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包套轧制粉末冶金法制备泡沫铝三明治板

东北大学学报（自然科学版） 2011年第2期32卷 277-280页

作者：宋滨娜祖国胤姚广春关志昊东北大学材料与冶金学院辽宁沈阳110819

以空气雾化的AlSi12合金粉、镁粉和氢化钛粉末为原料,采用包套轧制法成功制备出了泡沫铝三明治板材.利用300 dpi扫描仪、扫描电镜(SEM)和显微硬度仪等检测方法系统比较了复合轧制和包套轧制方法对制备前驱体的宏观形貌和界面结合及其泡... 详细信息

以空气雾化的AlSi12合金粉、镁粉和氢化钛粉末为原料,采用包套轧制法成功制备出了泡沫铝三明治板材.利用300 dpi扫描仪、扫描电镜(SEM)和显微硬度仪等检测方法系统比较了复合轧制和包套轧制方法对制备前驱体的宏观形貌和界面结合及其泡孔结构的影响,结果表明:包套轧制可以有效阻止面板材料裂纹的扩展,获得完整的和致密度均匀的预制坯,并能实现面板芯材的有效结合,最终获得泡孔结构完整和均匀的泡沫铝三明治板.

关键词：泡沫铝三明治板预制体包套轧制复合轧制界面粉末冶金

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闭孔泡沫铝材料吸声性能分析

东北大学学报（自然科学版） 2011年第1期32卷 114-116,132页

作者：梁李斯姚广春穆永亮华中胜东北大学材料与冶金学院辽宁沈阳110819

为更全面地反映闭孔泡沫铝材料的吸声降噪能力,从密度、厚度、背后空腔深度、打孔率几个方面,对闭孔泡沫铝材料的吸声性能进行研究.改变以往单纯用吸声系数的峰值表征的方法,而是用吸声系数的峰值、降噪系数、半峰宽3个指标来评价闭孔... 详细信息

为更全面地反映闭孔泡沫铝材料的吸声降噪能力,从密度、厚度、背后空腔深度、打孔率几个方面,对闭孔泡沫铝材料的吸声性能进行研究.改变以往单纯用吸声系数的峰值表征的方法,而是用吸声系数的峰值、降噪系数、半峰宽3个指标来评价闭孔泡沫铝材料的吸声性能.通过驻波管法测试吸声系数,用Origin软件进行吸声曲线的分析,建立一次函数.结果表明:在以往研究中个别吸声系数的峰值较高的样品,整体吸声效果不佳;而一些吸声系数的峰值处于中等水平的却具有较好的整体吸声效果,因此更适合于在实际应用中用于吸声结构的设计.

关键词：闭孔泡沫铝吸声降噪系数半峰宽吸声系数

Interaction mechanism between BaZrO_(3)/Y_(2)O_(3) refractory and Ti_(2)Ni alloy melts

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Journal of Iron and Steel Research International 2024年第6期31卷 1376-1388页

作者： Xiao Hou guang-yao Chen Jian Liu Ming-rui Lv Fei-hai Yu Qi-sheng Feng Rong-bin Li Xiong-gang Lu Chong-he Li State Key Laboratory of Advanced Special Steel and Shanghai Key Laboratory of Advanced Ferromeallurgy and School of Materials Science and Engineering Shanghai UniversityShanghai 200072China Shanghai Special Casting Engineering Technology Research Center Shanghai 201605China Zhejiang Institute of Advanced Materials Shanghai UniversityJiashan 314100ZhejiangChina School of Materials Science and Engineering Shanghai DianJi UniversityShanghai 201306China

The titanium alloys with highly chemical activity require stable crucible refractories that can withstand the erosion of alloy *** phase composition and microstructure are crucial factors that affect the stability of the refractory *** effect of Y_(2)O_(3) on the composition and microstructure of BaZrO_(3) crucible was systematically investigated,and the improved mechanism of the stability of BaZrO_(3)/Y_(2)O_(3) crucible was clarified in comparison with the BaZrO_(3) *** results showed that the erosion layer thickness of the BaZrO_(3)/Y_(2)O_(3) crucible was only 63μm,which was far less than that in the BaZrO_(3) crucible(485μm),and the erosion layer in the BaZrO_(3)/Y_(2)O_(3) crucible also exhibited a higher density than that in the BaZrO_(3) *** the sintering,Y_(2)O_(3) could improve the densification of the BaZrO_(3) crucible due to the solid solution effect between Y_(2)O_(3) and ZrO_(2),which also caused the evaporation of BaO,resulting in the generation of a Y_(2)O_(3)(ZrO_(2))film on the surface of the ***,the Y_(2)O_(3)(ZrO_(2))had higher thermodynamic stability than Y_(2)O_(3),confirming that the BaZrO_(3)/Y_(2)O_(3) crucible with high density exhibited a superior erosion resistance to titanium *** dual-phase structure provides a strategy to design a long-life and stable refractory for melting titanium alloys.

