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MXene@c-MWCNT Adhesive Silica Nanofiber Membranes Enhancing Electromagnetic Interference Shielding and Thermal Insulation Performance in Extreme Environments

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Nano-Micro Letters 2024年第10期16卷 82-98页

作者： Ziyuan Han yutao niu Xuetao Shi Duo Pan Hu Liu Hua Qiu Weihua Chen Ben Bin Xu Zeinhom MEl-Bahy Hua Hou Eman Ramadan Elsharkawy Mohammed AAmin Chuntai Liu Zhanhu Guo Key Laboratory of Materials Processing and Mold(Zhengzhou University) Ministry of EducationNational Engineering Research Center for Advanced Polymer Processing TechnologyZhengzhou UniversityZhengzhou 450002People's Republic of China School of Nano-Tech and Nano-Bionics University of Science and Technology of ChinaHefei 230026People's Republic of China Key Laboratory of Multifunctional Nanomaterials and Smart Systems Advanced Materials DivisionSuzhou Institute of Nano-Tech and Nano-BionicsChinese Academy of SciencesSuzhou 215123People's Republic of China Shaanxi Key Laboratory of Macromolecular Science and Technology School of Chemistry and Chemical EngineeringNorthwestern Polytechnical UniversityXi'an 710072People's Republic of China College of Chemistry&Green Catalysis Center Zhengzhou UniversityZhengzhou 450001People's Republic of China Mechanical and Construction Engineering Faculty of Engineering and EnvironmentNorthumbria UniversityNewcastle Upon Tyne NE18UK Department of Chemistry Faculty of ScienceAl-Azhar UniversityNasr City 11884CairoEgypt Department of Chemistry Faculty of ScienceNorthern Border UniversityArarSaudi Arabia Department of Chemistry College of ScienceTaif UniversityP.O.Box 1109921944 TaifSaudi Arabia

A lightweight flexible thermally stable composite is fabricated by com-bining silica nanofiber membranes(SNM)with MXene@c-MWCNT hybrid *** flexible SNM with outstanding thermal insulation are prepared from tetraethyl orthosilicate hydrolysis and condensation by electrospinning and high-temperature calcination;the MXene@c-MWCNT_(x:y)films are prepared by vacuum filtration *** particular,the SNM and MXene@c-MWCNT_(6:4)as one unit layer(SMC_(1))are bonded together with 5 wt%polyvinyl alcohol(PVA)solution,which exhibits low thermal conductivity(0.066 W m^(-1)K^(-1))and good electromagnetic interference(EMI)shielding performance(average EMI SE_(T),37.8 dB).With the increase in func-tional unit layer,the overall thermal insulation performance of the whole composite film(SMC_(x))remains stable,and EMI shielding performance is greatly improved,especially for SMC_(3)with three unit layers,the average EMI SET is as high as 55.4 *** addition,the organic combination of rigid SNM and tough MXene@c-MWCNT_(6:4)makes SMC_(x)exhibit good mechanical tensile ***,SMC_(x)exhibit stable EMI shielding and excellent thermal insulation even in extreme heat and cold ***,this work provides a novel design idea and important reference value for EMI shielding and thermal insulation components used in extreme environmental protection equipment in the future.

关键词： SiO_(2)nanofiber membranes MXene@c-MWCNT Composite film Thermal insulation Electromagnetic interference shielding

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Carbon nanotube fibers with excellent mechanical and electrical properties by structural realigning and densification

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Nano Research 2023年第11期16卷 12762-12771页

作者： Kunjie Wu Bin Wang yutao niu Wenjing Wang Cao Wu Tao Zhou Li Chen Xianghe Zhan Ziyao Wan Shan Wang Zhengpeng Yang Yichi Zhang Liwen Zhang Yongyi Zhang Zhenzhong Yong Muqiang Jian Qingwen Li Key Laboratory of Multifunctional Nanomaterials and Smart Systems Suzhou Institute of Nano-Tech and Nano-BionicsChinese Academy of SciencesSuzhou 215123China Division of Nanomaterials and Jiangxi Key Lab of Carbonene Materials Jiangxi Institute of NanotechnologyNanchang 330200China School of Nano-Tech and Nano-Bionics University of Science and Technology of ChinaHefei 230026China Henan Key Laboratory of Materials on Deep-Earth Engineering School of Materials Science and EngineeringHenan Polytechnic UniversityJiaozuo 454003China Beijing Graphene Institute(BGI) Beijing 100095China

