chinese Universities 1996年第4期12卷 348-353页

作者： zhang xin-xiang CHENG Jie-ke and ZENG Yun-e(Department of Chemistry,Wuhan University,Wuhan,430072) WUHAN UNIV DEPT CHEMWUHAN 430072PEOPLES R CHINA

A post-column reaction chemiluminescence detection method in ion chromatography is described in this *** chemiluminescence system was indigo cramine-hydrogen peroxide. The chemiluminescence reaction conditions and the separation conditions of Co and Cu in chromatography were *** detection limits were 1.0 and 2.0×10-8 g/mL for Co and Cu respectively.

关键词： s:Chemiluminescehce detection HPLC Cobalt Copper Indigo Carmine

Sandwich structures with tapered tubes as core:A quasi-static investigation

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Defence Technology（防务技术） 2024年第3期33卷 447-462页

作者： xinmei xiang Dehua Shao xin zhang Umer Sharif Ngoc San Ha Li xiang Jing zhang Jiang Yi School of Civil Engineering Guangzhou UniversityGuangzhouChina Department of Mechanics and Aerospace Engineering Southern University of Science and TechnologyShenzhenGuangdongChina School of Engineering Centre for Innovative Structures and MaterialsRMIT UniversityMelbourneAustralia China Southern Airlines Co. LtdShenzhen BranchShenzhen518000China

In this article,the experimental and finite element analysis is utilized to investigate the quasi-static compression features of sandwich constructions built with tapered tubes.3D printing technology was utilized to create the hollow centers of the tapering tubes,with and without *** results demonstrate that the energy absorption(EA)and specific energy absorption(SEA)of the single corrugated tapered tube sandwich are 51.6% and 19.8% higher,respectively,than those of the conical tube ***,the results demonstrate that energy absorbers can benefit from corrugation in order to increase their ***,the tapered corrugated tubes'resistance to oblique impacts was *** to a straight tube,the tapered tube is more resistant to oblique loads and has a lower initial peak crushing force(PCF),according to numerical *** conducting a parametric study,it was discovered that the energy absorption performance of the sandwich construction is significantly affected by the amplitude,number of corrugations,and wall *** and SEA of DTS with corrugation number of 8 increased by 17.4%and 29.6%,respectively,while PCF decreased by 9.2% compared to DTS with corrugation number of 10.

关键词： Sandwich structure Corrugated tube Tapered tube Quasi-static Energy absorption

Effects of Bulky LATP in PEO-based Hybrid Solid Electrolytes

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Chinese Journal of Structural Chemistry 2020年第11期39卷 1941-1948页

作者： XUE Xi-Lai zhang xiang-xin LIN Jun-Hong CHEN Su-Jing CHEN Yuan-Qiang LIU Yong-Chuan zhang Yi-Ning Key Laboratory of Optoelectronic Materials Chemistry and Physics Fujian Institute of Research on the Structure of MatterChinese Academy of SciencesFuzhou 350002China University of Chinese Academy of Sciences Beijing 100049China Dalian National Laboratory for Clean Energy Chinese Academy of SciencesDalian 161000China

Solid polymer electrolytes(SPEs) have been considered as the spotlight in recent years due to their high safety, non-flammability and good flexibility. Nonetheless, high crystallinity of polymer matrix leads to low ionic conductivity at ambient conditions and retards the practical applications of SPEs. Herein, we report hybrid solid electrolytes(HSE) containing bulky LATP in poly(ethylene oxide)(PEO) matrix, which significantly enhances the electrochemical properties. LATP has been easily obtained by an accessible solid-state method. The solid electrolyte based on 20 wt% LATP in PEO polymer matrix(abbreviated as PEO-20) exhibits an ionic conductivity of 2.1 ×10-5 S·cm-1 at 30 ℃, an order of magnitude higher than 2.9 × 10-6 S·cm-1 of the pristine PEO solid electrolyte(abbreviated as PEO-0), mainly resulting from the decline of crystallinity in polymer matrix. The electrochemical window of PEO-20 can reach 4.84 V at room temperature, compared with 4.40 V for PEO-0, which could be compatible with high-voltage cathode materials.

关键词： hybrid solid electrolytes bulky LATP polyethylene oxide

太行山中南段测鱼地区中新生代构造变形及构造应力场

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河北地质大学学报 2024年第4期47卷 1-10页

作者：张祥信申方乐李伟王芳秦巨富河北地质大学河北省战略性关键矿产资源重点实验室河北石家庄050031 河北地质大学地球科学学院河北石家庄050031 河北地质大学华信学院河北石家庄050700

太行山中南段测鱼地区中新生代构造变形强烈,构造形迹以断裂构造为主。以测鱼地区广泛发育的共轭剪节理和断层为研究对象,在详细的野外构造观测和解析基础上,应用共轭剪节理统计和断层滑动矢量数据分析,对研究区中新生代构造应力场进行... 详细信息