关键词： Barium zirconate Yttrium oxide Dual-phase refractory Titanium alloy Interaction

Electroless Ni-P plating on Mg-Li alloy by two-step method

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Transactions of Nonferrous Metals Society of China 2011年第10期21卷 2225-2230页

作者：罗洪杰宋滨娜刘宜汉姚广春东北大学材料与冶金学院沈阳110819

Pretreated Mg-Li alloy sheets were pre-plated in a NiCO3？2Ni（OH）2？4H2O solution to form a thin Ni-P alloy film and then plating in a NiSO4？6H2O solution was carried out to obtain a protective *** surface morphology,structure and corrosion resistance of the coating were *** results showed that a flat,bright and compact plating layer,which was integrated into the matrix metal,was *** P content of the Ni-P coating reached 13.56%（mass fraction）.The hardness value of the Ni-P coating was about HV *** polarization curve showed that the corrosion potential of the Ni-P coating reached ？0.249 V（vs SCE）.A long passivation region was found on the polarization curve,and this phenomenon indicated that the coating has an excellent anti-corrosion property.

关键词： Mg-Li alloy pretreatment electroless plating Ni-P coating corrosion resistance

Single transition-metal atoms anchored on a novel Diracdispersiveπ-πconjugated holey graphitic carbon nitride substrate:computational screening toward efficient bifunctional OER/ORR electrocatalysts

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Rare Metals 2024年第8期43卷 3819-3832页

作者： chun-yao Fang Xi-Hang Zhang Qiang Zhang Di Liu Xiao-Meng Cui Jing-Cheng Xu Cheng-Long Shi Meng-Yu Yang College of Science University of Shanghai for Science and TechnologyShanghai 200093China School of Materials and Chemistry University of Shanghai for Science and TechnologyShanghai 200093China

Nonprecious-metal-group single-metal-atom catalysts with bifunctional catalytic capabilities toward the oxygen evolution reaction(OER)and oxygen reduction reaction(ORR)are highly sought after in energy-conversion and storage ***,producing renewable and sustainable energy sources remains ***,single-transition metal atoms anchored onπ-πconjugated two-dimensional(2D)graphitic carbon nitride substrates formπ-d conjugated conductive channels that enhance the overall electrocatalytic ***,firstprinciples calculations were carried out to design and demonstrate a novel macropore graphitic carbon nitride(gC_(10)N_(3))as a promising 2D electrocatalyst substrate to support single-transition metal(TM,from Sc to Au).The"donation-acceptance"charge interaction in the TM-N_(2)moiety effectively balances the adsorption strength of oxygenated intermediates in Ni@g-C_(10)N_(3)and Rh@gC_(10)N_3,making them effective bifunctional OER/ORR electrocatalysts with IrO_(2)/Pt-beyond overpotentials being as low as 0.39/0.38 V and 0.54/0.44 V,***,they possess high stability and conductivity and are less susceptible to oxidation and corrosion under working *** guarantees high activity under ambient ***,the origin of the OER/ORR activity of TM@g-C_(10)N_(3) is explained using multilevel descriptors:intrinsic(p,Bader charge,integral crystal orbital Hamilton population(ICOHP),bond length,and d-band center(εd).In particular,for optimal Ni@g-C_(10)N_(3),the clear hybridization between the Ni-d orbital and surface O-p orbital causes the paired electrons to occupy the bonding *** enables OH~*to be adsorbed on the Ni@g-C_(10)N_(3),thereby achieving the highest catalytic performance.

