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Simultaneous enhancement of mechanical and shape memory properties by heat-treatment homogenization of Ti_(2)Ni precipitates in TiNi shape memory alloy fabricated by selective laser melting

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Journal of Materials Science & Technology 2022年第6期101卷 205-216页

作者： H.z.lu L.H.Liu C.yang X.luo C.H.Song z.Wang J.Wang y.D.Su y.F.Ding L.C.zhang y.y.Li National Engineering Research Center of Near-net-shape Forming for Metallic Materials South China University of TechnologyGuangzhou 510640China Musculoskeletal Oncology Department Sun Yat-Sen University Cancer CenterGuangzhouGuangdong ProvinceChina Shenyang Aircraft Design and Research Institute Shenyang 110035China Guangdong Huayi Plumbing Fittings Industry Co. Ltd.Kaiping 529321China School of Engineering Edith Cowan University270 Joondalup DriveJoondalupPerthWA 6027Australia

The excellent shape memory and mechanical properties of Ti Ni shape memory alloys(SMAs) fabricated using selective laser melting(SLM) are highly desirable for a wide range of critical applications. In this study, we examined the simultaneous enhancement of mechanical and shape memory properties using heat-treatment homogenization of Ti_(2)Ni precipitates in a Ti_(50.6)Ni_(49.4)SMA fabricated using SLM. Specifically, because of the complete solution treatment, nanoscale spherical Ti_(2)Ni precipitates were homogeneously dispersed throughout the grain interior. Interestingly, the resultant SMA exhibited an ultrahigh tensile strength of 880 ± 13 MPa, a large elongation of 22.4 ± 0.4%, and an excellent shape memory effect, with a recovery rate of > 98% and ultrahigh recoverable strain of 5.32% after ten loading–unloading cycles. These simultaneously enhanced properties are considerably superior than those of most previously reported Ti Ni SMAs fabricated using additive manufacturing. Fundamentally, the enhancement in tensile strength is ascribed to precipitation strengthening and work hardening, and the large plasticity is mainly attributed to the homogeneous nanoscale globular Ti_(2)Ni precipitates, which effectively impeded the rapid propagation of microcracks. Furthermore, the enhanced shape memory properties are derived from the suppression of dislocation movement and formation of retained stabilized martensite by the presence of high-density dislocations, nanoscale Ti_(2)Ni precipitates, and abundant interfaces. The obtained results provide insight into the enhancement of the two types of properties in Ti Ni SMAs and will accelerate the wider application of SMAs.

关键词： Shape memory alloy Selective laser melting Heat treatment Mechanical properties Shape memory properties

Mechanism of soft x-ray continuum radiation from low-energy pinch discharges of hydrogen and ultra-low field ignition of solid fuels

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Plasma Science and Technology 2017年第9期19卷 7-34页

作者： R MILLS J LOTOSKI y lu Brilliant Light Power Inc.493 Old Trenton RoadCranburyNJ 08512United States of America

EUV continuum radiation（10–30 nm） arising only from very low energy pulsed pinch gas discharges comprising some hydrogen was first observed at Black Light Power, Inc. and reproduced at the Harvard Center for Astrophysics（Cf A）. The source was determined to be due to the transition of H to the lower-energy hydrogen or hydrino state H（1/4） whose emission matches that observed wherein alternative sources were eliminated. The identity of the catalyst that accepts 3 · 27.2 eV from the H to cause the H to H（1/4） transition was determined to HOH versus 3H. The mechanism was elucidated using different oxide-coated electrodes that were selective in forming HOH versus plasma forming metal atoms as well as from the intensity profile that was a mismatch for the multi-body reaction required during 3H catalysis. The HOH catalyst was further shown to give EUV radiation of the same nature by igniting a solid fuel comprising a source of H and HOH catalyst by passing a low voltage, high current through the fuel to produce explosive plasma. No chemical reaction can release such high-energy light. No high field existed to form highly ionized ions that could give radiation in this EUV region that persisted even without power input. This plasma source serves as strong evidence for the existence of the transition of H to hydrino H（1/4） by HOH as the catalyst and a corresponding new power source wherein initial extraordinarily brilliant light-emitting prototypes are already producing photovoltaic generated electrical power. The hydrino product of a catalyst reaction of atomic hydrogen was analyzed by multiple spectroscopic techniques. Moreover, the m H catalyst was identified to be active in astronomical sources such as the Sun, stars and interstellar medium wherein the characteristics of hydrino match those of the dark matter of the Universe.

