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Enhanced high-temperature mechanical properties of laser-arc hybrid additive manufacturing of Al-Zn-Mg-Cu alloy via microstructure control

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Journal of Materials Science & Technology 2024年第2期169卷 220-234页

作者： Dehua Liu Dongjiang Wu yunsong wang Zhuo Chen Changrong Ge Qingyu Zhao Fangyong Niu Guangyi Ma State Key Laboratory of High-performance Precision Manufacturing Dalian University of TechnologyDalian 116024China

Recently,rapid and cost-effective additive manufacturing solutions for lightweight aluminum alloys with excellent high-temperature mechanical properties have been increasingly in demand.In this study,we combined laser-arc hybrid additive manufacturing with solution and artificial aging treatments to achieve Al-Zn-Mg-Cu alloy with favorable high-temperature strength via microstructure control.Hydrogen pores became the major defect in the as-deposited and heat-treated specimens.The continuous distribution of eutectics with hard-brittle characteristics at the grain boundaries was destructed following heat treat-ment.High-densityηprecipitates were uniformly dispersed in the heat-treated Al-Zn-Mg-Cu alloy,whereas appeared coarsened and dissolved at 473 K,owing to the rapid diffusion of Zn and Mg.The average 0.2%yield strength(318±16 MPa)and ultimate tensile strength(362±20 MPa)at 473 K af-ter heat treatment were enhanced by approximately 58%and 51%,respectively,compared to those of the as-deposited specimen.In addition,theηprecipitates contributed to lattice distortions and strain fields,which prevented dislocation motion and increased slip deformation resistance at high temper-atures.The as-deposited specimen exhibited intergranular fracture at 473 K,with cracks preferring to propagate along the aggregated eutectics.However,crack propagation proceeded in the sections with more pores in the heat-treated specimen.Our approach may provide a valid option for achieving alu-minum alloys with excellent high-temperature mechanical properties.

关键词： Laser-arc hybrid additive manufacturing Al-Zn-Mg-Cu alloy High-temperature strength Heat treatment,Microstructure evolution

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Competitive oxidation behavior of Ni-based superalloy GH4738 at extreme temperature

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International Journal of Minerals,Metallurgy and Materials 2024年第1期31卷 138-145页

作者： Hui Xu Shufeng Yang Enhui wang yunsong Liu Chunyu Guo Xinmei Hou Yanling Zhang State Key Laboratory of Advanced Metallurgy University of Science and Technology BeijingBeijing 100083China Institute for carbon neutrality University of Science and Technology BeijingBeijing 100083China

A high thrust-to-weight ratio poses challenges to the high-temperature performance of Ni-based superalloys. The oxidation behavior of GH4738 at extreme temperatures has been investigated by isothermal and non-isothermal experiments. As a result of the competitive diffusion of alloying elements, the oxide scale included an outermost porous oxide layer (OOL), an inner relatively dense oxide layer (IOL), and an internal oxide zone (IOZ), depending on the temperature and time. A high temperature led to the formation of large voids at the IOL/IOZ interface. At 1200℃, the continuity of the Cr-rich oxide layer in the IOL was destroyed, and thus, spallation occurred. Extension of oxidation time contributed to the size of Al-rich oxide particles with the increase in the IOZ. Based on this finding,the oxidation kinetics of GH4738 was discussed, and the corresponding oxidation behavior at 900-1100℃ was predicted.

关键词： Ni-based superalloy GH4738 extreme temperature competitive oxidation oxidation mechanism oxidation kinetics

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3D-printed Mg-1Ca/polycaprolactone composite scaffolds with promoted bone regeneration

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Journal of Magnesium and Alloys 2024年第3期12卷 966-979页

作者： Xiao Zhao Siyi wang Feilong wang Yuan Zhu Ranli Gu Fan Yang Yongxiang Xu Dandan Xia yunsong Liu Department of Prosthodontics Peking University School and Hospital of StomatologyBeijing 100081China National Center of Stomatology National Engineering Laboratory for Digital and Material Technology of StomatologyNational Clinical Research Center for Oral DiseasesBeijing Key Laboratory of Digital StomatologyResearch Center of Engineering and Technology for Computerized Dentistry Ministry of HealthNMPA Key Laboratory for Dental MaterialsBeijing 100081China Department of Dental Materials Peking University School and Hospital of StomatologyBeijing 100081China

