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Towards creep property improvement of selective laser melted Ni-based superalloy IN738LC

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Journal of materials Science & Technology 2022年第17期112卷 301-314页

作者： H.y.Song m.C.Lam y.Chen S.Wu P.D.Hodgson X.H.Wu y.m.zhu A.J.Huang monash Centre for Additive manufacturing 15-17 Normanby RdNotting HillVIC 3168Australia Department for of materials Science and Engineering Monash UniversityClaytonVIC 3800Australia monash Centre for Electron microscopy 10 Innovation WalkClaytonVIC 3800Australia Institute for Frontier materials Deakin UniversityVIC 3216Australia

Nickel-based superalloy IN738LC produced by selective laser melting(SLm)exhibits inferior hightemperature creep properties than its cast counterparts due to relatively smaller grain size,particularly for the plane normal to the building *** work studied effects of post heating strategy on the microstructure and especially the grain size to improve the high temperature creep *** asbuilt microstructure exhibited a fine grain size and large quantities of mC carbides that could effectively hinder grain *** was found that unconventional two-step heat treatments could lead to substantial grain growth,and the effect is particularly prominent at a specific *** ease of grain growth was explained after classifying the microstructural evolution(boundary carbide transformation)during each heating step and related to the reduced grain boundary pinning force from mC *** tests validated the effect of the new heat treatment scheme on the SLm-processed IN738LC at 850℃.An extended creep fracture life(1.5 to 4 times improvement)and lower secondary creep rates were achieved with samples subjected to the newly optimized two-step heat *** complete creep curves are also firstly presented for SLm-IN738LC,confirming the effectiveness of grain growth and highlighting the importance of dedicated heat treatment for SLm superalloys.

关键词： Selective laser melting IN738LC alloy Creep properties Heat treatments Grain structure

Profile of Dr. Jiaojun zhu

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Science China(Life Sciences) 2025年第2期68卷 311-313页

作者： zhu, Jiaojun

Dr. Jiaojun zhu is the director general of Institute of Applied Ecology(IAE), Chinese Academy of Sciences(CAS)(2018 to present). He received his B.S. degree in Forest Science from Shenyang Agricultural University, China in July 1987, and subsequently joined Institute of Forestry and Soil, CAS(now known as the IAECAS) to pursue his m.S. degree in *** graduation, he served as a research assistant and an associate research fellow in the IAE-CAS from 1990 to 1996.

关键词： Forest pursue assistant

A water probe for direct pH measurement of individual particles via micro-Raman spectroscopy

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Journal of Environmental Sciences 2025年第3期149卷 200-208页

作者： Xiaoyu Cui mingjin Tang Tong zhu School of Environmental Science and Engineering Tianjin UniversityTianjin 300072China BIC-ESAT and SKL-ESPC College of Environmental Sciences and EngineeringPeking UniversityBeijing 100871China State Key Laboratory of Organic Geochemistry and Guangdong Key Laboratory of Environmental Protection and Resources Utilization Guangzhou Institute of GeochemistryChinese Academy of SciencesGuangzhou 510640China

The acidity of atmospheric aerosols influences fundamental physicochemical processes that affect climate and human *** recently developed a novel and facilewater-probebased method for directly measuring of the pH for micrometer-size droplets,providing a promising technique to better understand aerosol acidity in the *** complex chemical composition of fine particles in the ambient air,however,poses certain challenges to using a water-probe for pH measurement,including interference from interactions between compositions and the influence of similar compositions on water *** explore the universality of our method,it was employed to measure the pH of ammonium,nitrate,carbonate,sulfate,and chloride *** pH of particles covering a broad range(0–14)were accurately determined,thereby demonstrating that our method can be generally applied,even to alkaline ***,a standard spectral library was developed by integrating the standard spectra of common hydrated ions extracted through the *** library can be employed to identify particle composition and overcome the spectral overlap problem resulting from similar *** the spectral library,all ions were identified and their concentrations were determined,in turn allowing successful pH measurement of multicomponent(ammonium-sulfate-nitrate-chloride)*** into the synergistic effect of Cl^(–),NO_(3)^(–),and NH_(4)^(+)depletion obtained with our approach revealed the interplay between pH and volatile *** the ubiquity of component partitioning and pH variation in particles,the water probemay provide a new perspective on the underlying mechanisms of aerosol aging and aerosol–cloud interaction.

