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Atomistic study on the microscopic mechanism of grain boundary embrittlement induced by small dense helium bubbles in iron

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Nuclear Science and Techniques 2024年第3期35卷 84-95页

作者： Lei Peng Yong-Jie Sun Jing-yi Shi yi-fei liu Shang-Ming Chen liu-liu Li State Key Laboratory of Particle Detection and Electronics University of Science and Technology of ChinaHefei 230026China School of Nuclear Science and Technology University of Science and Technology of ChinaHefei 230027China Science and Technology on Reactor System Design Technology Laboratory Nuclear Power Institute of ChinaChengdu 610213China

The helium bubbles induced by 14 MeV neutron irradiation can cause intergranular fractures in reduced activation ferritic martensitic steel,which is a candidate structural material for fusion *** order to elucidate the susceptibility of different grain boundaries(GBs)to helium-induced embrittlement,the tensile fracture processes of 10 types of GBs with and without helium bubbles in body-centered cubic(bcc)iron at the relevant service temperature of 600 K were investigated via molecular dynamics *** results indicate that in the absence of helium bubbles,the GBs studied here can be classified into two distinct categories:brittle GBs and ductile *** atomic scale analysis shows that the plastic deformation of ductile GB at high temperatures originates from complex plastic deformation mechanisms,including the Bain/Burgers path phase transition and deformation twinning,in which the Bain path phase transition is the most dominant plastic deformation ***,the presence of helium bubbles severely inhibits the plastic deformation channels of the GBs,resulting in a significant decrease in elongation at *** bubble-decorated GBs,the ultimate tensile strength increases with the increase in the misorientation ***,the coherent twin boundary∑3{112}was found to maintain relatively high fracture strength and maximum failure strain under the influence of helium bubbles.

关键词： Helium bubble Grain boundary Embrittlement Reduced activation ferritic martensitic steel Molecular dynamics Bain path

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Grain boundary engineering for enhancing intergranular damage resistance of ferritic/martensitic steel P92

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Nuclear Science and Techniques 2024年第5期35卷 186-199页

作者： Lei Peng Shang-Ming Chen Jing-yi Shi Yong-Jie Sun yi-fei liu yin-Zhong Shen Hong-Ya He Hui-Juan Wang Jie Tian State Key Laboratory of Particle Detection and Electronics University of Science and Technology of ChinaHefei 230026China School of Nuclear Science and Technology University of Science and Technology of ChinaHefei 230027China School of Materials Engineering Shanghai University of Engineering Science333 Long Teng RoadShanghai 201620China Experimental Center of Engineering and Material Science University of Science and Technology of ChinaHefei 230026China

Ferritic/martensitic(F/M)steel is widely used as a structural material in thermal and nuclear power ***,it is susceptible to intergranular damage,which is a critical issue,under service *** this study,to improve the resistance to intergranular damage of F/M steel,a thermomechanical process(TMP)was employed to achieve a grain boundary engineering(GBE)microstructure in F/M steel *** TMP,including cold-rolling thickness reduction of 6%,9%,and 12%,followed by austenitization at 1323 K for 40 min and tempering at 1053 K for 45 min,was applied to the as-received(AR)P92 *** prior austenite grain(PAG)size,prior austenite grain boundary character distribution(GBCD),and connectivity of prior austenite grain boundaries(PAGBs)were *** to the AR specimen,the PAG size did not change *** fraction of coincident site lattice boundaries(CSLBs,3≤Σ≤29)and Σ3^(n) boundaries along PAGBs decreased with increasing reduction ratio because the recrystallization fraction increased with increasing reduction *** PAGB connectivity of the 6%deformed specimen slightly deteriorated compared with that of the AR ***,potentiodynamic polarization studies revealed that the intergranular damage resistance of the studied steel could be improved by increasing the fraction of CSLBs along the PAGBs,indicating that the TMP,which involves low deformation,could enhance the intergranular damage resistance.

关键词： Grain boundary engineering Ferritic/martensitic steel Prior austenite grain boundary character distribution Grain boundary connectivity Intergranular damage resistance

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Microstructure quantification of Cu-4.7Sn alloys prepared by two-phase zone continuous casting and a BP artificial neural network model for microstructure prediction

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稀有金属：英文版 2019年第12期38卷 1124-1130页

作者： Ji-Hui Luo Xue-Feng liu Zhang-Zhi Shi yi-fei liu School of Materials Science and Engineering University of Science and Technology BeijingBeijing 100083China Beijing Laboratory of Metallic Materials and Processing for Modem Transportation University of Science and Technology BeijingBeijing 100083China