In bone tissue engineering,polycaprolactone(PCL)is a promising material with good biocompatibility,but its poor degradation rate,mechanical strength,and osteogenic properties limit its application.In this study,we developed an Mg-1Ca/polycaprolactone(Mg-1Ca/PCL)composite scaffolds to overcome these limitations.We used a melt blending method to prepare Mg-1Ca/PCL composites with Mg-1Ca alloy powder mass ratios of 5,10,and 20 wt%.Porous scaffolds with controlled macro-and microstructure were printed using the fused deposition modeling method.We explored the mechanical strength,biocompatibility,osteogenesis performance,and molecular mechanism of the Mg-1Ca/PCL composites.The 5 and 10 wt%Mg-1Ca/PCL composites were found to have good biocompatibility.Moreover,they promoted the mechanical strength,proliferation,adhesion,and osteogenic differentiation of human bone marrow stem cells(hBMSCs)of pure PCL.In vitro degradation experiments revealed that the composite material stably released Mg_(2)+ions for a long period;it formed an apatite layer on the surface of the scaffold that facilitated cell adhesion and growth.Microcomputed tomography and histological analysis showed that both 5 and 10 wt%Mg-1Ca/PCL composite scaffolds promoted bone regeneration bone defects.Our results indicated that the Wnt/β-catenin pathway was involved in the osteogenic effect.Therefore,Mg-1Ca/PCL composite scaffolds are expected to be a promising bone regeneration material for clinical application.Statement of significance:Bone tissue engineering scaffolds have promising applications in the regeneration of critical-sized bone defects.However,there remain many limitations in the materials and manufacturing methods used to fabricate scaffolds.This study shows that the developed Ma-1Ca/PCL composites provides scaffolds with suitable degradation rates and enhanced boneformation capabilities.Furthermore,the fused deposition modeling method allows precise control of the macroscopic morphology and microscopic porosity of the scaffold.The obtained porou

关键词： 3D printing Bone tissue engineering Magnesium Osteogenic Polycaprolactone Scaffold.

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Caliper-based precise positioning of the target(CALIPPOT)for transcranial magnetic stimulation without neuronavigation system

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General Psychiatry 2024年第2期37卷 311-314页

作者： yunsong Hu Rong Zeng Juan Yue Qiu Ge Hongxiao wang Zijian Feng Jue wang Yufeng Zang Center for Cognition and Brain Disorders The Affiliated Hospital of Hangzhou Normal UniversityHangzhouZhejiangChina Zhejiang Key Laboratory for Research in Assessment of Cognitive Impairments HangzhouZhejiangChina Institutes of Psychological Sciences Hangzhou Normal UniversityHangzhouZhejiangChina Transcranial Magnetic Stimulation Center Deqing Hospital of Hangzhou Normal UniversityDeqingZhejiangChina Institute of Sports Medicine and Health Chengdu Sport UniversityChengduSichuanChina Department of Neurology The Affiliated Hospital of Hangzhou Normal UniversityHangzhouZhejiangChina

To the editor:Transcranial magnetic stimulation(TMS)is a non-invasive brain modulation technique.One important usage of TMS is the transient interruption of cognitive brain function(also named virtual lesion)for investigating precisely where and when a specific cortical region contributes to a specific cognitive function.1 A more important usage of TMS is the treatment of brain disorders by repetitive TMS(rTMS).

关键词： stimulation technique. precise

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Research of cycloaliphatic epoxy resin and silicone rubber composite insulator interface based on four-electrode system and temperature rise model

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High Voltage 2023年第3期8卷 560-569页

作者： yunsong wang Yuhao Liu Hongwei Mei Min Xie Liming wang Shenzhen International Graduate School(SIGS) Tsinghua UniversityShenzhenChina Research Institute of Tsinghua Pearl River DeltaGuangzhouChina