关键词： Particle pH Water probe Standard spectral library micro-Raman spectroscopy Direct measurement

“One stone, two birds”: Salt template enabling porosity engineering and single metal atom coordinating toward high-performance zinc-ion capacitors

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Journal of Energy Chemistry 2025年第1期100卷 637-645页

作者： Chunliu zhu Huanyu Liang Ping Li Chenglong Qiu Jingyi Wu Jingwei Chen Weiqian Tian yue zhu Zhi Li Huanlei Wang School of materials Science and Engineering Ocean University of ChinaQingdao 266100ShandongChina Department of Chemical and materials Engineering University of AlbertaAlberta T6G 2V4EdmontonCanada

Zinc-ion hybrid capacitors (ZIHCs) have received increasing attention as energy storage devices owing to their low cost,high safety,and environmental ***,their progress has been hampered by low energy and power density,as well as unsatisfactory long-cycle stability,mainly due to the lack of suitable electrode *** this context,we have developed manganese single atoms implanted in nitrogen-doped porous carbon nanosheets (mnSAs/NCNs) using a metal salt template method as cathodes for *** metal salt serves a dual purpose in the synthesis process:It facilitates the uniform dispersion of mn atoms within the carbon matrix and acts as an activating agent to create the porous *** applied in ZIHCs,the mnSAs/NCNs electrode demonstrates exceptional performance,including a high capacity of 203 m Ah g^(-1),an energy density of 138 Wh kg^(-1)at 68 W kg^(-1),and excellent cycle stability with 91%retention over 10,000 *** calculations indicate that the introduced mn atoms modulate the local charge distribution of carbon materials,thereby improving the electrochemical *** work demonstrates the significant potential of carbon materials with metal atoms in zinc-ion hybrid capacitors,not only in enhancing electrochemical performance but also in providing new insights and methods for developing high-performance energy storage devices.

关键词： Zinc ion hybrid capacitors Cathodes Carbon materials Heteroatoms Single atoms

Toxicity variability in Alexandrium pacificum isolated from East China Sea:impact of temperature and light intensity

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Journal of Oceanology and Limnology 2025年第1期43卷 147-158页

作者： Xuexia zhu Tianchi yIN min PANG Jun WANG The First Institute of Oceanography Ministry of Natural Resources of the People’s Republic of ChinaQingdao 266061China College of Animal Science and Technology Yangzhou UniversityYangzhou 225009China College of Oceanography Hohai UniversityNanjing 210098China

Suitable temperature and light intensity play important roles in the formation of harmful algae blooms(HABs),which can pose serious threats to aquatic ecosystems and human *** this study,we measured the growth,physiological function,and paralytic shellfish toxins(PSTs)production of Alexandrium pacificum(CCmA-272),a strain isolated from East China Sea,at different temperatures(15,20,and 25℃)and light intensities(30,60,and 90μmol photons/(m^(2)·s)).Results indicate that temperature and light intensity significantly affected the growth,physiology,and toxigenic potentials of *** optimal conditions for the growth of *** were observed at 20℃ under60μmol photons/(m^(2)·s).Regarding the production of PSTs,this strain of *** produced 12 PSTs,including carbamate toxins:saxitoxin(STX),neosaxitoxin(NEO),and gonyautoxin 1–4(GTX1,GTX2,GTX3,GTX4);dicarbamoyl toxins:dicarbamoylsaxitoxin(dcSTX),dicarbamoylgonyautoxin 2,3(dcGTX2,dcGTX3);and N-sulfocarbamoyl toxins:N-sulfocarbamoylgonyautoxin 1,2(C1,C2),and gonyautoxin 5(GTX5).Among all the PSTs,C2 was the most *** temperature(15℃)and high light intensity(90μmol photons/(m^(2)·s))were beneficial for the production of PSTs in *** cultured at 20 and 25℃,*** generated comparable total quantities of PSTs,yet the toxicity levels were lower at 25℃.Intra-cellular PSTs contents were greater than extra-cellular PSTs contents,except those under the condition of 25℃ with 30μmol photons/(m^(2)·s).However,as the increase of temperature,*** released more amounts of analogues with higher toxicity levels(e.g.,STX and dcGTX_(2))into the environment than *** findings emphasize the significant sensitivity of *** to temperature and light intensity,highlighting the importance of evaluating both intra-cellular and extra-cellular PSTs for assessing its toxicity and aiding in the prediction and management of HABs.

