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生物炭及其复合材料活化过硫酸盐研究进展

材料工程 2023年第2期51卷 80-90页

作者：苏浩杰吴俊峰王召东成先雄 STOLBIKHIN yury v 江西理工大学赣江流域水质安全保障技术创新中心江西赣州341000 河南城建学院河南省水体污染防治与修复重点实验室河南平顶山467036 圣彼得堡国立建筑工程大学环境与市政工程学院俄罗斯圣彼得堡190005

以硫酸根自由基(SO_(4)^(-)·)为基础的高级氧化工艺被公认为是降解有机废水的有效方法之一。作为一种经济、易得的含碳材料,生物炭已逐渐应用于高级氧化领域。生物炭及其复合材料活化过硫酸盐已成为一种较有前景的有机污染物降解体系... 详细信息

以硫酸根自由基(SO_(4)^(-)·)为基础的高级氧化工艺被公认为是降解有机废水的有效方法之一。作为一种经济、易得的含碳材料,生物炭已逐渐应用于高级氧化领域。生物炭及其复合材料活化过硫酸盐已成为一种较有前景的有机污染物降解体系。本文分析了用于过硫酸盐活化的不同典型生物炭基催化剂最新研究进展,包括原始生物炭、过渡金属负载生物炭、非金属掺杂生物炭、金属与非金属共掺杂生物炭等。总结了其合成方法和理化性质,并分别讨论了生物炭基催化剂对过硫酸盐的活化性能与机理,以及该体系对有机污染物的降解机理。最后根据现有研究进展,分别从不同生物质来源、金属非金属共同改性生物炭技术以及降解过程中生态毒性动态变化等角度,针对降解机制探索、潜在催化剂开发和实际催化系统应用等方面,对生物炭及其复合材料进行了相关讨论并提出建议。

关键词：生物炭合成过硫酸盐降解机理

Relation of the IGF/IGF1R system to autophagy in colitis and colorectal cancer

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World Journal of Gastroenterology 2017年第46期23卷 8109-8119页

作者： Ferenc Sipos Hajnal Székely Imre Dániel kis Zsolt Tulassay Gyorgyi Muzes 2nd Department of Internal Medicine Semmelweis University Faculty of Medicine Semmelweis University Molecular Medicine Research Group Hungarian Academy of Sciences

Metabolic syndrome(Met S), as a chronic inflammatory disorder has a potential role in the development of inflammatory and cancerous complications of the colonic tissue. The interaction of DNA damage and inflammation is affected by the insulin-like growth factor 1 receptor(IGF1 R) signaling pathway. The IGF1 R pathway has been reported to regulate autophagy, as well, but sometimes through a bidirectional context. Targeting the IGF1 R-autophagy crosstalk could represent a promising strategy for the development of new antiinflammatory and anticancer therapies, and may help for subjects suffering from Met S who are at increased risk of colorectal cancer. However, therapeutic responses to targeted therapies are often shortlived, since a signaling crosstalk of IGF1 R with other receptor tyrosine kinases or autophagy exists, leading to acquired cellular resistance to therapy. From a pharmacological point of view, it is attractive to speculate that synergistic benefits could be achieved by inhibition of one of the key effectors of the IGF1 R pathway, in parallel with the pharmacological stimulation of the autophagy machinery, but cautiousness is also required, because pharmacologic IGF1 R modulation can initiate additional, sometimes unfavorable biologic effects.

关键词： Insulin-like growth factor IGF1R Autophagy Colitis Colorectal cancer Metabolic syndrome

Wafer-scale MOCvD growth of monolayer M0S2 on sapphire and SiO2

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Nano Research 2019年第10期12卷 2646-2652页

作者： Huanyao Cun Michal Macha HoKwon Kim Ke Liu Yanfei Zhao Thomas LaGrange Andras kis Aleksa ndra Radeno vic Laboratory of Nanoscale Biology Institute of BioengineeringEcole Polytechnique Federate de Lausanne(EPFL)1015 LausanneSwitzerland Nanoscale Electronics and Structures Electrical Engineering InstituteEcole Poly technique Federate de Lausanne(EPFL)1015 LausanneSwitzerland Nanoscale Electronics and Structures Institute of Materials Science and EngineeringEcole Poly technique Federate de Lausanne(EPFL)1015 LausanneSwitzerland Interdisciplinary Center for Electron Microscopy(CIME) Ecole Polytechnique Federale de Lausanne(EPFL)1015 LausanneSwitzerland