关键词： ignition continuum brilliant catalysis matches elucidated reproduced spectroscopic figure helium

Staged dendrite suppression for high safe and stable lithium-sulfur batteries

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Journal of Energy Chemistry 2025年第1期100卷 674-683页

作者： Jun Jiang zhenjie lu yanwen Ding Shujun Liu zhijie Qi Tian Tang yunfan zhang zhiyuan Ma Jingwen Sun Liang Xue Wenyao zhang Pan Xiong Xin Wang Junwu zhu yongsheng Fu Key Laboratory for Soft Chemistry and Functional Materials of Ministry of Education Nanjing University of Science and Technology Jiangsu Pylon Battery Co.Ltd

The unavoidable dendrite growth and shuttle effect have long been stranglehold challenges limiting the safety and practicality of lithium-sulfur ***,we propose a dual-action strategy to address the lithium dendrite issue in stages by constructing a multifunctional surface-negatively-charged nanodiamond layer with high ductility and robust puncture resistance on polypropylene （PP） *** uniformly loaded compact negative layer can not only significantly enhance electron transmission efficiency and promote uniform lithium deposition,but also reduce the formation of dendrite during early deposition *** importantly,under the strong puncture stress encountered during the deterioration of lithium dendrite growth under limiting current,the high ductility and robust puncture resistance（145.88 MPa） of as-obtained nanodiamond layer can effectively prevent short circuits caused by unavoidable lithium *** Li||Li symmetrical cells assembled with nanodiamond layer modified PP demonstrated a stable cycle of over 1000 h at 2 mA cm-2with a polarization voltage of only 29.3 ***,the negative charged layer serves as a physical barrier blocking lithium polysulfide ions,effectively mitigating capacity *** improved cells achieved a capacity decay of only 0.042%per cycle after 700 cycles at 3 C,demonstrating effective suppression of dendrite growth and capacity attenuation,showing promising prospect.

关键词： Ductility

Overcoming the strength-ductility trade-off by tailoring grain-boundary metastable Si-containing phase in β-type titanium alloy

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Journal of Materials Science & Technology 2021年第9期68卷 112-123页

作者： X.luo L.H.Liu C.yang H.z lu H.W.Ma z.Wang D.D.Li L.C.zhang y.y.Li National Engineering Research Center of Near-net-shape Forming for Metallic Materials South China University of TechnologyGuangzhou510640China State Key Laboratory of Materials Processing and Die&Mould Technology Huazhong University of Science and TechnologyWuhan430074China Key Laboratory of Automobile Materials of MOE Department of Materials ScienceJilin UniversityChangchun130012China School of Engineering Edith Cowan University270Joondalup DriveJoondalupPerthWA 6027Australia

It is well accepted that grain-boundary phases in metallic alloys greatly deteriorate the mechanical *** our work,we report on a novel strategy to prepare high strength-ductility β-type(Ti69.71 Nb23.72zr4.83Ta1.74)97Si3(at.%)(TNzTS) alloys by tailoring grain-boundary metastable Si-containing ***,the thin shell-shaped metastable S1 phase surrounding the columnar β-Ti grain was intercepted successfully via nonequilibrium rapid solidification achieved by selective laser melting(SLM).Subsequently,the thin shell-shaped metastable(Ti,Nb,zr)5 Si3(called S1) phase was transformed into globular(Ti,Nb,zr)2 Si(called S2) phase by the solution heat ***,the globular S2 phases reinforced TNzTS alloy exhibits ultrahigh yield strength of 978 MPa,ultimate strength of 1010 MPa and large elongation of 10.4 %,overcoming the strength-ductility trade-off of TNzTS alloys by various ***,the reported yield strength herein is 55 % higher than that of conventionally forged TNzT *** analysis indicates the globularization process of the metastable S1 phase is controlled by the model of termination *** quantitative analysis on strengthening mechanism demonstrates that the increase in yield strength of the heat-treated alloys is mainly ascribed to the strengthening of the precipitated silicide and the dislocations induced by high cooling *** obtained results provide some basis guidelines for designing and fabricating β-titanium alloys with excellent mechanical properties,and pave the way for biomedical application of TNzTS alloy by SLM.

