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A new technology for treating waste incineration fly ash by shaft furnace

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Journal of Iron and Steel Research International 2021年第7期28卷 773-784页

作者： Cui wang Long-zhi Chen Zheng-jian Liu Yang Li yao-zu wang Ke-xin Jiao State Key Laboratory of Advanced Metallurgy University of Science and Technology BeijingBeijing 100083China School of Metallurgical and Ecological Engineering University of Science and Technology BeijingBeijing 100083China

At present,lots of municipal solid wastes(MSWs)are treated by incineration technology,which produces a large amount of fly ash that needs to be treated innocuously.A new method of using metallurgical shaft furnace to treat the MSW fly ash was thus proposed,and some research was done for this ***,the basic physical properties of MSW fly ash were analyzed,and then,the briquetting experiment and melting treatment of MSW fly ash were *** the process of briquet-ting,the influence of different factors(water content,cement content,forming pressure and curing time)on the compressive strength of the briquettes was *** results showed that with the increase in water content,cement content,forming pressure and curing time,the compressive strength of the briquettes increased ***,the compressive strength of the briquettes showed a downward trend when these values exceeded a specific *** the melting experiment,it was found that some heavy metals(such as Cr,Be and Ba)could be solidified in the slag when the fly ash was treated at 1450℃ for 50 min,and the leaching toxicity of heavy metals was lower than the landfill standard of waste in *** the same time,the decomposition rate of dioxins in fly ash reached 99.66%after melting treatment.

关键词： Fly ash Shaft furnace Compressive strength Melting treatment Heavy metal Dioxin

Softening–melting behavior of mixed burden based on low-magnesium sinter and fluxed pellets

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International Journal of Minerals,Metallurgy and Materials 2021年第4期28卷 621-628页

作者： Gui-lin wang Jian Kang Jian-liang Zhang yao-zu wang Zhi-yu wang Zheng-jian Liu Chen-yang Xu School of Metallurgical and Ecological Engineering University of Science and Technology BeijingBeijing 100083China School of Chemical Engineering The University of QueenslandSt LuciaQLD 4072Australia Institute of Artificial Intelligence University of Science and Technology BeijingBeijing 100083China Baosteel Zhanjiang Iron and Steel Co. Ltd.Zhanjiang 524072China

A low MgO content in sinter is conducive to reduce the MgO content in blast furnace *** study investigated the effect of MgO content in sinter on the softening–melting behavior of the mixed burden based on fluxed *** the MgO content increased from 1.31 wt% to 1.55 wt%, the melting temperature of sinter increased to 1521℃.Such an increase was due to the formation of the high-meltingpoint slag *** reduction degradation index of sinter with 1.31 wt% MgO content was better than that of *** initial softening temperature of the mixed burden increased from 1104 to 1126℃ as MgO content in sinter increased from 1.31 wt% to 1.55 wt%, and the melting temperature decreased from 1494 to 1460℃.The permeability index(S-value) of mixed burden decreased to 594.46 kPa·℃ under a high MgO content with 1.55 wt%, indicating that the permeability was *** slag phase composition of burden was mainly akermarite(Ca_(2)MgSiO_(7)) when the MgO content in sinter was 1.55 wt%.The melting point of akermarite is 1450℃, which is lower than other phases.

关键词： magnesia softening–melting behavior low-magnesium sinter fluxed pellets slag

Corrosion resistance properties of colored zirconium conversion coating and powder coating on cold-rolled steel

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Rare Metals 2023年第3期42卷 1005-1010页

作者： Ai-Hua Wu yao-zu wang Tong-Kuan Xu Zhi Li Sheng-Ji Luan Feng-zuo Qu Shenzhen Key Laboratory of Environment Simulation and Pollution Control PKU-HKUST Shenzhen-HongKong InstitutionShenzhen 518057China Faculty of Light Industry and Chemical Engineering Dalian Polytechnic UniversityDalian 116034China

Jiuhe Corporation developed a new surface pretreatment for producing a phosphate-free and colored zirconium conversion coating on cold-rolled steel(CRS).Scanning electron microscopy(SEM)and energy-dispersive spectroscopy(EDS)were applied to study the surface morphology and elemental composition of the golden yellow-colored conversion *** trochemic al impedance spectroscopy(EIS)was used to investigate the electrochemical performance of the conversion coatings with different *** corrosion resistance properties of the powder coatings were characterized using the neutral salt spray test(NSS)and the tape adhesion *** EIS and NSS results demonstrate that the colored zirconium conversion coatings exhibit excellent corrosion resistance properties compared with the bare *** golden yellow-colored conversion coating has a maximum EIS value(748Ω·cm^(2))and achieves 0 mm degree of corrosion,as stipulated by EN ISO *** paper proposes a hypothesis concerning the ZrO_(2)-(β-FeOOH)-polymer conversion reaction to explain the color changes.