Interface degradation between mandrel and sheath can cause a decrease in insulation performance and mechanical strength of composite insulators.In this study,the interface ageing properties of cycloaliphatic epoxy resin and silicone rubber composite insulator were compared.A water diffusion test was adopted to simulate the composite insulator ageing in a hot and humid environment.A four-electrode system was built to detect leakage current at different locations(mandrel,sheath and interface),which is an important basis for evaluating insulator performance.The ageing degree of insulator could be quantitatively characterised by leakage current change.It was found that the infiltrated moisture had a great effect on insulation performance.Based on the water absorption test result,the interface performance of two insulators was mainly influenced by their sheath sealing quality.As an auxiliary evaluation method,temperature rise during the test was recorded using an infrared camera.The experiment results showed that interface degradation was the main factor for the insulation performance decrease of silicone rubber composite insulators.However,insulation level reduction of the cycloaliphatic epoxy resin was caused by the wet sheath.In addition,a model for temperature rise of cycloaliphatic epoxy resin insulators was proposed based on good correspondence between sheath material and insulation.The model incorporated multiple processes such as ageing and heating of insulators,and it can predict the early temperature rise well.

关键词： insulator composite interface

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Highly Differentiated Target Detection under Extremely Low-Light Conditions Based on Improved YOLOX Model

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Computer Modeling in Engineering & Sciences 2024年第8期140卷 1507-1537页

作者： Haijian Shao Suqin Lei Chenxu Yan Xing Deng yunsong Qi School of Computer Jiangsu University of Science and TechnologyZhenjiang212003China Department of Electrical and Computer Engineering University of NevadaLas VegasNV89154USA Zhejiang Geely Automobile Research Institute Ningbo315336China

This paper expounds upon a novel target detection methodology distinguished by its elevated discriminatory efficacy,specifically tailored for environments characterized by markedly low luminance levels.Conventional methodologies struggle with the challenges posed by luminosity fluctuations,especially in settings characterized by diminished radiance,further exacerbated by the utilization of suboptimal imaging instrumentation.The envisioned approach mandates a departure from the conventional YOLOX model,which exhibits inadequacies in mitigating these challenges.To enhance the efficacy of this approach in low-light conditions,the dehazing algorithm undergoes refinement,effecting a discerning regulation of the transmission rate at the pixel level,reducing it to values below 0.5,thereby resulting in an augmentation of image contrast.Subsequently,the coiflet wavelet transform is employed to discern and isolate high-discriminatory attributes by dismantling low-frequency image attributes and extracting high-frequency attributes across divergent axes.The utilization of CycleGAN serves to elevate the features of low-light imagery across an array of stylistic variances.Advanced computational methodologies are then employed to amalgamate and conflate intricate attributes originating from images characterized by distinct stylistic orientations,thereby augmenting the model’s erudition potential.Empirical validation conducted on the PASCAL VOC and MS COCO 2017 datasets substantiates pronounced advancements.The refined low-light enhancement algorithm yields a discernible 5.9%augmentation in the target detection evaluation index when compared to the original imagery.Mean Average Precision(mAP)undergoes enhancements of 9.45%and 0.052%in low-light visual renditions relative to conventional YOLOX outcomes.The envisaged approach presents a myriad of advantages over prevailing benchmark methodologies in the realm of target detection within environments marked by an acute scarcity of luminosity.

关键词： Target detection extremely low-light wavelet transformation highly differentiated features YOLOX

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Degradation behaviors of Nabumetone and its metabolite during UV/monochloramine process:Experimental and theoretical study

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Journal of Environmental Sciences 2024年第8期142卷 103-114页

作者： Xiang Tu yunsong Bai Qing Fu Sheng Chang Kunfeng Zhang Yang Pan Ruiyang Xiao Yifu Fu Qi Zhang State Key Laboratory of Environmental Criteria and Risk Assessment State Environmental Protection Key Laboratory of Drinking Water Source ProtectionResearch Centre of Lake EnvironmentNational Engineering Laboratory for Lake Pollution Control and Ecological RestorationChinese Research Academy of Environmental SciencesBeijing 100012China School of Environmental Science and Engineering Suzhou University of Science and TechnologySuzhou 215009China Institute of Environmental Engineering School of Metallurgy and EnvironmentCentral South UniversityChangsha 410083China School of Forestry Northeast Forestry UniversityHarbin 150040China