Microstructures of Cu-4.7Sn(%) alloys prepared by two-phase zone continuous casting(TZCC)technology contain large columnar grains and small grains.A compound grain structure,composed of a large columnar grain and at least one small grain within it,is observed and called as grain-covered grains(GCGs).Distribution of small grains,their numbers and sizes as well as numbers and sizes of columnar grains were characterized quantitatively by metallographic *** propagation(BP) artificial neural network was employed to build a model to predict microstructures produced by different processing *** of the model are five processing parameters,which are temperatures of melt,mold and cooling water,speed of TZCC,and cooling *** of the model are nine microstructure quantities,which are numbers of small grains within columnar grains,at the boundaries of the columnar grains,or at the surface of the alloy,the maximum and the minimum numbers of small grains within a columnar grain,numbers of columnar grains with or without small grains,and sizes of small grains and columnar *** model yields precise prediction,which lays foundation for controlling microstructures of alloys prepared by TZCC.

关键词： Two-phase zone continuous casting Cu-Sn alloy Grains-covered grains Microstructure quantification Back propagation artificial neural network

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A highly efficient humidity sensor based on lead(Ⅱ) coordination polymer via in-situ decarboxylation and hydrolysis synthesis

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Rare Metals 2022年第5期41卷 1652-1660页

作者： Hao Dong Le-Xi Zhang Heng Xu Yan-Yan yin yi-fei liu Li-Jian Bie School of Materials Science and Engineering Tianjin Key Laboratory for Photoelectric Materials and DevicesKey Laboratory of Display Materials and Photoelectric Devices(Ministry of Education)National Demonstration Center for Experimental Function Materials EducationTianjin University of TechnologyTianjin 300384China Department of Environmental Science and Engineering Nankai University Binhai CollegeTianjin 300270China

Function-oriented design of coordination polymers is emerging as an attracting topic to explore their practical applications, e.g., gas/humidity sensing. However,the successful synthesis of new coordination polymers showing splendid sensing property is an urgent need in fields of materials and sensors, yet still at the initial *** this contribution, a new one-dimensional(1D) coordination polymer with formula of [Pb(TAA)(BA)(H_(2)O)]_(n)(namedasPbL,HTAA = 3-thiopheneaceticacid,HBA = benzoic acid) has been successfully synthesized by a hydrothermal method, which involves in-situ synthesis of both decarboxylation and hydrolysis. As an impedimetric humidity sensing material, this coordination polymer exhibits excellent humidity sensing performance including high response, fast response, small hysteresis, and good repeatability. In the total relative humidity range(11%–97%) at room temperature, it is worth noting that the sensitivity of the humidity sensor is as high as 1.18×10^(4),the response time is only 2 s, and the max humidity hysteresis is as small as 1.8%. At last, we discussed the sensing mechanism using the alternating current(AC) impedance technique at various relative humidity.

关键词： Lead Coordination polymer In-situ synthesis Humidity sensor

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Impact of flow rate on dynamic imbibition in fractured tight sandstone cores

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Petroleum Science 2022年第6期19卷 2895-2904页

作者： yi-fei liu Cai-Li Dai Chen-Wei Zou Qing You Ming-Wei Zhao Guang Zhao Yong-Peng Sun Shandong Key Laboratory of Oilfield Chemistry(China University of Petroleum(East China)) Qingdao266580ShandongChina Key Laboratory of Unconventional Oil&Gas Development(China University of Petroleum(East China)) Ministry of EducationQingdao266580ShandongChina School of Energy Resources China University of GeosciencesBeijing100083China

Dynamic imbibition,which is significantly affected by flow rate,plays an important role in the development of tight *** study investigated the impact of flow rate on dynamic imbibition in fractured tight sandstone cores via online nuclear magnetic resonance core-flooding *** oil expulsion efficiency and capillary number of multiscale pores were quantitatively analyzed to elucidate the influence of flow rate on the oil recovery during dynamic *** pores of the cores used were divided into micropores(0.01-1.00 μm in diameter),mesopores(1.00-30.00 μm in diameter),and macropores(30.00-400.00 μm in diameter) by matching the T_(2)spectrum and the mercury intrusion *** volume proportion of micropores was 52.0%,and that of macropores was 19.0%.The total oil recovery of the core was found to reach 29.8% at the optimal flow rate of 0.1 mL/*** the optimal flow rate,the oil recovery of micropores reached 50.4%,followed by that of macropores(28.6%),and that of mesopores was the lowest(15.8%).The oil expulsion efficiency,the capillary number,and the contribution to total oil recovery of micropores significantly increased with the decrease in flow rate,while those of macropores *** was caused by the synergy of capillary force and displacement *** dynamic imbibition at a low flow rate,the oil in micropores was effectively expelled driven by capillary force,and the effect of displacement pressure was weak,leading to large amounts of remaining oil trapped in *** the contrary,when the flow rate was too high,large amounts of remaining oil would be trapped in *** at a moderate flow rate did the capillary force and displacement pressure both have significant effects on oil expulsion,and the oil in different sized pores was effectively expelled,thus generating a relatively high total oil recovery.