太行山中南段测鱼地区中新生代构造变形强烈,构造形迹以断裂构造为主。以测鱼地区广泛发育的共轭剪节理和断层为研究对象,在详细的野外构造观测和解析基础上,应用共轭剪节理统计和断层滑动矢量数据分析,对研究区中新生代构造应力场进行了反演。构造解析表明,测鱼地区中新生代经历了3期构造应力场的演化,分别是中晚侏罗世NW-SE向挤压、早白垩世NW-SE向伸展和古新世-始新世NE-SW向挤压。根据区域构造演化特征,推测中晚侏罗世NW-SE向挤压应力场可能与古太平洋板块由NW向亚洲大陆东部俯冲消减有关;早白垩世NW-SE向伸展应力场与东亚活动陆缘的弧后伸展有关,形成于华北克拉通破坏阶段;古新世-始新世NE-SW向挤压应力场可能与太平洋板块的俯冲方向由NNW向往NWW向逆时针偏转有关。测鱼地区的上述3期构造应力场记录了太行山中南段中新生代构造演化和动力学背景信息。

关键词：构造变形构造应力场构造演化中新生代太行山中南段

Modeling of LF refining process:a review

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Journal of Iron and Steel Research International 2024年第2期31卷 289-317页

作者： Zi-cheng xin Jiang-shan zhang Kai-xiang Peng Jun-guo zhang Chun-hui zhang Qing Liu State Key Laboratory of Advanced Metallurgy University of Science and Technology BeijingBeijing100083China School of Automation and Electrical Engineering University of Science and Technology BeijingBeijing100083China Tangshan Branch Hebei Iron and Steel Co.Ltd.Tangshan063000HebeiChina xinjiang Bayi Iron and Steel Co. Ltd.Baosteel GroupWulumuqi830022XinjiangChina

With the increasing demand for energy conservation and emission reduction,more attentions have been paid to the intelligentization,greenization and low carbonization during the transformation and upgrading of steelmaking *** furnace(LF)refining is one of the key procedures in steelmaking process and has been widely used in steelmaking plants for its high equipment matching degree,low equipment investment and outstanding refining *** to the main tasks of LF refining process,the modeling methods of temperature prediction model,slag-making model,alloying model,argon blowing model and model of inclusions behavior were systematically reviewed,and the advantages and disadvantages of each modeling method were *** addition,the technical framework for the future has also been proposed based on existing works,including classification of raw materials,graphic representation of knowledge,introduction,upgradation and management of device/equipment,customization of steelmaking,modeling of refining process,synergy of models,intelligentization of decision-making,automation of control,and digitization of processes and operations,aiming to provide a reference for the modeling and intelligent development of LF refining process.

关键词： LF refining Temperature prediction Slag-making Alloying Argon blowing Inclusion behavior Modeling method

Clinical application of eight-zone laparoscopic dissection strategy for rectal cancer:Experience and discussion

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World Journal of Gastroenterology 2024年第30期30卷 3574-3583页

作者： Chang Chen xiang zhang xin Li Yan-Lei Wang Department of General Surgery Rongchang People's HospitalChongqing 250012China Department of Colorectal Surgery Qilu HospitalShandong UniversityJinan 250012Shandong ProvinceChina Department of General Surgery Huantai Branch of Qilu Hospital of Shandong UniversityZibo 255000Shandong ProvinceChina

BACKGROUND The incidence of rectal cancer is increasing worldwide,and surgery remains the primary treatment *** the advent of total mesorectal excision(TME)technique,the probability of tumor recurrence post-surgery has significantly ***'focus has gradually shifted towards minimizing the impact of surgery on urinary and sexual *** these concerns,the optimal dissection of the rectal lateral ligaments and preservation of the pelvic floor neuro-vascular bundle have become *** explore the optimal surgical technique for TME and establish a standardized surgical protocol to minimize the impact on urinary and sexual functions,we propose the eight-zone dissection strategy for pelvic floor *** To compare the differences in surgical specimen integrity and postoperative quality of life satisfaction between the traditional pelvic floor dissection strategy and the innovative eight-zone dissection *** We analyzed the perioperative data of patients who underwent laparoscopic radical resection of rectal cancer at Qilu Hospital of Shandong University between January 1,2021 and December 1,*** study included a total of 218 patients undergoing laparoscopic radical surgery for rectal cancer,among whom 109 patients underwent traditional pelvic floor dissection strategy,and 109 patients received the eight-zone dissection *** There were no significant differences in general characteristics between the two *** in the eight-zone dissection group had higher postoperative specimen integrity(88.1%vs 78.0%,P=0.047).At the 3-month followup,patients in the eight-zone surgery group had better scores in urinary issues(6.8±3.3 vs 5.3±2.5,P=0.045)and male sexual desire(2.2±0.6 vs 2.5±0.5,P=0.047)compared to the traditional surgery strategy *** This study demonstrates that the eight-zone dissection strategy for laparoscopic lateral ligament dissection of rectal cancer is safe and ***

关键词： Eight-zone dissection strategy Rectal cancer Lateral ligament dissection Nerve injury Total mesorectal excision surgery

Coordination-driven self-assembly of a molecular 818knot and molecular borromean rings

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Science China Chemistry 2024年第11期67卷 3652-3656页

作者： xiang Gao Dong Liu Hai-Ning zhang Guo-xin Jin Department of Chemistry Fudan University

We report the facile construction of a molecular 818knot and a molecular Borromean rings assembly through self-assembly directed by Cp*Rh corner units. Two curved ligands of similar size and shape were used in this study. The slight steric differences between the two ligands induce the formation of distinctly different topologies of the assembled products. The structures were confirmed by single-crystal X-ray analysis and nuclear magnetic resonance spectroscopy.

关键词： coordination-driven Cp*Rh 818 knot Borromean rings