This study investigated degradation behaviors of a nonsteroidal anti-inflammatory drug Nabumetone(NMT)and its major metabolite 6-methoxy-2-naphthylacetic acid(MNA)in the coupling process of ultraviolet and monochloramine(UV/NH2Cl).The second-order rate constants of the contaminants reacting with reactive radicals(HO·,Cl·,Cl_(2)·-,and CO_(3)·^(-))were determined by laser flash photolysis experiments.HO·and Cl·contributed predominantly with 52.3%and 21.7%for NMT degradation and 60.8%and 22.3%for MNA degradation.The presence of chlorides retarded the degradation of NMT,while promoted the destruction of MNA,which was ascribed to the photosensitization effects of MNA under UV irradiation.Density functional theory(DFT)calculations revealed that radical adduct formation(RAF)was dominant pathway for both HO·and Cl·reacting with the contaminants,and hydrogen atom transfer(HAT)preferred to occur on side chains of NMT and MNA.NMT reacted with NO_(2)·through single electron transfer(SET)with the second-order rate constant calculated to be 5.35×10^(7)(mol/L)^(-1)sec^(-1),and the contribution of NO_(2)·was predicted to be 13.0%of the total rate constant of NMT in pure water,which indicated that NO_(2)·played a nonnegligible role in the degradation of NMT.The acute toxicity and developmental toxicity of NMT were enhanced after UV/NH_(2)Cl treatment,while those of MNA were alleviated.The transformation products of both NMT and MNA exhibited higher mutagenicity than their parent compounds.This study provides a deep understanding of the mechanism of radical degradation of NMT and MNA in the treatment of UV/NH2Cl.

关键词： UV/NH_(2)Cl Reactive species Degradation kinetics Reaction mechanism Degradation products

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高效通信的在轨分布式高光谱图像处理

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测绘学报 2024年第4期53卷 589-598页

作者：谢卫莹王子璇李云松西安电子科技大学空天地一体化综合业务网全国重点实验室陕西西安710071

随着在轨遥感卫星数量的增加及高光谱成像技术的进步,能够获取到的高光谱数据量急剧增长,人类步入了大数据应用和数据驱动的科学发现时代。然而,如此大体量、大幅宽的高光谱数据导致了深度学习算法难以在单节点上学习和推理,为实时高效... 详细信息

随着在轨遥感卫星数量的增加及高光谱成像技术的进步,能够获取到的高光谱数据量急剧增长,人类步入了大数据应用和数据驱动的科学发现时代。然而,如此大体量、大幅宽的高光谱数据导致了深度学习算法难以在单节点上学习和推理,为实时高效的信息智能解译带来了极大的挑战。因此,需要综合多星资源分布式协同解析,以解决分块处理带来的块效应。然而,协同处理必然伴随着信息的交互与传输,为进一步降低传输信息量,需要对梯度进行压缩,以缓解分布式学习中的通信瓶颈。本文综合探讨了多种主流的高效通信梯度压缩算法,特别关注其在通信受限的在轨环境下的优劣,并展望了梯度压缩的发展趋势。通过广泛的试验对比,本文全面评估了多种梯度压缩方法在高光谱图像处理中的表现,试验证明不同方法的适用性和性能差异,为未来在实际应用中选择最合适的梯度压缩方法提供了有力的参考。

关键词：分布式学习梯度压缩高效通信高光谱图像在轨处理

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Catalytic wet oxidation of N,N-dimethyl formamide over ruthenium supported on CeO_2 and Ce_(0.7)Zr_(0.3)O_2 catalysts

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Journal of Rare Earths 2019年第3期37卷 265-272页

作者： Jiawen Gong Dongzhi Li Li wang wangcheng Zhan Yanglong Guo yunsong wang Yun Guo Key Laboratory for Advanced Materials and Research Institute of Industrial Catalysis School of Chemistry & Molecular Engineering East China University of Science and Technology

A series of Ru supported on CeO_2 and Ce_(0.7)Zr_(0.3)O_2(CeZrO) was prepared by incipient-wet impregnation method and investigated in the catalytic wet oxidation of N,N-dimethyl formamide(DMF) in batch reactor. The physicochemical property of the catalysts was characterized by Brunauer-Emmett-Teller(BET), X-ray diffraction(XRD), H_2 temperature-programmed reduction(H_2-TPR), X-ray photoelectron spectroscopy(XPS) and thermogravimetry(TG). Compared with 3%Ru/CeO_2, 3%Ru/Ce_(0.7)Zr_(0.3)O_2 catalyst exhibits much higher performance for DMF degradation due to the promotion of Ru dispersion and the transfer of active oxygen, and 99% DMF conversion and 97% COD elimination are obtained at 453 K,2.5 MPa oxygen pressure after 5 h. The reaction mechanism of DMF degradation was suggested. The carbonaceous species deposition and oxidation of Ru can be responsible for catalyst deactivation. And the catalyst activity can be recovered by air calcination and H_2 reduction.