关键词： Selective laser melting βtitanium alloys Heat treatment

Efficient large-area flexible organic photovoltaic modules on transparent thin silver electrodes

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Science China Chemistry 2025年

作者： Cong Xie zedong Xiong Xinlu Liu Wen Wang yang Liu Xueshi Jiang Xin lu lulu Sun yinhua zhou Wuhan National Laboratory for Optoelectronics Huazhong University of Science and Technology Kunming Institute of Physics

Large-area flexible organic photovoltaic（OPV） modules are challenging to achieve high power conversion efficiency（PCE）.Electrical shunts or shortages generally occur in large-area OPV modules due to the ultrathin（100–200 nm） and soft active layers. Improving the surface smoothness of bottom transparent electrode will be able to suppress the shunts and shortages. In this work, we report a method to fabricate smooth and flexible transparent electrodes based on thin silver film, and further to fabricate efficient large-area flexible OPV modules. The fabricated thin silver transparent electrodes simultaneously have high conductivity, high optical transmittance, good mechanical flexibility and low surface roughness. Humidity exposure（h.e.）treatment on MoO3effectively facilitates the continuous growth of the thin transparent silver electrode. 6 nm silver film on MoO3（h.e.） on plastic substrate shows a transmittance up to 89%, a sheet resistance of 15 Ω/sq, and a low surface roughness with a rootmean-square value of 0.276 nm. Furthermore, 52-cm2flexible organic solar modules（15 subcells） showed a certified PCE of12.66%. Furthermore, a 1350 cm2flexible component assembled by 25 pieces of 52–55 cm2modules showed certified PCE of12.10% with an open-circuit voltage of 62.85 V.

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Derimorphisms over Algebras and Applications

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Algebra Colloquium 2023年第2期30卷 193-204页

作者： X.Cao S.H.Liu X.S.lu z.J.ye z.R.yu y.H.zhang School of Mathematical Sciences Shanghai Jiao Tong University 800 Dongchuan RoadShanghai 200240China MoE Key Lab of Scientific and Engineering Computing Shanghai Jiao Tong University 800 Dongchuan RoadShanghai 200240China

The new concept"derimorphism"generalizing both derivation and homomor-phism is *** a derimorphism is invertible,its inverse is a Rota-Baxter *** general theory of derimorphism is *** classification of all derimorphisms over an associative unital algebra is *** to the nonexistence of nontriv-ial positive derivations,it is shown that nontrivial positive derimorphisms do exist over any pair of opposite orderings over R[x],the lattice-ordered full matrix algebra and upper triangular matrix algebra over a totally ordered field.

关键词： derimorphism Rota-Baxter operator opposite orderings positive derimor-phism

Carbon dots self-assembly enables near-infrared emission

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Science China Chemistry 2025年

作者： Shurong Ding Shasha Liu yuzhuo yang Linlin Shi yongqiang zhang Jingkun yu Haoqiang Song yingge Shi Siyu lu College of Chemistry Pingyuan Laboratory Zhengzhou University Henan Institute of Advanced Technology Zhengzhou University

In the fields of biomedicine, detection, and anti-counterfeiting, there is a widespread demand for cost-effective, easily synthesized, and environmentally friendly near-infrared(NIR) materials. Carbon dots(CDs), a cheap and non-toxic zero-dimensional carbon nanomaterial exhibiting exceptional photoluminescence(PL) properties and facile structural modification, have emerged as a promising candidate for the development of novel NIR materials. This study presents the synthesis of CDs capable of emitting a wide range of wavelengths from blue to NIR(456–836 nm) as their concentrations increase. The incorporation of oxygen and nitrogen co-doped atoms facilitates the optimization of non-coplanar angles, thereby promoting favorable π-πstacking interactions. This leads to the formation of metal-free rigid clusters through interconnecting adjacent nanoparticles in a gear-like meshing pattern through self-assembly. Consequently, intramolecular motion is constrained, vibration coupling is mitigated, non-radiative transition losses are minimized, and efficient NIR emission from CD clusters in high concentrations is ensured. Furthermore, NIR light-emitting diode(NIR LED) based on the CD clusters was successfully fabricated and employed for various applications including information encryption, anti-counterfeiting, and penetration detection in the field of NIR imaging.

