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A robust viscoelastic surfactant tolerating 20% HCl up to 150℃ for oil well stimulation

Petroleum Science 2024年第3期21卷 1865-1874页

作者： Ji Wang Ning Qi Hong-Yao Yin yu-jun feng Polymer Research Institute State Key Laboratory of Polymer Materials EngineeringSichuan UniversityChengdu610065SichuanPR.China Tianfu Yongxing Laboratory New Theory and Technology of CO_(2) Capture Research CenterChengdu610065SichuanPR China School of Petroleum Engineering China University of Petroleum(East China)Qingdao266580ShandongPR China

Viscoelastic surfactants(VES)are often used as viscous diverters in acidizing stimulation to prolong the acid consumption time and maximize zonal coverage of the acid for improving well ***,the ceiling temperature of commercial VES cannot exceed 120℃in practical use because of the poor thermal stability and fragile molecular structure,hindering their implementation in hightemperature oil reservoirs,i.e.,≥150℃.Here we synthesized a novel C22-tailed diamine,N-erucaminopropyl-N,N-dimethylamine(EDPA),and examined comparatively its rheological behavior,assemblies morphology and molecular stability in 20 wt%HCl with a commercial VES,erucyl dimethyl amidopropyl betaine(EDAB).The feasibility of EDPA for acidizing stimulation was assessed by acid etching of carbonate rock with its HCl solution at 150℃.Rheological results showed that the 2.5 wt%EDPA—20 wt%HCl solution maintains stable viscosity of 90 m Pa s at 150℃for 60 min,while that of 2.0 wt%EDAB HCl solution is just 1 m Pa s under identical conditions.1H NMR spectra and cryo-TEM observations revealed that the chemical structure and self-assembled architectures of EDPA remained intact in such context,but the EDAB suffered from degradation due to the hydrolysis of the amide group,accounting for the poor heat-resistance and *** reaction rate of 2.5 wt%EDPA HCl solution with carbonate rock was one order of magnitude lower than that of 20 wt%HCl solution at 150℃,underpinning the potential of EDPA to be used in the high-temperature reservoirs *** work improved the thermal tolerance of VES in highly concentrated HCl solution,paving a feasible way for the acidization of high-temperature reservoir environments(~150℃).

关键词： Viscoelastic surfactants Thermal stability Self-diverting acid Wormlike micelles Acidizing stimulation

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A salt-induced viscosifying smart polymer for fracturing inter-salt shale oil reservoirs

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Petroleum Science 2019年第4期16卷 816-829页

作者： Xian’e Li Hong-Yao Yin Ru-Sheng Zhang Jia Cui jun-Wen Wu yu-jun feng State Energy Center for Shale Oil Research and Development Beijing 100083People’s Republic of China Polymer Research Institute Sichuan UniversityChengdu 610065People’s Republic of China Petroleum Exploration&Production Research Institute SINOPECBeijing 100083People’s Republic of China

Inter-salt shale oil reservoirs located between two salt layers are always accompanied by high temperature and high salinity. However, the present commonly used water-soluble polymers in fracturing fluids su er from poor tolerance to high temperature and high salinity. Thermoviscosifying polymers(TVP) whose aqueous solution shows viscosity increase upon increasing temperature and salt concentration have received considerable attention recently, which is promising for utilization in fracturing fluids to overcome these problems. In this work, both the salt-induced viscosifying property and mechanism of a TVP solution were investigated and the performance of TVP used as fracturing fluid based on the conditions of the Jianghan inter-salt shale oil reservoir in China was evaluated. It is found that the salt-induced viscosifying property of the TVP solution decreases with temperature and shear rate, but increases with polymer concentration. The number of intermolecular hydrophobic domains increases with the salt concentration contributing to the strengthening of a 3D network structure, which results in an increase in viscosity. In addition, the TVP fracturing fluid formulated with saturated brine exhibits excellent temperature and shear resistance, sand-suspending performance, and gel-breaking performance. Its viscosity remains above50 m Pa s after being sheared for 1 h even at a high temperature of 140 °C and the sand-suspending stability can be maintained for more than 1 week at 100 °C. Furthermore, the fracturing fluid can be easily broken down within 12h using 0.2 wt%–0.3 wt% potassium persulfate without residue.