Floating catalysis chemical vapor deposition(FCCVD)direct spinning process is an attractive method for fabrication of carbon nanotube fibers(CNTFs).However,the intrinsic structural defects,such as entanglement of the constituent carbon nanotubes(CNTs)and inter-tube gaps within the FCCVD CNTFs,hinder the enhancement of mechanical/electrical properties and the realization of practical applications of ***,achieving a comprehensive reassembly of CNTFs with both high alignment and dense packing is particularly ***,an efficient reinforcing strategy for FCCVD CNTFs was developed,involving chlorosulfonic acid-assisted wet stretching for CNT realigning and mechanical rolling for *** reveal the intrinsic relationship between the microstructure and the mechanical/electrical properties of CNTFs,the microstructure evolution of the CNTFs was characterized by cross-sectional scanning electron microscopy(SEM),wide angle X-ray scattering(WAXS),polarized Raman spectroscopy and Brunauer–Emmett–Teller(BET)*** results demonstrate that this strategy can improve the CNT alignment and eliminate the inter-tube voids in the CNTFs,which will lead to the decrease of mean distance between CNTs and increase of inter-tube contact area,resulting in the enhanced inter-tube van der Waals *** microstructural evolutions are beneficial to the load transfer and electron transport between CNTs,and are the main cause of the significant enhancement of mechanical and electrical properties of the ***,the tensile strength,elastic modulus and electrical conductivity of the high-performance CNTFs are 7.67 GPa,230 GPa and 4.36×10^(6)S/m,*** paves the way for further applications of CNTFs in high-end functional composites.

关键词： carbon nanotube fibers mechanical property electrical property alignment packing density

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Hollow Gradient-Structured Iron-Anchored Carbon Nanospheres for Enhanced Electromagnetic Wave Absorption

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Nano-Micro Letters 2023年第1期15卷 144-160页

作者： Cao Wu Jing Wang Xiaohang Zhang Lixing Kang Xun Cao Yongyi Zhang yutao niu Yingying Yu Huili Fu Zongjie Shen Kunjie Wu Zhenzhong Yong Jingyun Zou Bin Wang Zhou Chen Zhengpeng Yang Qingwen Li Key Laboratory of Multifunctional Nanomaterials and Smart Systems Advanced Materials DivisionSuzhou Institute of Nano-Tech and Nano-BionicsChinese Academy of SciencesSuzhou 215123JiangsuPeople’s Republic of China School of Science Nanchang Institute of TechnologyNanchang 330099JiangxiPeople’s Republic of China Division of Nanomaterials and Jiangxi Key Lab of Carbonene Materials Jiangxi Institute of NanotechnologyNanchang 330200JiangxiPeople’s Republic of China School of Nano-Tech and Nano-Bionics University of Science and Technology of ChinaHefei 230026AnhuiPeople’s Republic of China School of Materials Science and Engineering Nanyang Technological University50 Nanyang AvenueSingapore 639798Singapore Jiangsu Key Laboratory of Micro and Nano Heat Fluid Flow Technology and Energy Application School of Physical Science and TechnologySuzhou University of Science and TechnologySuzhou 215009People’s Republic of China School of Mechanical and Power Engineering Nanjing Tech UniversityNanjing 211800People’s Republic of China Henan Key Laboratory of Materials On Deep-Earth Engineering School of Materials Science and EngineeringHenan Polytechnic UniversityJiaozuo 454003People’s Republic of China College of Safety Science and Engineering Xi’an University of Science and TechnologyXi’an 710054People’s Republic of China

In the present paper,a microwave absorber with nanoscale gradient structure was proposed for enhancing the electromagnetic absorption *** inorganic-organic competitive coating strategy was employed,which can effectively adjust the thermodynamic and kinetic reactions of iron ions during the solvothermal *** a result,Fe nanoparticles can be gradually decreased from the inner side to the surface across the hollow carbon *** results reveal that it offers an outstanding reflection loss value in combination with broadband wave absorption and flexible adjustment ability,which is superior to other relative graded distribution structures and satisfied with the requirements of lightweight *** addition,this work elucidates the intrinsic microwave regulation mechanism of the multiscale hybrid electromagnetic wave *** excellent impedance matching and moderate dielectric parameters are exhibited to be the dominative factors for the promotion of microwave absorption performance of the optimized *** strategy to prepare gradient-distributed microwave absorbing materials initiates a new way for designing and fabricating wave absorber with excellent impedance matching property in practical applications.