High-quality and large-scale growth of monolayer molybdenum disulfide(MoS2)has caught intensive attention because of its potential in many applications due to unique electronic ***,we report the wafer-scale growth of high-quality mono layer MoS2 on singlecrystalline sapphire and also on SiO2 substrates by a facile metal-organic chemical vapor deposit!on(MOCvD)*** to growth,an aqueous solution of sodium molybdate(Na2MoO4)is spun onto the substrates as the molybdenum precursor and diethyl sulfide((C2H5)2S)is used as the sulfur precursor duri ng the *** grown MoS2 films exhibit crystal I i nity,good electrical performa nee(electro n mobility of 22 cm2·v^-1·s^-1)and structural continuity maintained over the entire *** sapphire substrates are reusable for subsequent *** same method is applied for the synthesis of tungsten disulfide(WS2).Our work provides a facile,reproducible and cost-efficient method for the scalable fabricati on of high-quality mono layer MoS2 for versatile applicati ons,such as electro nic and optoelectr onic devices as well as the membranes for desalination and power generation.

关键词： molybdenum disulfide two-dimensional(2D)materials metal-organic chemical vapor deposition(MOCvD) wafer-scale fabrication

Identifying sex-specific injury predictors as a key factor in maintaining optimal physical activity levels

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World Journal of Orthopedics 2023年第3期14卷 146-154页

作者： Maria v Sankova vladimir N Nikolenko Marine v Oganesyan Andjela D vovkogon Aida N Gadzhiakhmedova Tatyana S Zharikova yury O Zharikov Department of Human Anatomy and Histology I.M.Sechenov First Moscow State Medical University(Sechenov University)Moscow 125009Russia Department of Normal and Topographic Anatomy Lomonosov Moscow State UniversityMoscow 119991Russia European Osteopathic Clinical Center of the Moscow Branch of the“Medical Academy of Osteopathic Education” Saint Petersburg 199106Russia Institute of Clinical Medicine I.M.Sechenov First Moscow State Medical University(Sechenov University)Moscow 119991Russia

BACKGROUND Optimal physical activity is known to reduce cardiovascular,respiratory and endocrine system diseases and,as a consequence,improve quality of *** important risk factor for reinjuries during normal exercise is the initial connective tissue *** variety of clinical dysplastic manifestations significantly complicate the timely diagnosis of this *** To establish pathognomonic sex-specific dysplasia phenotypes that indicate a particular sensitivity to physical *** The study involved 117 participants with recurrent musculoskeletal injuries that occurred during normal *** were 67 women(57.26%)and 50 men(42.74%),which made it possible to compare the presence of the identified signs between sexes.A validated questionnaire was used to screen their connective tissue *** Ranking the most commonly revealed dysplasia signs depending on their clinical significance made it possible to establish pathognomonic sex-specific phenotypes that indicated a particular susceptibility to *** programs of optimal physical activity are necessary for men with chest deformities,flat-valgus feet,dolichostenomelia,arachnodactylia,hemorrhoids,abdominal muscle diastasis and recurrent *** women,special sensitivity to physical exertion was associated with a combination of signs such as asthenic body,joint hypermobility,overly soft auricles,thin hyperelastic skin,atrophic striae,telangiectasias and varicose *** particular importance were universal signs such as gothic palate,scoliosis,kyphosis,leg deformities,temporomandibular joint crunching,and moderate to high *** Participants’connective tissue condition should be considered when designing optimal physical activity *** the established sex-specific dysplasia phenotypes will allow timely optimization of training loads,thus reducing the risk of injury.