关键词： Tight oil Dynamic imbibition Flow rate Oil recovery Nuclear magnetic resonance

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Self-assembly of perovskite nanocrystals:From driving forces to applications

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Journal of Energy Chemistry 2024年第1期88卷 561-578,I0013页

作者： yi Li fei Zhang School of Chemical Engineering and Technology Tianjin UniversityTianjin 300072China Collaborative Innovation Center of Chemical Science and Engineering(Tianjin) Tianjin 300072China

Self-assembly of metal halide perovskite nanocrystals(NCs)into superlattices can exhibit unique collective properties,which have significant application values in the display,detector,and solar cell *** review discusses the driving forces behind the self-assembly process of perovskite NCs,and the commonly used self-assembly methods and different self-assembly structures are ***,we summarize the collective optoelectronic properties and application areas of perovskite superlattice ***,we conclude with an outlook on the potential issues and future challenges in developing perovskite NCs.

关键词： Self-assembly Metal halide perovskite Nanocrystals Driving forces

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Archean (about 2500 Ma) anatexis in eastern North China Block

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China Geology 2021年第2期4卷 215-229页

作者： Si-hong Jiang Leon Bagas yi-fei liu Li-li Zhang Ministry of Natural Resources Key Laboratory of Metallogeny and Mineral Assessment Institute of Mineral ResourcesChinese Academy of Geological SciencesBeijing 100037China Centre for Exploration Targeting The University of Western AustraliaCrawleyWA 6009Australia

Two Neoarchean alkaline feldspar-rich granites sourced from partially melted granulite-facies granodioritic orthogneiss have been here recognised in the eastern part of the North China Block(NCB).These poorly foliated granites have previously been assumed to be Mesozoic in age and never dated,and so their significance has not been recognised until *** first granite(AG1)is a porphyritic syenogranite with megacrystic K-feldspar,and the second(AG2)is a quartz syenite with perthitic *** from the granites yield LA-ICP-MS U-Pb ages of 2499±10 Ma(AG1),and 2492±28 Ma(AG2),which are slightly younger than the granodioritic orthogneiss that they intrude with a crystallisation U-Pb age of 2537±34 *** younger granites have higher assays for SiO_(2)(71.91%for AG1 and 73.22%for AG2)and K_(2)O(7.52%for AG1 and 8.37%for AG2),and much lower assays for their other major element than the granodioritic *** of the granodioritic orthogneiss and granite samples have similar trace element patterns,with depletion in Th,U,Nb,and Ti and enrichment in Rb,Ba,K,La,Ce,and *** indicates that the granites are derived from the orthogneiss as partial *** they exhibit a similar REE pattern,the granites have much lower total REE contents(30.97×10^(−6) for AG1,and 25.93×10^(−6) for AG2),but pronounced positive Eu anomalies(Eu/Eu^(*)=8.57 for AG1 and 27.04 for AG2).The granodioritic orthogneiss has an initial ^(87)Sr/^(86)Sr ratio of 0.70144,εNd(t)value of 3.5,and εHf(t)values ranging from−3.2 to+*** orthogneiss is a product of fractional crystallisation from a dioritic magma,which was derived from a mantle source contaminated by melts derived from a felsic *** contrast,the AG1 sample has an initial ^(87)Sr/^(86)Sr ratio of 0.6926 that is considered too low in value,εNd(t)value of 0.3,andεHf(t)values between+0.57 and+3.82;whereas the AG2 sample has an initial ^(87)Sr/^(86)Sr ratio of 0.70152,εNd(t)value of 1.3,andεHf(t)values between+0.5 and+***

关键词： Neoarchean granodioritic orthogneiss Granulite-facies Neoarchean granite Isotope disequilibrium Geological survey engineering North China Block

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Experimental investigation on migration and retention mechanisms of elastic gel particles(EGPs)in pore-throats using multidimensional visualized models

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Petroleum Science 2022年第5期19卷 2374-2386页

作者： yi-fei liu Chen-Wei Zou Xu-Guang Lou Ming-Wei Gao Guang Zhao Ming-Wei Zhao Cai-Li Dai Shandong Key Laboratory of Oilfield Chemistry(China University of Petroleum(East China)) Qingdao266580PR China Key Laboratory of Unconventional Oil&Gas Development(China University of Petroleum(East China)) Ministry of EducationQingdao266580PR China China Southern Petroleum Exploration&Development Corporation HaikouHainan570216People's Republic of China