关键词： Catalytic wet oxidation N,N-dimethyl formamide Ru Degradation Catalyst deactivation and regeneration Rare earths

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萨迦穹隆北侧苦堆淡色花岗岩的形成机制及对喜马拉雅造山带演化的约束

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岩石学报 2024年第5期40卷 1647-1668页

作者：王宏立范云松张进江古大祥林超王晓先北京大学地球与空间科学学院造山带与地壳演化教育部重点实验室北京100871 紫金矿业集团股份有限公司厦门361000 应急管理部国家自然灾害防治研究院北京100085

萨迦穹隆位于北喜马拉雅片麻岩穹隆带中部。野外构造解析表明,萨迦穹隆北侧剖面可划分为由浅变质特提斯喜马拉雅沉积岩系构成上构造层,糜棱状石榴石片岩构成中构造层,糜棱状的正片麻岩和副片麻岩复合体构成下构造层(穹隆核部)。从上构... 详细信息

萨迦穹隆位于北喜马拉雅片麻岩穹隆带中部。野外构造解析表明,萨迦穹隆北侧剖面可划分为由浅变质特提斯喜马拉雅沉积岩系构成上构造层,糜棱状石榴石片岩构成中构造层,糜棱状的正片麻岩和副片麻岩复合体构成下构造层(穹隆核部)。从上构造层向中构造层变质变形程度连续增高,但没有明显的拆离断层分隔,中构造层与下构造层被拆离面分隔。不同构造层次都具有统一的近北倾的线理和面理,运动学特征都指示了上盘向北的伸展剪切,表明萨迦穹隆北侧剖面的剪切变形可能代表了藏南拆离系在北喜马拉雅穹隆的出露。苦堆白云母花岗岩和石榴石花岗岩以顺层(面理化)和切层形式侵位于下构造层片麻岩中,呈现明显的同构造变形特征。两类淡色花岗岩具有相似的全岩主量元素特征:高的SiO_(2)(73.26%~74.87%)、Al_(2)O_(3)(14.37%~15.03%)和CaO(1.51%~1.81%),A/CNK指数在1.08~1.16之间。白云母花岗岩表现出较高的Ba(398×10^(-6)~739×10^(-6))和Sr(135×10^(-6)~165×10^(-6)),低的Rb(180×10^(-6)~201×10^(-6))和Rb/Sr比(1.22~1.34),变化的Eu/Eu*(0.76~1.47),轻重稀土分异明显,球粒陨石标准化稀土元素配分图呈明显右倾趋势。石榴石花岗岩表现出低的Ba(204×10^(-6)~282×10^(-6))和Sr(81×10^(-6)~103×10^(-6)),较高的Rb(243×10^(-6)~281×10^(-6))和Rb/Sr比(2.37~3.22),明显的Eu负异常(Eu/Eu*=0.46~0.66),轻重稀土分异不明显,球粒陨石标准化稀土元素配分图呈“海鸥型”。苦堆淡色花岗岩的初始87 Sr/86 Sr比为0.762732~0.766668,ε_(Nd)(t)为-13.1~-12.5,与大喜马拉雅结晶岩系一致。年代学结果表明苦堆白云母花岗岩形成于约27Ma,石榴石花岗岩形成于27.5~28.1Ma。根据岩相学、年代学、运动学、地球化学等分析,认为苦堆白云母花岗岩起源于大喜马拉雅结晶岩系白云母水致熔融,源岩为大喜马拉雅较深位置的变杂砂岩,石榴石花岗岩是白云母花岗岩进一步结晶分异的结果。同构造的苦堆淡色花岗岩反映了渐新世早期藏南拆离系已经启动,藏南拆离系的启动诱发了地壳深部的白云母水致熔融,形成淡色花岗岩,并沿着藏南拆离系侵位。喜马拉雅造山带在渐新世(集中于28~26Ma)已从碰撞增厚转换为代表松弛与折返的伸展构造背景。

关键词：苦堆岩体淡色花岗岩藏南拆离系地球化学喜马拉雅造山带

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