关键词： Injury risk Physical activity Connective tissue condition Sex-specific dysplasia phenotypes Clinical dysplastic manifestations

Synthesis, X-ray Structure and Bioactivity of N-4-Methyl-1,2,3-thiadiazole-5-carbonyl-N′-3,5- dichloro-4-(1,1,2,2-tetrafluoroethoxyl)phenyl Urea

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Chinese Journal of Structural Chemistry 2012年第12期31卷 1721-1728页

作者：国丹丹王盾范志金李娟娟宋海斌范谦 Tatiana A. Kalinina Morzherin yury Yur'evich Belskaya N. Pavlovna Bakulev v. Alekseevich State Key Laboratory of Elemento Organic Chemistry Nankai University Sichuan Functional Heterocyclic Compounds Engineering Technology Research Center The Ural Federal University Named after the First President of Russia B. N. Yeltsin

The title compound N-4-methyl-1,2,3-thiadiazole-5-carbonyl-N＇-3,5-dichloro-4- （1,1,2,2- tetrafluoroethoxyl）phenyl urea （C13H8Cl2F4N4O3S, Mr = 447.19） has been synthesized from 4-methyl- 1,2,3-thiadiazole-5-carbonyl chloride as the starting material, and its structure was characterized by proton Nuclear Magnetic Resonance （1H NMR）, Infra Red Spectroscopy （IR）, high-resolution mass spectroscopy （HRMS）, and single-crystal X-ray diffraction. The crystal of the title compound belongs to triclinic, space group Pi with a = 6.0780（8）, b = 11.3760（14）, c = 12.1440（18） A, α = 96.887（7）, β = 91.027（12）, γ= 104.252（13）°, Z = 2, v= 806.98（19）A3, Dc = 1.840 g/cm3, μ= 0.601 mm-1, F（000） = 448, R = 0.0450 and wR = 0.0869. X-ray analysis indicates that the 1,2,3-thiadiazole ring is not coplanar with the phenyl ring, and the dihedral angle is 33.57°. Two intermolecular hydrogen bonds N（2）-H…O（1 ）, S（1 ）…H-C（11）, and three weak intermolecular interactions, C（11）…O（1）, N（1）…O（2） and S…O（1）, are observed. The bioassay results indicate that the title compound has good insecticidal activity against Culex pipiens pallens and good induction activity for tobacco against tobacco mosaic virus which is equal to that of TDL.

关键词： crystal structure 1,2,3-thiadiazole synthesis biological activity

Boundary Eigenvalue Problem for Maxwell Equations in a Nonlinear Dielectric Layer

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Applied Mathematics 2010年第1期1卷 29-36页

作者： yury G. Smirnov Dmitry v. valovik Department Mathematics and Supercomputer Modeling Penza State University Penza Russia

The propagation of TM-polarized electromagnetic waves in a dielectric layer filled with lossless, nonmagnetic, and isotropic medium is considered. The permittivity in the layer defines by Kerr law. We look for eigenvalues of the problem and reduce the issue to the analysis of the corresponding dispersion equation. The equivalence of the boundary eigenvalue problem and the dispersion equation is proved. We show that the solution of the problem exists and from dispersion equation it can be numerically obtained. Using this solution the components of electromagnetic field in the layer can be numerically obtained as well. Transition to the limit in the case of a linear medium in the layer is proved. Some numerical results are presented also.

关键词： Maxwell Equations Nonlinear Boundary Eigenvalue Problem Dispersion Equation Nonlinear Slab (Film)

Anatomical basis for pancreas transplantation via isolated splenic artery perfusion:A literature review

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World Journal of Clinical Cases 2022年第35期10卷 12844-12853页

作者： Ilya Dmitriev Marine Oganesyan Antonina Popova Egor Orlov Mikhail Sinelnikov yury Zharikov Department of Pancreas and Kidney Transplantation N.V.Sklifosovsky Research Institute for Emergency CareMoscow 107045Russia Department of Human Anatomy Sechenov First Moscow State Medical University(Sechenov University)Moscow 125009Russia Department of Oncology Radiotherapy and Reconstructive SurgerySechenov First Moscow State Medical University(Sechenov University)Moscow 119048Russia Laboratory of clinical morphology Research Institute of Human MorphologyMoscow 117418Russia

The variability of vascular anatomy of the pancreas underlines the difficulty of its *** regarding the consistency of anatomical variations shows splenic arterial dominance in most *** can significantly improve transplantation success.A systematic literature review was performed according to the quality standards described in the AMSTAR measurement tool and the PRISMA *** valuated existing literature regarding the vascularization and blood perfusion patterns of the pancreas in terms of dominance and *** collected data was independently analyzed by two *** of vascular anatomy was seen to be underreported in literature,though significant findings have been included and discussed in this study,providing valuable insight into the dynamics of pancreatic perfusion and feasibility of transplantation on several different supplying *** splenic artery(SA)has a high percentage of consistency in all found studies(over 90%).High frequency of anastomoses between arterial pools supplying the pancreas can mediate sufficient blood supply through a dominant vessel,such as the SA,which is present in most *** transplantation with isolated SA blood supply can provide sufficient arterial perfusion of the pancreas for stable transplant viability due to high anatomical consistency of the SA and vast communications with other arterial systems.