关键词： Fracturing Salt-induced viscosifying Thermoviscosifying Smart polymer Rheological properties

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装配式旋压扩大头钢管桩的设计与施工

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建筑与装饰 2024年第10期 16-18页

作者：黄振华黄磊群玉俊峰广西盛虎建筑科技有限公司广西南宁 530000 南宁市建筑规划设计集团有限公司广西南宁 530000 广西淮君桩工设备租赁有限公司广西南宁 530000

文章对装配式旋压扩大头钢管桩的优势进行讨论,提出了装配式旋压扩大头钢管桩的设计思路,即围绕一般规定、构造及焊缝形式和尺寸,通过对有关设计参数及流程展开讨论,论述了装配式旋压扩大头钢管桩具体施工流程,并对制作与施工、产品制... 详细信息

文章对装配式旋压扩大头钢管桩的优势进行讨论,提出了装配式旋压扩大头钢管桩的设计思路,即围绕一般规定、构造及焊缝形式和尺寸,通过对有关设计参数及流程展开讨论,论述了装配式旋压扩大头钢管桩具体施工流程,并对制作与施工、产品制作与出厂检验施工准备施工工艺等进行分析研究.研究结果表明,在关键施工工艺中,吊装时应对构件进行进场验收,主要通过复核桩芯位置、检验机械水平度等方式,通过高效率的施工方式决定桩架及吊装次序.

关键词：装配式旋压扩大头钢管桩设计参数施工工艺

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Visualization of adaptive polymer flow and displacement in medium-permeable 3D core-on-a-chip

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Petroleum Science 2023年第2期20卷 1018-1029页

作者： Yan Zhang Xue-Zhi Zhao Pei-Hui Han Li-yuan Zhang David A.Weitz yu-jun feng Polymer Research Institute State Key Laboratory of Polymer Materials EngineeringSichuan UniversityChengdu610065SichuanPR China EOR Laboratory Exploration&Development Research InstituteDaqing Oilfield Limited CompanyPetroChinaDaqing163712HeilongjiangPR China School of Engineering and Applied Sciences Harvard UniversityCambridge02138United States School of Petroleum Engineering China University of PetroleumQingdao266580ShandongPR China

Polymer flooding has been witnessed an effective technology for enhancing oil recovery from medium-to low-permeability reservoirs;however, direct visualization of polymer solution flow in such reservoir condition is still lacking. In this work, a three-dimensional (3D) core-on-a-chip device with a permeability of around 200 mD was prepared and employed to visualize the pore-scale flow and displacement of a self-adaptive polymer (SAP, 8.7 × 106 g·mol−1)−whose microscopic association structure and macroscopic viscosity can reversibly change in response to shear action−versus partially hydrolyzed polyacrylamide (HPAM), by recording their flow curves, monitoring dynamic transportation process via particle imaging velocimetry, and building 3D structure of remaining oil. The results show that, in single-phase flow, all polymer solutions exhibit flow thinning and then thickening regions as flow rate increases, but the transition between two regimes occurs at a small Weissenberg number (10−3−10−1) in this medium-permeable condition. In contrast to HPAM-1 with close weight-average molecular weight (Mw), the adaptive character not only extends SAP's shear-govern region, allowing SAP to propagate piece by piece and achieve higher accessible pore volume, but it also enhances the elastic resistibility of polymer in the extension-dominated regime, increasing the microscopic displacement efficiency. These two effects result in 1.5–3 times more oil recovery factor for SAP than for HPAM-1. Regarding ultra-high-Mw HPAM-2 (25 × 106 g·mol−1), plugging and chain degradation do occur, thus producing lower oil recovery than SAP. This work provides a direct approach for in-situ assessment of polymer-based displacing system under a more authentic condition of practical reservoirs.

关键词： Polymer flooding Medium-permeable transparent media Adaptive polymer In-situ rheology Particle imaging velocimetry

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关于魔力弹簧的收缩时间和上端运动问题

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大学物理 2024年第5期43卷 13-18页

作者：于凤军张希威汤振杰鞠林田俊龙安阳师范学院物理与电气工程学院河南安阳455000 广西师范大学物理科学与技术学院广西桂林541001

针对有关魔力弹簧研究中的几个问题进行探讨和澄清.建立了预收缩力弹簧的模型,推出其形变规律.根据质心运动定理,导出这种弹簧自由下落时,收缩到原长所用的时间、其上端的运动方程和速度公式.研究表明,对于通常演示所用的魔力弹簧,在自... 详细信息

针对有关魔力弹簧研究中的几个问题进行探讨和澄清.建立了预收缩力弹簧的模型,推出其形变规律.根据质心运动定理,导出这种弹簧自由下落时,收缩到原长所用的时间、其上端的运动方程和速度公式.研究表明,对于通常演示所用的魔力弹簧,在自由下落时的收缩阶段,其上端不是作匀速直线运动.