关键词： Gradient structures Carbon nanospheres Electromagnetic wave absorption Impedance matching

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One-step wet-spinning assembly of twisting-structured graphene/carbon nanotube fiber supercapacitor

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Journal of Energy Chemistry 2020年第12期29卷 434-441页

作者： Zhengpeng Yang Yuanheng Jia yutao niu Yongyi Zhang Chunjing Zhang Ping Li Meng Zhu Qingwen Li Henan Key Laboratory of Materials on Deep-Earth Engineering School of Materials Science and EngineeringHenan Polytechnic UniversityJiaozuo 454003HenanChina Key Laboratory of Multifunctional Nanomaterials and Smart Systems Advanced Materials DivisionSuzhou Institute of Nano-Tech and Nano-BionicsChinese Academy of SciencesSuzhou 215123JiangsuChina School of Nano-Tech and Nano-Bionics University of Science and Technology of ChinaHefei 230026AnhuiChina Division of Nanomaterials and Jiangxi Key Lab of Carbonene Materials Suzhou Institute of Nano-Tech and Nano-BionicsNanchangChinese Academy of SciencesNanchang 330200JiangxiChina

Graphene fiber-based supercapacitors hold great promise as flexible energy-storage devices. However, simultaneously achieving high ion-transport ability in electrode and electrolyte layer, which is crucial for realizing the high electrochemical performance, still remains challenging. Here, a facile and effective strategy to solve the problem was proposed by developing a twisting-structured graphene/carbon nanotube(CNT) fiber supercapacitor via one-step wet-spinning process with customized multi-channel *** remarkable structure features of the resulting fiber supercapacitor with wrinkled and thin electrolyte layer, and well-developed porosity of fiber electrode favored the rapid infiltration and transport of electrolyte ions inside the electrode, as well as between electrode and electrolyte, thus boosting high specific capacitance of 187.6 mF cm^(-2) and energy density of 30.2 μWh cm^(-2), and featuring long cycling life(93%capacitance retention after 10,000 cycles) and excellent flexibility. Moreover, the specific capacitance and energy density could be further improved to 267.2 m F cm^(-2) and 66.8 μWh cm^(-2), respectively, when Mn O2 was incorporated into the fiber.

关键词： One-step wet-spinning Graphene fiber-based supercapacitor Twisting-structured fiber Ion transport

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Design and Verification of Parallel Hip Exoskeleton Considering Output Torque Anisotropy

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Journal of Bionic Engineering 2024年第3期21卷 1305-1320页

作者： Jilong Xu Yunzhan niu Fucai Liu Engineering Research Center of the Ministry of Education for Intelligent Control System and Intelligent Equipment Yanshan UniversityQinhuangdao066004China Key Laboratory of Industrial Computer Control Engineering of Heibei Province Yanshan UniversityQinhuangdao066004China College of Mechanical Engineering Yanshan UniversityQinhuangdao066004China

In rehabilitation training,it is crucial to consider the compatibility between exoskeletons and human legs in ***,most exoskeletons today adopt an anthropomorphic serial structure,which results in rotational centers that are not precisely aligned with the center of the hip *** address this issue,we introduce a novel exoskeleton called the Parallel Hip Exoskeleton(PH-Exo)in this ***-Exo is meticulously designed based on the anisotropic law of output *** the friction of the drive components,a dynamic model of the human-machine complex is *** analysis demonstrates that PH-Exo not only exhibits outstanding torque performance but also achieves high controllability in both flexion/extension and adduction/abduction ***,a robust controller is designed to address model uncertainty,friction,and external *** experiments indicate that under the control of the robust controller,each motor achieves excellent tracking performance.

关键词： Hip exoskeleton Parallel mechanism Misalignment Anisotropy Output torque

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An integrative mathematical model of microwave ion thruster for mHz-frequency thrust noise analysis

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Chinese Journal of Aeronautics 2024年第4期37卷 121-136页

作者： Xiang niu Hui LIU Daren YU Plasma Propulsion Laboratory Harbin Institute of TechnologyHarbin 150001China

Many high-precision space missions need thrusters to produce thrust with low noise to compensate for disturbances and ensure satellite platform stability. Microwave ion thruster is characterized with a wide thrust range and potential for these missions. A cost-effective and accurate mathematical model is crucial for mHz-frequency thrust noise analysis and feedback controller design. The Particle-In-Cell(PIC) and global models are two common simulation tools. The PIC model is characterized with high accuracy but huge computation cost, which is difficult to analyze long-time performance characteristics. Now, the global model is only used for the discharge chamber with low accuracy and cannot reflect ion extraction properties. In this paper, an integrative mathematical model is built for a 1-cm microwave ion thruster and can reflect ion beamlet divergence and impingement on the Accelerator Grid(AG). Simulation results show good agreement with experiments at 0.06 sccm. However, the model demonstrates worse consistency with experiments when the flux increases to 0.1 sccm, which may be because the influence of neutral gas on the Electron Cyclotron Resonance(ECR) is not considered in the model. A long-time(1000 s) simulation is conducted with this model under 35 μN. It takes 3 hrs, and the thrust noise reaches 1 μN/Hz^(0.5) at 1 mHz.