关键词： First-principles calculation Oxygen evolution reaction Oxygen reduction reaction Bifunctional electrocatalysts Single-metal-atom electrocatalysts

Local and Parallel Finite Element Algorithms Based on Two-grid Discretizations for the Unsteady MHD Equations with Low Electromagnetic Reynolds Number

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Acta Mathematicae Applicatae Sinica 2024年

作者： Shi-lin MI guang-zhi DU yao RONG Li-yun ZUO School of Mathematics and Statistics Shandong Normal University College of Engineering Physics Shenzhen Technology University School of Mathematical Sciences University of Jinan

This paper mainly presents and studies some local and parallel finite element methods for the unsteady magnetohydrodynamic equations with low electromagnetic Reynolds number. Firstly, both the semi discrete and fully discrete local algorithms are provided and investigated, and the theoretical tool crucial to the analysis of the fully discrete local algorithm is obtained. Subsequently, we generalize the fully discrete local algorithm to the fully discrete parallel algorithm. At the end, some numerical experiments are provided to validate the effectiveness and efficiency of our algorithms.

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低温固相反应合成NiFe_2O_4尖晶石纳米粉

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东北大学学报（自然科学版） 2010年第6期31卷 868-872页

作者：张志刚姚广春马佳华中胜东北大学材料与冶金学院辽宁沈阳110004

以FeSO4.7H2O,NiSO4.6H2O和NaOH为原料,NaCl为分散剂,在室温下充分研磨反应制备前驱体,然后将前驱体进行煅烧得到NiFe2O4尖晶石纳米粉.重点研究了分散剂含量、煅烧温度和保温时间对粉体粒度和形貌的影响.利用X射线衍射仪(XRD)和扫描电... 详细信息

以FeSO4.7H2O,NiSO4.6H2O和NaOH为原料,NaCl为分散剂,在室温下充分研磨反应制备前驱体,然后将前驱体进行煅烧得到NiFe2O4尖晶石纳米粉.重点研究了分散剂含量、煅烧温度和保温时间对粉体粒度和形貌的影响.利用X射线衍射仪(XRD)和扫描电子显微镜(SEM)对所得产物进行表征.结果表明:添加20%(质量分数)NaCl制得的前驱体在800℃下煅烧1.5h得到的纳米粉分布均匀,颗粒呈球形并且晶型完整单一,平均粒径约为75nm.

关键词： NiFe2O4尖晶石纳米粉低温固相反应分散剂

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铝熔体中磁性杂质颗粒的电磁分离

材料科学与工艺 2006年第5期14卷 524-526页

作者：张磊焦万丽尉海军姚广春东北大学材料与冶金学院辽宁沈阳110004

分析了磁性杂质颗粒在电磁场中的受力情况,采用磁平衡法测量了铝熔体中两种典型富铁相杂质颗粒的磁化率,指出铝熔体中的富铁相杂质是顺磁性物质,在电磁场中受到电磁力和磁场力的驱动作用,确定其在分离器上的聚集方式.静态电磁分离试验... 详细信息

分析了磁性杂质颗粒在电磁场中的受力情况,采用磁平衡法测量了铝熔体中两种典型富铁相杂质颗粒的磁化率,指出铝熔体中的富铁相杂质是顺磁性物质,在电磁场中受到电磁力和磁场力的驱动作用,确定其在分离器上的聚集方式.静态电磁分离试验结果表明,当磁场强度大于145 mT时,电磁力起主要作用;当磁场强度小于120mT时,磁场力起主要作用.

关键词：磁性杂质颗粒磁化率电磁力磁场力电磁分离

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泡沫铝夹心板芯层泡沫结构的研究

功能材料 2007年第5期38卷 859-861页

作者：祖国胤张敏姚广春李红斌东北大学材料与冶金学院辽宁沈阳110004

研究了采用轧制复合-粉末冶金发泡法制备的泡沫铝夹心板的生产工艺,探讨了主要工艺条件对芯层泡沫结构的影响,得到了优化的工艺参数。研究结果表明：轧制复合工艺可以使芯层粉末达到很高的致密度,为发泡过程创造了有利条件。轧制复合板... 详细信息

研究了采用轧制复合-粉末冶金发泡法制备的泡沫铝夹心板的生产工艺,探讨了主要工艺条件对芯层泡沫结构的影响,得到了优化的工艺参数。研究结果表明：轧制复合工艺可以使芯层粉末达到很高的致密度,为发泡过程创造了有利条件。轧制复合板适宜的发泡温度为615-620℃,温度过高会导致芯层出现大尺寸连通孔。发泡时间对熔融态泡沫体的凝固过程有显著影响,时间过长会使泡沫层塌陷,发泡温度为620℃时,经4-6min发泡芯层可形成良好的泡沫结构。

关键词：泡沫铝夹心板轧制复合粉末冶金发泡致密度发泡温度发泡时间