关键词：魔力弹簧预收缩力弹簧收缩时间质心运动定理

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Laparoscopic anatomical liver resection of segment 7 using a sandwich approach to the right hepatic vein (with video)

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Hepatobiliary & Pancreatic Diseases International 2024年第2期23卷 217-220页

作者： Song-feng yu Wei-Chen Zhang jun yu Department of Hepatobiliary and Pancreatic Surgery the First Affiliated HospitalZhejiang University School of MedicineHangzhou 310003China

Full laparoscopic liver resection has been performed widely since it was introduced in the early *** has been expanded from initial for partial resection of the anterolateral segments to non-restriction of area of the liver[1–3].Anatomical liver resec-tion is considered to have potential superiority than non-anatomic resection in terms of tumor prognosis,thus it is more often rec-ommended in the treatment of hepatocellular carcinoma[4,5].Recently,laparoscopic segmental liver resection according to the Couinaud classification has been widely performed due to its ad-vantages in minimal invasiveness and tumor prognosis.

关键词： resection liver hepatic

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Gas channeling control with an in-situ smart surfactant gel during water-alternating-CO_(2) enhanced oil recovery

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Petroleum Science 2023年第5期20卷 2835-2851页

作者： Xin-Jie Luo Bing Wei Ke Gao Bo Jing Bo Huang Ping Guo Hong-Yao Yin yu-jun feng Xi Zhang Polymer Research Institute State Key Laboratory of Polymer Materials EngineeringSichuan UniversityChengdu 610065SichuanChina National Key Laboratory of Oil and Gas Reservoir Geology and Exploitation Southwest Petroleum UniversityChengdu 610500SichuanChina National Key Laboratory of Offshore Oil Exploitation CNOOC Research Institute Ltd.Beijing 102209China

Undesirable gas channeling always occurs along the high-permeability layers in heterogeneous oil reservoirs during water-alternating-CO_(2)(WAG)flooding,and conventional polymer gels used for blocking the“channeling”paths usually suffer from either low injectivity or poor gelation ***,we for the first time developed an in-situ high-pressure CO_(2)-triggered gel system based on a smart surfactant,N-erucamidopropyl-N,N-dimethylamine(UC22AMPM),which was introduced into the aqueous slugs to control gas channeling inWAG *** water-like,low-viscosity UC22AMPM brine solution can be thickened by high-pressure CO_(2) owing to the formation of wormlike micelles(WLMs),as well as their growth and shear-induced structure buildup under shear *** thickening power can be further potentiated by the generation of denser WLMs resulting from either surfactant concentration augmentation or a certain range of heating,and can be impaired via pressurization above the critical pressure of CO_(2) because of its soaring solvent *** flooding tests using heterogeneous cores demonstrated that gas channeling was alleviated by plugging of high-capacity channels due to the in-situ gelation of UC22AMPM slugs upon their reaction with the pre-or post-injected CO_(2) slugs under shear flow,thereupon driving chase fluids into unrecovered low-permeability areas and producing an 8.0% higher oil recovery factor than the conventional WAG *** smart surfactant enabled high injectivity and satisfactory gelation control,attributable to low initial viscosity and the combined properties of one component and CO_(2)-triggered gelation,*** work could provide a guide towards designing gels for reducing CO_(2) spillover and reinforcing the CO_(2) sequestration effect during CO_(2) enhanced oil recovery processes.

