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Advances of Electrochemical and Electrochemiluminescent Sensors Based on Covalent Organic Frameworks

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Nano-Micro Letters 2024年第2期16卷 395-422页

作者： Yue Cao Ru Wu yan‑yan gao yang Zhou jun‑Jie Zhu Key Laboratory for Organic Electronics and Information Displays(KLOEID)and Institute of Advanced Materials(IAM) Nanjing University of Posts and Telecommunications(NJUPT)Nanjing 210023People’s Republic of China State Key Laboratory of Analytical Chemistry for Life Science School of Chemistry and Chemical EngineeringNanjing UniversityNanjing 210023People’s Republic of China

Covalent organic frameworks(COFs),a rapidly developing category of crystalline conjugated organic polymers,possess highly ordered structures,large specific surface areas,stable chemical properties,and tunable pore *** the first report of boroxine/boronate ester-linked COFs in 2005,COFs have rapidly gained popularity,showing important application prospects in various fields,such as sensing,catalysis,separation,and energy *** them,COFs-based electrochemical(EC)sensors with upgraded analytical performance are arousing extensive *** this review,therefore,we summarize the basic properties and the general synthesis methods of COFs used in the field of electroanalytical chemistry,with special emphasis on their usages in the fabrication of chemical sensors,ions sensors,immunosensors,and ***,the emerged COFs in the electrochemiluminescence(ECL)realm are thoroughly covered along with their preliminary ***,final conclusions on state-of-the-art COFs are provided in terms of EC and ECL sensors,as well as challenges and prospects for extending and improving the research and applications of COFs in electroanalytical chemistry.

关键词： Covalent organic frameworks Electrochemistry Electrochemiluminescence Sensors

Detection of Nonlinear Behavior Induced by Hard Limiting in Voltage Source Converters in Wind Farms Based on Higher-order Spectral Analysis

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Journal of Modern Power Systems and Clean Energy 2024年第2期12卷 630-645页

作者： Zetian Zheng Shaowei Huang Qiangsheng Bu Chen Shen jun yan State Key Laboratory of Power Systems Department of Electrical EngineeringTsinghua UniversityBeijing 100084China State grid Jiangsu Electric Power Co. Ltd.Research InstituteNanjingChina

In recent years, sub-synchronous oscillation accidents caused by wind power integration have received extensive attention. The recorded constant-amplitude waveforms can be induced by either linear or nonlinear oscillation mechanisms. Hence, the nonlinear behavior needs to be distinguished prior to choosing the analysis method. Since the 1960s, the higher-order statistics(HOS) theory has become a powerful tool for the detection of nonlinear behavior(DNB) in production quality control wherein it has mainly been applied to mechanical condition monitoring and fault diagnosis. This study focuses on the hard limiters of the voltage source converter(VSC) control systems in the wind farms and attempts to detect the nonlinear behavior caused by bi-or uni-lateral saturation hard limiting using the HOS analysis. First, the conventional describing function is extended to obtain the detailed frequency domain information on the bi-and uni-lateral saturation hard limiting. Furthermore, the bi-and tri-spectra are introduced as the HOS, which are extended into bi-and tri-coherence spectra to eliminate the effects of the linear parts on the harmonic characteristics of hard limiting in the VSC control system, respectively. The effectiveness of the HOS in the DNB and the classification of the hard-limiting types is proven, and its detailed derivation and estimation procedure is presented. Finally, the quadratic and cubic phase coupling in the signals is illustrated, and the performance of the proposed method is evaluated and discussed.

关键词： Bi-coherence spectrum detection of nonlinear behavior hard limiting higher-order statistics tri-coherence spectrum voltage source converter wind farms.

FADSF:A Data Sharing Model for Intelligent Connected Vehicles Based on Blockchain Technology

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Computers, Materials & Continua 2024年第8期80卷 2351-2362页

作者： yan Sun Caiyun Liu jun Li Yitong Liu Data Security Institute China Industrial Control Systems Cyber Emergency Response TeamBeijing100040China

With the development of technology,the connected vehicle has been upgraded from a traditional transport vehicle to an information terminal and energy storage *** data of ICV(intelligent connected vehicles)is the key to organically maximizing their ***,in the context of increasingly strict global data security supervision and compliance,numerous problems,including complex types of connected vehicle data,poor data collaboration between the IT(information technology)domain and OT(operation technology)domain,different data format standards,lack of shared trust sources,difficulty in ensuring the quality of shared data,lack of data control rights,as well as difficulty in defining data ownership,make vehicle data sharing face a lot of problems,and data islands are *** study proposes FADSF(Fuzzy Anonymous Data Share Frame),an automobile data sharing scheme based on *** data holder publishes the shared data information and forms the corresponding label storage on the *** data demander browses the data directory information to select and purchase data assets and verify *** data demander selects and purchases data assets and verifies them by browsing the data directory ***,this paper designs a data structure Data Discrimination Bloom Filter(DDBF),making complaints about illegal *** the number of data complaints reaches the threshold,the audit traceability contract is triggered to punish the illegal data publisher,aiming to improve the data quality and maintain a good data sharing *** this paper,based on Ethereum,the above scheme is tested to demonstrate its feasibility,efficiency and security.