关键词： temperature light intensity Alexandrium pacificum paralytic shellfish toxin harmful algal bloom

Sequence-activated chemiluminescence probes:programmable illumination for high-contrast in vivo sensing and imaging

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Science China Chemistry 2025年第1期68卷 26-34页

作者： yutao Zhang Juan Li Wei-Hong zhu Zhiqian Guo Shanghai Key Laboratory of Functional materials Chemistry Joint International Research Laboratory of Precision Chemistry and Molecular EngineeringInstitute of Fine ChemicalsSchool of Chemistry and Molecular EngineeringEast China University of Science and TechnologyShanghai 200237China State Key Laboratory of Bioreactor Engineering Shanghai Frontier Science Research Base of Optogenetic Techniques for Cell MetabolismEast China University of Science&TechnologyShanghai 200237China

Sequence-activated chemiluminescence(CL)technique offers a unique approach to detecting specific biomolecules or cellular events with high sensitivity and spatial *** fundamental principle behind sequence-activated CL probes involves tailoring highly-controllable CL signals in response to specific sequences or events of interest,thus enabling high-contrast signals under complex physiological *** sequential activation could be triggered by enzymes,reactive oxygen species(ROS),biothiols or changes in the *** unique sequence-activated CL probes bestow several advantages,including minimal background,deep-tissue penetration,and the ability of non-invasive or minimally invasive *** sequence-activated CL techniques represent a significant advancement in molecular imaging and *** this mini-review,we focus on the latest developments in sequential CL probes,addressing the technical challenges and discussing the future trajectory by harnessing CL signaling and molecular recognition.

关键词： chemiluminescnece sequence-activation in-vivo bioimaging cyclic peroxide

Defect Engineering with Rational Dopants modulation for High‑Temperature Energy Harvesting in Lead‑Free Piezoceramics

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Nano-micro Letters 2025年第3期17卷 87-101页

作者： Kaibiao Xi Jianzhe Guo mupeng Zheng mankang zhu yudong Hou Key Laboratory of Advanced Functional materials Ministry of EducationCollege of Materials Science and EngineeringBeijing University of TechnologyBeijing 100124People’s Republic of China

High temperature piezoelectric energy harvester(HTPEH)is an important solution to replace chemical battery to achieve independent power supply of HT wireless ***,simultaneously excellent performances,including high figure of merit(FOm),insulation resistivity(ρ)and depolarization temperature(Td)are indispensable but hard to achieve in lead-free piezoceramics,especially operating at 250°C has not been reported ***,well-balanced performances are achieved in BiFeO3–BaTiO3 ceramics via innovative defect engineering with respect to delicate manganese *** to the synergistic effect of enhancing electrostrictive coefficient by polarization configuration optimization,regulating iron ion oxidation state by high valence manganese ion and stabilizing domain orientation by defect dipole,comprehensive excellent electrical performances(Td=340°C,ρ250°C>10^(7)Ωcm and FOm_(250°C)=4905×10^(–15)m^(2)N^(−1))are realized at the solid solubility limit of manganese *** HT-PEHs assembled using the rationally designed piezoceramic can allow for fast charging of commercial electrolytic capacitor at 250°C with high energy conversion efficiency(η=11.43%).These characteristics demonstrate that defect engineering tailored BF-BT can satisfy high-end HT-PEHs requirements,paving a new way in developing selfpowered wireless sensors working in HT environments.