Knowledge of migration and retention mechanisms of elastic gel particles(EGPs)in pore-throats is essential for the effective application of EGPs as a smart sweep improvement and profile control agent for enhanced oil recovery(EOR).The matching coefficient(defined as the ratio of particle size to pore-throat size)is used to investigate its influence on migration,retention and profile control performance of EGPs.A 1-D continuous pore-throat visualization model(PTVM),a 2-D heterogeneous PTVM and a 3-D heterogeneous core model were constructed and used to investigate pore-scale migration,retention and controlling mechanism of migration and retention characteristics on EGPs profile *** results of the 1-D continuous PTVM indicated that while the matching coefficient was in the optimal range(i.e.,0.20-0.32),the EGPs could not only smoothly migrate to the deeper pore-throats,but also form stable retention in the pores to resist the erosion of injected water,which was conducive to the effective indepth profile *** results of the 2-D heterogeneous PTVM verified that the sweep efficiency in low-permeability regions could be significantly improved by in-depth migration and stable retention of EGPs in the pore-throats with an optimal matching coefficient(0.29),which was much better than that in cases with a smaller matching coefficient(0.17)or an excessive matching coefficient(0.39).Moreover,the NMR displacement experiments of 3-D heterogeneous cores were carried out to simulate the EGPs profile control in actual reservoir porous *** images and T2 spectrum curves of crude oil showed that EOR in the low-permeability layer was highest(56.1%)using EGPs profile control with an optimal matching coefficient,attributing to the in-depth migration and stable retention of EGPs.

关键词： Enhanced oil recovery Elastic gel particles Matching coefficient In-depth profile control Pore-throat visualization models

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Three-dimensionally oriented organization of hexagonal MIL-96 microplates toward superior film microstructure

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Chinese Journal of Chemical Engineering 2024年第8期72卷 69-73页

作者： Sixing Chen Xinmiao Jin Yuyang Wu Taotao Ji fei Wang yi liu State Key Laboratory of Fine Chemicals Frontiers Science Center for Smart MaterialsSchool of Chemical EngineeringDalian University of TechnologyDalian 116024China State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of MatterChinese Academy of SciencesFuzhou 350002China Dalian Key Laboratory of Membrane Materials and Membrane Processes Dalian University of TechnologyDalian 116024China

Preferential orientation control of metal—organic framework(MOF)films is advantageous for maximizing pore uniformity and minimizing grain-boundary ***,the preparation of MOF films with both in-plane and out-of-plane orientations remains a grand *** this study,we reported the preparation of three-dimensionally oriented MIL-96 layers through combining morphology control of MIL-96 seeds with addition of polyvinylpyrrolidone surfactants and arachidonic *** three-dimensionally oriented MIL-96 film was readily obtained through in-plane epitaxial *** is anticipated that the aforementioned protocol can be effective for obtaining diverse MOF films with a three-dimensionally oriented organization.

关键词： Metaleorganic framework Film Orientation Epitaxial growth Morphological control

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Pt nanoclusters modified porous g-C_(3)N_(4)nanosheets to significantly enhance hydrogen production by photocatalytic water reforming of methanol

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Chinese Journal of Chemical Engineering 2024年第2期66卷 40-50页

作者： yi-fei Liang Jin-Rong Lu Shang-Kun Tian Wen-Quan Cui Li liu Hebei Provincial Key Laboratory of Environmental Photocatalytic and Electrocatalytic Materials College of Chemical EngineeringNorth China University of Science and TechnologyTangshan 063210China

For the use of green hydrogen energy,it is crucial to have efficient photocatalytic activity for hydrogen generation by water reforming of methanol under mild *** attention has been paid to gC_(3)N_(4)as a promising photocatalyst for the generation of *** improve the separation of photogenerated charge,porous nanosheet g-C_(3)N_(4)was modified with Pt nanoclusters(Pt/g-C_(3)N_(4))through impregnation and following photo-induced *** catalyst showed excellent photocatalytic activity of water reforming of methanol fo r hydrogen production with a 17.12 mmol·g^(-1)·h^(-1)rate at room temperature,which was 311 times higher than that of the unmodified g-C_(3)N_(4).The strong interactions of Pt-N in Pt/g-C_(3)N_(4)constructed effective electron transfer channels to promote the separation of photogenerated electrons and holes *** addition,in-situ infrared spectroscopy was used to investigate the intermediates of the hydrogen production reaction,which proved that methanol and water eventually turn into H_(2)and CO_(2)via formaldehyde and *** study provides insights for understanding the photocatalytic hydrogen production in the water reforming of methanol.

关键词： Water reforming of methanol Photocatalysis g-C_(3)N_(4) Pt nanoclusters Hydrogen production

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