关键词： CO_(2)flooding Enhanced oil recovery Gas channeling Water-alternating-CO_(2) Smart surfactant Gel

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Approximate Synchronization of Multi-Agent Systems over Finite Fields

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Journal of Systems Science & Complexity 2024年第4期37卷 1561-1580页

作者： yu Miao feng jun-e XIA Jianwei FU Shihua SHEN Hao School of Mathematical Sciences Liaocheng UniversityLiaocheng 252059China School of Mathematics Shandong UniversityJinan 250100China School of Electrical and Information Engineering Anhui University of TechnologyMaanshan 243002China

In this paper,the approximate synchronization of leader-follower multiagent systems(MASs) over finite fields is studied in regard to local and global ***,the approximately synchronous state set(ASSS) is ***,combined with ASSS and transient periods,some criteria for the local and global approximate synchronization of systems are ***,the algorithms for calculating the maximum approximately synchronous basin(MASB) and the maximum control invariant set(MCIS) are ***,the global approximate synchronization of the system is achieved by designing the state feedback control,and a design algorithm of the controller using the truth matrix method is ***,the results of approximate synchronization are degenerated to complete ***,two examples are shown to demonstrate the results of this paper.

关键词： Approximate synchronization finite field multiagent system semi-tensor product state feedback control

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Supermassive black holes triggered by QCD axion bubbles

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Communications in Theoretical Physics 2024年第5期76卷 134-139页

作者： Hai-jun Li Ying-Quan Peng Wei Chao yu-feng Zhou Key Laboratory of Theoretical Physics Institute of Theoretical PhysicsChinese Academy of SciencesBeijing 100190China Center for Advanced Quantum Studies Department of PhysicsBeijing Normal UniversityBeijing 100875China School of Physical Sciences University of Chinese Academy of SciencesBeijing 100049China School of Fundamental Physics and Mathematical Sciences Hangzhou Institute for Advanced StudyUCASHangzhou 310024China International Centre for Theoretical Physics Asia-Pacific Beijing/HangzhouChina

Supermassive black holes(SMBHs)are ubiquitous in the center of galaxies,although the origin of their massive seeds is still *** this paper,we investigate the formation of SMBHs from the quantum chromodynamics(QCD)axion *** this case,primordial black holes(PBHs)are considered as the seeds of SMBHs,which are generated from the QCD axion bubbles due to an explicit Peccei–Quinn(PQ)symmetry breaking after *** QCD axion bubbles are formed when the QCD axion starts to oscillate during the QCD phase *** consider a general case in which the axion bubbles are formed with the bubble effective angle θ_(eff)∈(0,π],leading to the minimum PBH mass∼■(10^(4)−10^(7))M⊙for the axion decay constant f_(a)∼■(10^(16))*** PBHs at this mass region may account for the seeds of SMBHs.

关键词： supermassive black holes primordial black holes quantum chromodynamics axion

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New insights into the mechanism of surfactant enhanced oil recovery:Micellar solubilization and in-situ emulsification

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Petroleum Science 2022年第2期19卷 870-881页

作者： Xue-Zhi Zhao Guang-Zhi Liao Ling-Yan Gong Huo-Xin Luan Quan-Sheng Chen Wei-Dong Liu Dong Liu yu-jun feng Polymer Research Institute State Key Laboratory of Polymer Materials EngineeringSichuan UniversityChengdu610065People's Republic of China PetroChina Exploration&Production Company Beijing100007People's Republic of China Research Institute of Experiment and Detection Xinjiang Oilfield Branch CompanyPetroChinaKaramay834000People's Republic of China Research Institute of Petroleum Exploration&Development PetroChina Company LimitedBeijing100083People's Republic of China Institute of Nuclear Physics and Chemistry China Academy of Engineering PhysicsMianyang621000People's Republic of China

Reducing the oil-water interfacial tension(IFT)to ultra-low is believed the primary mechanism for surfactant-based enhanced oil recovery(EOR)***,field trials have shown that low concentration surfactant flooding can also improve oil recovery without ultra-low *** clarify the mechanism behind,the currently-used surfactant,naphthenic arylsulfonate(NAS),was used to unravel its function during surfactant flooding from the horizon of micron-and *** solubilization capacity of NAS micelle to petroleum fractions was evaluated through light absorbance strategy,smallangle neutron scattering,dynamic light scattering and transmission electron *** was found that micellar solubilization plays a significant role during the surfactant ***-situ emulsification was visualized in microfluidics with three types of microchips,respectively.A series of displacement tests were carried out with NAS solution pumping into oil-saturated *** results show that in-situ emulsification improve oil recovery mainly through blocking and entrainment *** from this work aid in understanding the interaction between surfactant solution and petroleum fractions at low surfactant concentration,which is helpful for design surfactant-based displacing system for EOR process.

关键词： Enhanced oil recovery Surfactant flooding Micellar solubilization Microfluidics In-situ emulsification

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