关键词： Lead-free piezoceramic Defect engineering Dopants modulation High-temperature Piezoelectric energy harvester

mossbauer,optical and structural properties of Fe^(3+) ion in borate glass

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Journal of Rare Earths 2025年第1期43卷 162-170,I0006页

作者： Essam A.Elkelany Hesham y.Amin A.Samir m.m.EL-Hady H.H.El-Bahnasawy moukhtar A.Hassan Basic Science Department Faculty of EngineeringSinai UniversityAl-Arish45511Egypt School of Information and Electrical Engineering Hangzhou City UniversityHangzhou30015China State Key Laboratory of modern Optical Instrumentation College of Optical Science and EngineeringZhejiang UniversityHangzhou310027China Basic Science Department Faculty of Engineering at ShoubraBenha University11629Egypt Physics Department Faculty of ScienceAl-Azhar University11884CairoEgypt

Lanthanum-bearing iron lithium borate glass is a quaternary system for oxide glasses and was prepared via the melt-quenching *** present article correlates the structure,optical,ligand field and m?ssbauer data on iron lithium borate glass co ntaining La^(3+).The density was measured,while the molar volume was *** physical parameters are *** increasing the La_(2)O_(3) content within the glass network,infrared spectra analysis reveals structural modifications such as the increase in BO_(4) units and the decline in both BO_(3) units and NBO bonds ***,optical absorption spectra were *** absorption spectra disclose a plethora of electronic transitions that are related to Fe^(3+)in tetrahedral and octahedral sites,however,Fe^(2+)phase is not observed in optical spectra,but it has a clear signature in m?ssbauer ***,the glass absorption edges undergo a clear blue shift,reflecting an increased band gap energy(1.96-2.28 eV).The decline in NBO bonds justifies this ***,the values of crystal field splitting are increased,while the values of Racah parameters are *** trend is justified by the decline in NBO bonds and increases electron localization around Fe cations.m?ssbauer spectra confirm the existence of Fe^(3+)in tetrahedral and octahedral sites,while Fe^(2+)exists in only a tetrahedral *** increasing La_(2)O_(3) content,the isomer shift of Fe^(3+)in tetrahedral sites changes to be 0.312-0.329 mm/s,while the isomer shift of octahedral Fe^(3+)is 0.424-0.456 mm/*** findings coincide with optical *** the isomer shift of tetrahedral Fe^(2+)is 0.902-0.911 mm/*** results of structural,optical and ligand field associated with m?ssbauer spectra open more vistas toward the utility of these samples in the optics realm.

关键词： Fe3+ions Rare-earth oxide mossbauer spectra Ligand field parameters Optical properties

Domain generalization with semi-supervised learning for people-centric activity recognition

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Science China(Information Sciences) 2025年第1期68卷 171-188页

作者： Jing LIU Wei zhu Di LI Xing HU Liang SONG Academy for Engineering & Technology Fudan University Shanghai East-bund Research Institute on Networking Systems of AI School of Optoelectronic Information and Computer Engineering University of Shanghai for Science & Technology

People-centric activity recognition is one of the most critical technologies in a wide range of real-world applications,including intelligent transportation systems, healthcare services, and brain-computer interfaces. Large-scale data collection and annotation make the application of machine learning algorithms prohibitively expensive when adapting to new tasks. One way of circumventing this limitation is to train the model in a semi-supervised learning manner that utilizes a percentage of unlabeled data to reduce the labeling burden in prediction tasks. Despite their appeal, these models often assume that labeled and unlabeled data come from similar distributions, which leads to the domain shift problem caused by the presence of distribution gaps. To address these limitations, we propose herein a novel method for people-centric activity recognition,called domain generalization with semi-supervised learning(DGSSL), that effectively enhances the representation learning and domain alignment capabilities of a model. We first design a new autoregressive discriminator for adversarial training between unlabeled and labeled source domains, extracting domain-specific features to reduce the distribution gaps. Second, we introduce two reconstruction tasks to capture the task-specific features to avoid losing information related to representation learning while maintaining task-specific consistency. Finally, benefiting from the collaborative optimization of these two tasks, the model can accurately predict both the domain and category labels of the source domains for the classification task. We conduct extensive experiments on three real-world sensing datasets. The experimental results show that DGSSL surpasses the three state-of-the-art methods with better performance and generalization.

关键词： activity recognition deep learning domain generalization semi-supervised learning adversarial training

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