关键词： Surface pretreatment Colored conversion coating Zirconium oxide Powder coating Corrosion protection

Interface interaction between SiO_(2) and magnetite under high temperature:particle migration and inhibition mechanism

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Journal of Iron and Steel Research International 2024年第3期31卷 561-572页

作者： yao-zu wang Jian-liang Zhang Qiang Cheng Hui-qing Jiang Zheng-jian Liu Yu-bo Tan School of Intelligent Science and Technology University of Science and Technology BeijingBeijing 100083China School of Metallurgical and Ecological Engineering University of Science and Technology BeijingBeijing 100083China School of Advanced Engineering University of Science and Technology BeijingBeijing 100083China

Silicon is one of the main gangue components in iron ore,usually in the form of quartz and *** studies have shown that SiO_(2) has a two-sided effect on the consolidation of pellets during high-temperature oxidation roasting of ***,it is very difficult to capture the structural evolution and migration mechanisms during high-tem-perature roasting process by existing experimental ***,the influence of SiO_(2) on the consolidation behavior of magnetite was studied through a series of roasting experiments and molecular dynamic *** results show that the consolidation index and particle growth index decrease with the increase in SiO_(2) content in the *** 1573 K,the liquid phase promotes the recrystallization growth of hematite at high *** dynamic study shows that it is difficult for quartz SiO_(2) to form sintering neck with Fe_(2)O_(3).When the calcination temperature is higher than 1400 K,the Fe_(2)O_(3)-Fe_(2)SiO_(4) system produces a considerable sintering neck structure after *** atomic migration ability of Fe_(2)SiO_(4) is much higher than that of Fe_(2)O_(3).The higher atomic migration ability of Fe_(2)SiO_(4) is the main reason for the formation of the sintering neck.

关键词： Sintering neck Crystal growth Consolidation Molecular dynamics SiO_(2)

Characteristics of combustion zone and evolution of mineral phases along bed height in ore sintering

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International Journal of Minerals,Metallurgy and Materials 2017年第10期24卷 1087-1095页

作者： yao-zu wang Jian-liang Zhang Zheng-jian Liu Ya-peng Zhang Dong-hui Liu Yi-ran Liu School of Metallurgical and Ecological Engineering University of Science and Technology Beijing Beijing 100083 China

Quantitative parameters of bed combustion, including the thickness of the combustion zone(TCZ), the maximum temperature of the combustion zone(MTCZ), and the bed shrinkage, were characterized through a series of sinter pot tests in transparent quartz pots. The results showed that TCZ first ascended and then descended as the sintering process proceeded. The sintering process was divided into four stages according to the variation rate of the TCZ. A "relative-coordinate" method was developed to obtain the actual reaction temperature of sinter along the height direction. With increasing the sintering temperature, the reactants transformed and entered into liquid phases. The mineral composition and microstructure of the sinter were characterized through X-ray diffraction and scanning electron microscopy–energy-dispersive X-ray spectroscopy. Liquid phases with greater Fe and Al contents were more likely to form acicular-like silico-ferrite of calcium and aluminum after crystallization because of the outward spread of Al, which led to a better fluidity of the liquid. An evolution mechanism of "solid-state reaction—liquid phases formation—crystallization" of the mineral phases is proposed.

关键词： flame front mineral phases sintering evolution mechanism transparent quartz pots

Magnesium-containing pellet regulating blast furnace ferrous burden interaction:softening-melting behavior and mechanism

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Journal of Iron and Steel Research International 2024年第7期31卷 1623-1635页

作者： Li-ming Ma Jian-liang Zhang yao-zu wang Xiao-yong Ma Gui-lin wang Zhuo Li Hui-qing Jiang Zheng-jian Liu School of Metallurgical and Ecological Engineering University of Science and Technology BeijingBeijing 100083China School of Intelligence Science and Technology University of Science and Technology BeijingBeijing 100083China Lingyuan Iron and Steel Group Co. Lingyuan 122500LiaoningChina

MgO participates in all stages of sintering,pelletizing,and blast furnace ironmaking,and synergistically optimizing the distribution of MgO in ferrous burden can effectively enhance the interaction within the ferrous burdens and optimize the softening-melting properties of the mixed ***-containing pellets mixed with low-MgO sinter or mixed with high-MgO sinter in the blast furnace ferrous burden structure have opposite softening-melting performance *** the structure of the ferrous burden is magnesium-containing pellets mixed with low-MgO sinter,the magnesium-containing pellets can enhance the interaction of the ferrous burden in the process of softening-melting,which can optimize the composition of the slag phase and improve the slag *** the structure of the ferrous burden is magnesium-containing pellets mixed with high-MgO sinter,the magnesium-containing pellets weaken the interaction of the ferrous burden in the process of softening-melting,increase the content of the high melting point solid-phase particles in the slag,lead to an increase in the viscosity of the slag and difficult separation of the slag and iron,and decrease the permeability of the charge ***,to ensure good permeability of the mixed burden,the following measures are suggested:optimizing the MgO distribution of the ferrous burden,reducing the MgO content of the sinter to 1.96 wt.%,increasing the MgO content of the pellets to 1.03-1.30 wt.%,controlling the MgO/Al_(2)O_(3) ratio of the mixed burden within 1.15-1.32,narrowing the position of the cohesive zone,and maintaining an S value(permeability index)of approximately 150 kPa℃.