关键词： Pancreas transplantation Isolated splenic artery supply Pancreas anatomy pancreatic perfusion Minireview

variational Structure and Uniqueness of Generalized Kähler-Ricci Solitons

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Peking Mathematical Journal 2023年第2期6卷 307-351页

作者： vestislav Apostolov Jeffrey Streets yury Ustinovskiy Départment de Mathématiques Universitédu QuébecàMontréalCase Postale 8888Succursale Centre-VilleMontréalQCH3C 3P8Canada Laboratoire de Mathématiques Jean Leray Universitéde Nantes2Rue de la HoussinièreBP 9220844322NantesFrance Rowland Hall University of CaliforniaIrvineCA92617USA Department of Mathematics Lehigh UniversityChandler-Ullmann Hall 17Memorial Drive EastBethlehemPA18015USA

Under broad hypotheses we derive a scalar reduction of the generalized Kähler-Ricci soliton *** realize solutions as critical points of a functional,analogous to the classical Aubin energy,defined on an orbit of the natural Hamiltonian action of diffeomorphisms,thought of as a generalized Kähler *** functional is convex on a large set of paths in this space,and using this we show rigidity of solitons in their generalized Kähler *** an application we prove uniqueness of the generalized Kähler-Ricci solitons on Hopf surfaces constructed in Streets and Ustinovskiy[*** ***.74(9),1896-1914(2020)],finishing the classification in complex dimension 2.

关键词： Generalized Ricci solitons Hopf surfaces Poisson structures Aubin functional

Doped GaSe crystals for laser frequency conversion

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Light(Science & Applications) 2015年第1期4卷 47-58页

作者： Jin Guo Ji-Jiang Xie Dian-Jun Li Gui-Long Yang Fei Chen Chun-Rui Wang Lai-Ming Zhang yury M Andreev Konstantin A Kokh Gregory v Lanskii valery A Svetlichnyi State Key Laboratory of Laser Interaction with Matter Changchun Institute of OpticsFine Mechanics and PhysicsCASChangchun 130033China Innovation Laboratory of Electro-Optical Countermeasures Technology Changchun Institute of OpticsFine Mechanics and PhysicsCASChangchun 130033China Laboratory of GeosphereBiosphere Interactions Institute of Monitoring of Climatic and Ecological SystemsSB RASTomsk 634055Russia Laboratory of Advanced Materials and Technologies Siberian Physical-Technical Institute of Tomsk State UniversityTomsk 634050Russia Crystal Growth Laboratory Institute of Geology and MineralogySB RASNovosibirsk 630090Russia Novosibirsk State University Novosibirsk 630090Russia

In this review,we introduce the current state of the art of the growth technology of pure,lightly doped,and heavily doped(solid solution)nonlinear gallium selenide(GaSe)crystals that are able to generate broadband emission from the near infrared(IR)(0.8 mm)through the mid-and far-IR(terahertz(THz))ranges and further into the millimeter wave(5.64 mm)*** the first time,we show that appropriate doping is an efficient method controlling a range of the physical properties of GaSe crystals that are responsible for frequency conversion efficiency and exploitation *** appropriate doping,uniform crystals grown by a modified technology with heat field rotation possess up to 3 times lower absorption coefficient in the main transparency window and THz ***,doping provides the following benefits:raises by up to 5 times the optical damage threshold;almost eliminates two-photon absorption;allows for dispersion control in the THz range independent of the mid-IR dispersion;and enables crystal processing in arbitrary directions due to the strengthened ***,doped GaSe demonstrated better usefulness for processing compared with GaSe grown by the conventional technology and up to 15 times higher frequency conversion efficiency.

关键词： frequency conversion GaSe solid solution crystal THz