关键词： Electric propulsion Microwave ion thruster Integrative model Sheath property Ion beamlet divergence Thrust noise Plasma

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Vascularization ability of glioma stem cells in different three-dimensional microenvironments

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Regenerative Biomaterials 2024年第1期3卷 34-43页

作者： Xuanzhi Wang Tao Xu Chaoshi niu Department of Neurosurgery The First Affliated Hospital of USTCDivision of Life Sciences and MedicineUniversity of Science and Technology of ChinaHefeiAnhui230036China Department of Neurosurgery Sichuan Provincial People's HospitalUniversity of Electronic Science and Technology of ChinaChengdu 610072People's Republic of China Center for Bio-intelligent Manufacturing and Living Matter Bioprinting Research Institute of Tsinghua University in ShenzhenTsinghua UniversityShenzhen 518057People's Republicof China

Glioblastoma(GBM)is among the most common and aggressive adult central nervous system *** prominent charac-teristic of GBM is the presence of abnormal microvessels.A significant correlation between angiogenesis and prognosis has been *** reconstructing this neovascula-rization and tumor microenvironment through personalized in vitro disease models presents a significant ***,it is crucial to develop new anti-angiogenic therapies for *** this study,3D bioprinted glioma stem cell(GSC)-laden hydrogel scaffolds,hybrid Gsc hydrogels and ceil-free hydrogel scaffolds were manufactured to investigate the vas-cularization ability of GsCs in varying 3D microenvironments.

关键词： 3D bioprinting xenograft tumors GSC-laden hydrogel scaffold glioblastoma angiogenesis

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Event-triggered sliding mode control of linear repetitive processes and its application in metal rolling process

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Science China(Information Sciences) 2024年第3期67卷 167-181页

作者： Xinyu LV Yugang niu James LAM Key Laboratory of Smart Manufacturing in Energy Chemical Process (East China University of Science and Technology) Ministry of Education Department of Mechanical Engineering The University of Hong Kong

This paper investigates the design problem of a sliding mode controller for linear repetitive processes(LRPs) with a finite pass length on each pass. Under limited communication resources, an eventtriggered mechanism is implemented from the sensors to the controller, whose triggered sequence is consistent with the evolution direction of LRPs. To periodically orchestrate communication between the controller and actuator, a round-robin scheduling mechanism is established based on the pass length. A sliding function involving the state and pass profile is constructed, and the sliding mode controller is designed using triggered states and pass profile signals. Feasible controller gains are attained to ensure the stability of the resultant closed-loop system. Finally, the proposed strategy is implemented for a multi-roll metal rolling process.

关键词： event-triggered mechanism linear repetitive processes metal rolling process round-robin scheduling sliding mode control

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Bilayer solid-electrolyte interphase structure enables a 440 Wh kg^(-1) lithium metal pouch cell to achieve 130 cycles

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Science China Chemistry 2024年第3期67卷 751-752页

作者： Xiong Liu Chaojiang niu School of Materials Science and Engineering Zhengzhou UniversityZhengzhou 450001China

Lithium(Li) metal has been considered one of the most promising anodes due to its high theoretical capacity, lightweight and low electrochemical potential. The cell-level energy density of rechargeable lithium metal batteries(LMBs) is expected to surpass 500 Wh kg^(-1) after replacing the graphite anode in lithium-ion batteries [1].

关键词： lithium electrolyte layer

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An Asynchronous Variational Integrator for Contact Problems Involving Elastoplastic Solids

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Acta Mechanica Solida Sinica 2024年第2期37卷 305-315页

作者： Zongwu niu Zixiao Wang Yongxing Shen University of Michigan-Shanghai Jiao Tong University Joint Institute Shanghai Jiao Tong UniversityShanghai200240China School of Agriculture and Biology Shanghai Jiao Tong UniversityShanghai200240China Department of Biostatistics Johns Hopkins Bloomberg School of Public HealthBaltimoreMaryland21205USA

Simulations of contact problems involving at least one plastic solid may be costly due to their strong nonlinearity and requirements of *** this work,we develop an explicit asynchronous variational integrator(AVI)for inelastic non-frictional contact problems involving a plastic *** AVI assigns each element in the mesh an independent time step and updates the solution at the elements and nodes *** asynchrony makes the AVI highly efficient in solving such bi-material *** advantage of the AVI,the constitutive update is locally performed in one element at a time,and contact constraints are also enforced on only one *** time step of the contact element is subdivided into multiple segments,and the fields are updated *** a contact event,only one element involving a few degrees of freedom is considered,leading to high *** proposed formulation is first verified with a pure elastodynamics benchmark and further applied to a contact problem involving an elastoplastic solid with non-associative volumetric *** numerical results indicate that the AVI exhibits excellent energy behaviors and has high computational efficiency.

关键词： Asynchronous variational integrator Plasticity Contact Computational efficiency Finite element method

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