关键词： Blockchain connected vehicles data sharing smart contracts credible traceability

Switched-capacitor Based Seven-level Boost Inverter with a Reduced Number of Devices

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CSEE Journal of Power and Energy Systems 2024年第1期10卷 381-391页

作者： Weijie Lin jun Zeng Bo Fu Zhixing yan junfeng Liu School of Electric Power Engineering South China University of TechnologyGuangzhou 510641China WISDRI Engineering&Research Incorporation Limited Wuhan 430074China Department of Energy Aalborg UniversityAalborg 9220Denmark School of Automation Science and Engineering South China University of TechnologyGuangzhou 510641China

The conventional multilevel inverters(MLIs)have the disadvantages of numerous devices,incapacity of boost,unbalance for capacitor’s voltage,high complexity for control,and *** by this issue,a seven-level boost inverter(7LBI)based on a switched capacitor is presented for singlephase applications in this *** proposed 7LBI using only seven transistors can achieve seven output levels,1.5 voltage gain,and natural balance of capacitors’voltages without sensors or other auxiliary methods,which illustrates its suitability for the applications of renewable energy *** configuration of topology and operating principles are illustrated in *** natural balance of capacitors and capacitance calculations are deduced as ***,the comparative study is conducted for different types of *** results illustrate the merits of the proposed 7LBI with respect to reduced devices,lower voltage stress,and less power ***,a simulation for the proposed 7LBI with PWM modulation is realized based on the theoretical analysis;an experimental prototype is also implemented,verifying multilevel output,boost ability,natural balance for switched capacitors,and performance of transient response.

关键词： Multilevel inverters voltage gain natural balance renewable energy generation reduced number of elements

Two-way shape memory effect in a Ti-Zr-Nb-Ta high-temperature shape memory alloy

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Rare Metals 2024年第3期43卷 1257-1262页

作者： Cheng-yang Xiong Tuo Li jun Wang yan Li School of Materials Science and Engineering Beihang UniversityBeijing100191China

The two-way shape memory effect in a Ti-18.5Zr-10Nb-3.5Ta high-temperature shape memory alloy was investigated.X-ray diffraction measurem ent shows that the alloy is composed of orthorhombicα"-martensite.ωphase is not found in Ti-18.5Zr-10Nb-3.5Ta alloy due to the suppressing effect of Ta ***α"-martensite laths are found in the transmission electron microscope observation;after the bending deformation,there appear a lot of *** alloy exhibits a shape memory strain of 3.8%aud a high reverse martensite transformation start temperature of 464 *** maximum two-way shape memory strain of 1.2%is obtained in the alloy with the prebending training strain of 10%.The mechanism can be ascribed to the effect of internal stress field caused by dislocations.

关键词： Ti-Zr Shape memory alloys Two-way shape memory effect

A Novel Disturbance Observer Based Fixed-Time Sliding Mode Control for Robotic Manipulators With global Fast Convergence

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IEEE/CAA Journal of Automatica Sinica 2024年第3期11卷 661-672页

作者： Dan Zhang Jiabin Hu jun Cheng Zheng-guang Wu Huaicheng yan IEEE Zhejiang University of Technology guangxi Normal University Zhejiang University the East China University of Science and Technology

This paper proposes a new global fixed-time sliding mode control strategy for the trajectory tracking control of uncertain robotic ***,a fixed-time disturbance observer(FTDO) is designed to deal with the adverse effects of model uncertainties and external disturbances in the manipulator *** an adaptive scheme is used and the adaptive FTDO(AFTDO) is developed,so that the priori knowledge of the lumped disturbance is not ***,a new non-singular fast terminal sliding mode(NFTSM) surface is designed by using an arctan function,which helps to overcome the singularity problem and enhance the robustness of the *** on the estimation of the lumped disturbance by the AFTDO,a fixed-time non-singular fast terminal sliding mode controller(FTNFTSMC)is developed to guarantee the trajectory tracking errors converge to zero within a fixed *** settling time is independent of the initial state of the *** addition,the stability of the AFTDO and FTNFTSMC is strictly proved by using Lyapunov ***,the fixed-time NFESM(FTNFTSM) algorithm is validated on a 2-link manipulator and comparisons with other existing sliding mode controllers(SMCs) are *** comparative results confirm that the FTNFTSMC has superior control performance.