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A novel flexible nerve guidance conduit promotes nerve regeneration while providing excellent mechanical properties

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Neural Regeneration Research 2025年第7期20卷 2084-2094页

作者： Tong Li Quhan Cheng Jingai zhang Boxin Liu yu Shi Haoxue Wang Lijie Huang Su zhang Ruixin zhang Song Wang Guangxu lu Peifu Tang zhongyang Liu Kai Wang Department of Orthopedics the Fourth Medical Center of Chinese PLA General HospitalBeijingChina Department of Training and Sports Medicine Characteristic Medical Center of Chinese People’s Armed Police ForceTianjinChina Medical School of Chinese PLA BeijingChina Key Laboratory of Bioactive Materials for the Ministry of Education College of Life SciencesNankai UniversityTianjinChina Department of Orthopedics Tianjin HospitalTianjinChina Department of Rehabilitation Medicine Er Quan Hospital of PAPWuxiJiangsu ProvinceChina

Autografting is the gold standard for surgical repair of nerve defects>5 mm in length;however,autografting is associated with potential complications at the nerve donor *** an alternative,nerve guidance conduits may be *** ideal conduit should be flexible,resistant to kinks and lumen collapse,and provide physical cues to guide nerve *** designed a novel flexible conduit using electrospinning technology to create fibers on the innermost surface of the nerve guidance conduit and employed melt spinning to align ***,we prepared disordered electrospun fibers outside the aligned fibers and helical melt-spun fibers on the outer wall of the electrospun fiber *** presence of aligned fibers on the inner surface can promote the extension of nerve cells along the *** helical melt-spun fibers on the outer surface can enhance resistance to kinking and compression and provide *** novel conduit promoted nerve regeneration and functional recovery in a rat sciatic nerve defect model,suggesting that it has potential for clinical use in human nerve injuries.

关键词： aligned fibers anti-kinking helical fibers nerve guidance conduit nerve regeneration peripheral nerve injury topological guidance

Dietary carbohydrate intake and risk of type 2 diabetes:a 16-year prospective cohort study

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Science China Life Sciences 2025年

作者： lu Gan yi yang Bin zhao Kai yu Kehua Guo Fang Fang zhiguang zhou Demetrius Albanes Jiaqi Huang Key Laboratory of Diabetes Immunology Ministry of Education and Department of Metabolism and Endocrinology The Second Xiangya Hospital of Central South University CSU-Sinocare Research Center for Nutrition and Metabolic Health Xiangya School of Public Health Central South UniversityFurong Laboratory Division of Cancer Epidemiology and Genetics National Cancer Institute NIH Department of Health and Human Services School of Computer Science and Engineering Central South University Institute of Environmental Medicine Karolinska Institute National Clinical Research Center for Metabolic Diseases Key Laboratory of Diabetes Immunology Ministry of Education and Department of Metabolism and Endocrinology The Second Xiangya Hospital of Central South University

Despite considerable research underscoring the importance of carbohydrate intake in relation to the risk of type 2 diabetes(T2D), a comprehensive assessment of this relationship is currently lacking. We aimed to examine the associations of various types and food sources of dietary carbohydrate intake with the risk of T2D, to evaluate potential effect modification by other factors, including genetic susceptibility,and to explore the potential mediators for such associations. The present study included 161,872 participants of the UK Biobank who were free of prevalent cancer, cardiovascular disease, or diabetes, and had at least one validated 24-h dietary recall assessment. Multivariableadjusted age-stratified Cox proportional hazard regression models were applied to estimate hazard ratios(HRs) and 95% confidence intervals(CI) for the associations of various types and food sources of dietary carbohydrate intake with risk of T2D. During a median follow-up of13.6 years, 4,176 incident cases of T2D were identified. In the multivariable-adjusted models, a greater intake of fiber, carbohydrates from whole grains, and carbohydrates from non-starchy vegetables was significantly associated with a lower risk of T2D(highest vs. lowest quantile, HR [95% CI]=0.70 [0.62–0.79], 0.74 [0.67–0.82], and 0.83 [0.75–0.92], respectively, all P for trend ydrate from starchy vegetables was associated with an increased risk of T2D(highest vs. lowest quantile, HR [95%CI]=1.31 [1.16–1.48] and 1.19 [1.09–1.31], respectively, both P for trend y vegetables with an equal amount of whole grains or non-starchy vegetables was associated with 4% to 10% lower risk of T2D(all P values y similar across population subgroups, including individuals with different genetic susceptibility to T2D. Mediation analyses of the inverse association between T

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