关键词： Ironmaking Ferrous burden Softening-melting property Interaction Permeability Slag

Proposing a machine learning approach to analyze and predict basic high-temperature properties of iron ore fines and its factors

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Journal of Iron and Steel Research International 2024年第5期31卷 1082-1094页

作者： Qing-ke Sun yao-zu wang Jian-liang Zhang Zheng-jian Liu Le-le Niu Chang-dong Shan Yun-fei Ma Institute of Artificial Intelligence University of Science and Technology BeijingBeijing100083China School of Intelligence Science and Technology University of Science and Technology BeijingBeijing100083China School of Metallurgical and Ecological Engineering University of Science and Technology BeijingBeijing100083China

The basic high-temperature properties of iron ore play a crucial role in optimizing sintering and ore blending,but the testing process for these properties is complex and has significant lag time,which cannot meet the actual needs of ore blending.A prediction model for the basic high-temperature properties of iron ore fines was thus proposed based on a combination of machine learning algorithms and genetic ***,the prediction accuracy of different machine learning models for the basic high-temperature properties of iron ore fines was ***,a random forest model optimized by genetic algorithms was built,further improving the prediction accuracy of the *** test results show that the random forest model optimized by genetic algorithms has the highest prediction accuracy for the lowest assimilation temperature and liquid phase fluidity of iron ore,with a determination coefficient of 0.903 for the lowest assimilation temperature and 0.927 for the liquid phase fluidity after *** trained model meets the fluctuation requirements of on-site testing and has been successfully applied to actual production on site.

关键词： Iron ore Basic high-temperature property Machine learning Random forest Genetic algorithm

O_(2) adsorption on Fe_(3)O_(4) (110) surface and effect of gangue element Al doping: combined study of binding experiment and ab initio molecular dynamics

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Journal of Iron and Steel Research International 2024年第4期31卷 810-827页

作者： Zheng-jian Liu Hui-qing Jiang yao-zu wang Jian-liang Zhang Hong-mei Qiao An-yang Zheng Fang-yu Guo School of Metallurgical and Ecological Engineering University of Science and Technology BeijingBeijing 100083China School of Intelligence Science and Technology University of Science and Technology BeijingBeijing 100083China Beijing Shougang Co. Ltd.Qian'an 064404HebeiChina Department of Physics National University of Defense TechnologyChangsha 410128HunanChina

At high temperature,the chemical reaction mechanism at the interface of magnetite and the influence mechanism of gangue element Al on the oxidation performance of magnetite are not *** addition,due to the limitation of existing experimental equipment,it is difficult to clarify the interface reaction mechanism in the oxidation process and the influence mechanism of Al on the surface oxidation reaction of Fe_(3)O_(4) at an atomic scale at high *** surface oxidation reaction mechanism of magnetite and the influence mechanism of Al on the oxidation of magnetite were studied by experiments and AIMD(ab initio molecular dynamics).The experimental results show that the existence of Al_(2)O_(3) will reduce the initial oxidation temperature and comprehensive oxidation performance of *** AIMD results show that aluminum can accelerate the interface reaction rate of Fe_(3)O_(4) in the high-temperature oxidation atmosphere,but the strong Al-O binding ability is not conducive to the transfer of O atoms in the oxidation process.

关键词： Ironmaking Magnetite oxidation Interface reaction Adsorption-Gangue aluminum AIMD

Synergistic reaction behavior of pyrolysis and reduction of briquette prepared by weakly caking coal and metallurgical dust

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Journal of Iron and Steel Research International 2023年第7期30卷 1367-1380页

作者： Zheng-jian Liu Ming-hui Cao Jian-liang Zhang Run-sheng Xu yao-zu wang Ji-yong Yu Yu-chen Zhang School of Metallurgical and Ecological Engineering University of Science and Technology BeijingBeijing 100083China State Key Laboratory of Advanced Metallurgy University of Science and Technology BeijingBeijing 100083China

Co-carbonization of weakly caking coal and zinc-containing dust to prepare highly reactive ferro-coke and collaboratively recover zinc powder is one of the feasible ways for steel enterprises to recycle zinc-containing *** pyrolysis mass loss behavior of adding blast furnace dust with different zinc contents to different ferro-coke materials was systematically studied by thermogravimetry and differential thermogravimetry analysis,and the kinetic mechanism of pyrolysis-reduction reaction of hybrid briquette was *** results of thermogravimetric curve analysis show that the addition of zinc oxide to the sample has no significant effect on the mass loss rate of the sample below 580℃,and the pyrolysis mass loss of zinc oxide mainly occurs between 800 and 1000℃.Kinetic analysis results show that the pyrolysis of zinc-containing samples is controlled by chemical reactions below 580℃.The reaction at 580–700℃ is controlled by the nucleation and growth model,and that above 700℃ is mainly controlled by *** results of X-ray diffraction analysis show that the pyrolysis process can effectively remove zinc oxide from ferro-coke.

关键词： Zinc-containing dust Weakly caking coal Ferro-coke Pyrolysis Reduction Thermal reaction analysis Kinetic analysis