关键词： Disturbance observer(DO) fixed-time non-singular sliding mode control robotic manipulator trajectory tracking

Arbitrarily rotating polarization direction and manipulating phases in linear and nonlinear ways using programmable metasurface

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Light(Science & Applications) 2024年第9期13卷 1789-1800页

作者： Wei Liu Si Ran Wang jun yan Dai Lei Zhang Qiao Chen Qiang Cheng Tie jun Cui State Key Laboratory of Millimeter Waves Southeast UniversityNanjing 210096China Institute of Electromagnetic Space Southeast UniversityNanjing 210096China Frontiers Science Center for Mobile Information Communication and Security Southeast UniversityNanjing 210096China Electrical Engineering Department Chalmers University of TechnologyGothenburg 41258Sweden

Independent controls of various properties of electromagnetic(EM)waves are crucially required in a wide range of *** metasurface is a promising candidate to provide an advanced platform for manipulating EM ***,we propose an approach that can arbitrarily control the polarization direction and phases of reflected waves in linear and nonlinear ways using a stacked programmable ***,we extend the space-timecoding theory to incorporate the dimension of polarization,which provides an extra degree of freedom for manipulating EM *** proof-of-principle application examples,we consider polarization rotation,phase manipulation,and beam steering at linear and nonlinear *** validation,we design,fabricate,and measure a metasurface *** experimental results show good agreement with theoretical predictions and *** proposed approach has a wide range of applications in various areas,such as imaging,data storage,and wireless communication.

关键词： surface. nonlinear rotating

Bio-inspired surface manipulation of halloysite nanotubes for highperformance flame retardant polylactic acid nanocomposites

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Nano Research 2024年第3期17卷 1595-1606页

作者： Yaru Sun Bin Yu yan Liu junbo yan Zixi Xu Bo Cheng Fenglei Huang jun Wang State Key Laboratory of Explosion Science and Technology Beijing Institute of TechnologyBeijing 100081China State Key Laboratory of Fire Science University of Science and Technology of ChinaHefei 230026China Beijing Institute of Technology Chongqing Innovation Center Chongqing 401120China National Engineering Research Center of Flame Retardant Materials Beijing Institute of TechnologyBeijing 100081China

High-performance flame-retardant polylactic acid(PLA)bio-composites based on biobased fillers to meet usage requirements represents a promising direction for creating a sustainable *** flame retardant PLA composites have been reported extensively,it still remains a huge challenge to develop mechanically *** flame retardant PLA composites due to plastication effect of organic flame retardants and poor compatibility of organic fillers with the matrix lead to the severe deterioration in mechanical *** this work,a bio-inspired surface manipulation strategy for halloysite nanotubes(HNTs)was proposed via a facile and green self-assembly *** structure and morphology of bio-inspired HNTs(b-HNTs)proved that biomass nanofillers(PA-NA-Fe)grew well both within the lumen and on the surface of *** growth of biomass on the inner and outer surfaces of HNTs was inspired from wooden towards enhancing the interface compatibility and imparting multi-properties to PLA *** mechanical properties(tensile,thermomechanical and anti-impact mechanical),great fire safety(heat release and smoke emission),thermostability and improved electromagnetic interference shielding effectiveness of this well-designed PLA nanocomposite were *** mechanisms of the enhanced performances of the PLA bio-composites by loading b-HNTs were *** work presents a facile and environmentally-friendly bio-inspired modification strategy for HNTs to fabricate high-performance,multi-functional polymer composites,which is also suitable for surface modification of many other nanomaterials,including nanofibers,nanotubes,nanowires,and nanosheets.

关键词： mechanical properties thermostability fire safety electromagnetic interference shielding biomass

Evaluating the tumor stratification with a lysosomal pH sensitive-probe by fluorescence lifetime imaging

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Chinese Chemical Letters 2024年第3期35卷 262-267页

作者： jun yan Xing Liang Qian Zhang Luolin Wang Weiying Lin guangxi Key Laboratory of Electrochemical Energy Materials Institute of Optical Materials and Chemical BiologySchool of Chemistry and Chemical EngineeringGuangxi UniversityNanning 530004China

Owing to the anaerobic metabolism in the tumor,abundant acidic metabolites are produced and accumulated in the ***,the cells in different tumor layers are directly linked to the pH ***,due to the lack of robust tools,the high-efficient evaluation of the acidic micro-environment of tumor stratification faces the challenge of accurate *** designed a new pH sensitive fluorescent lifetime probe target to *** we expected,the fluorescence lifetime of PLN possesses a good linear fit to the pH value,which could detect the pH change at a single lysosome level in real time,and then evaluate the different acidity of tumor *** probe PLN is successfully used to evaluate the tumor stratification by fluorescence lifetime imaging microscopy(FLIM)for the first time,which is of great significance in the preoperative diagnosis of clinical tumor treatment or evaluation of drug delivery effect.

关键词： FLIM pH Fluorescence imaging Lysosome Tumor imaging