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Rare Metals 2019年第12期38卷 1178-1186页

作者： jian-Chao Wang Hong-Sheng Luo Ming-Hai Zhang Xi-Hong Zu Jie Zhang Yu-xin gu guo-Bin Yi School of Chemical Engineering and Light Industry Guangdong University of TechnologyGuangzhou 510006China guangdong Provincial Key Laboratory of Advanced Coatings Research and Development China National Electric Apparatus Research Institute Co.Ltd.Guangzhou 510300China

A new substrate,aligned Ag nanowires decorated with silver nanoparticle composite structure(AgNWs@AgNPs),was fabricated to investigate metalenhanced fluorescence(MEF) and its *** new composite structure was fabricated via a three-phase interface assembly method followed by SnCl2 sensitization and AgNO3 reduction *** size and distribution of the nanoparticles on silver nanowires increased with the sensitization and reduction *** formation of AgNPs on the surfaces of AgNWs was confirmed by multiple characterization methods including scanning electron microscopy(SEM),transmission electron microscope(TEM),atomic force microscopy(AFM) and X-ray diffraction(XRD).The results show that the fluorescence intensity of the poly(3-hexylthiophene)(P3HT) on the composite structure was greatly enhanced compared with that on bare glass substrate,and the intensity increased with the increase in particle sizes and *** mechanism was basedo n the increase in excitation rate and the radiation decay *** new type of substrate could serve as a good and efficient MEF substrate for high-performance fluorescence-based devices.

关键词： Fluorescence enhancement Aligned Ag nanowires Self-assembly Mechanism

Superconducting Single-Layer T-Graphene and Novel Synthesis Routes

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Chinese Physics Letters 2019年第9期36卷 46-63页

作者： Qinyan gu Dingyu xing jian Sun National Laboratory of Solid State Microstructures School of Physics and Collaborative Innovation Center of Ad vanced MicrostructuresNanjing UniversityNanjing 210093

Single-layer superconductors are ideal materials for fabricating superconducting nano ***,up to date,very few single-layer elemental superconductors have been predicted and especially no one has been successfully synthesized ***,using crystal structure search techniques and ab initio calculations,we predict that a single-layer planar carbon sheet with 4-and 8-membered rings called T-graphene is a new intrinsic elemental superconductor with superconducting critical temperature(Tc)up to around 20.8 *** importantly,we propose a synthesis route to obtain such a single-layer T-graphene,that is,a T-graphene potassium intercalation compound(C4 K with P4/mmm symmetry)is firstly synthesized at high pressure(>11.5 GPa)and then quenched to ambient condition;and finally,the single-layer T-graphene can be either exfoliated using the electrochemical method from the bulk C4 K,or peeled off from bulk T-graphite C4,where C4 can be obtained from C4 K by evaporating the K ***,we find that the calculated Tc of C4 K is about 30.4 K at 0 GPa,which sets a new record for layered carbon-based *** present findings add a new class of carbon-based *** particular,once the single-layer T-graphene is synthesized,it can pave the way for fabricating superconducting devices together with other 2 D materials using the layer-by-layer growth techniques.

关键词： red Superconducting Single-Layer T-Graphene and Novel Synthesis Routes Graphene

PREDICTION OF VORTEX-INDUCED VIBRATION OF LONG FLEXIBLE CYLINDERS MODELED BY A COUPLED NONLINEAR OSCILLATOR:INTEGRAL TRANSFORM SOLUTION

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Journal of Hydrodynamics 2012年第6期24卷 888-898页

作者： gu Ji-jun AN Chen LEVI Carlos SU jian Ocean Engineering Program COPPEUniversidade Federal do Rio de Janeiro Nuclear Engineering Program COPPEUniversidade Federal do Rio de Janeiro

The Generalized Integral Transform Technique （GITT） was applied to predict dynamic response of Vortex-Induced Vibration （VIV） of a long flexible cylinder. A nonlinear wake oscillator model was used to represent the cross-flow force acting on the cylinder, leading to a coupled system of second-order Partial Differential Equations （PDEs） in temporal variable. The GITT approach was used to transform the system of PDEs to a system of Ordinary Differential Equations （ODEs）, which was numerically solved by using the Adams-Moulton and Gear method （DIVPAG） developed by the International Mathematics and Statistics Library （IMSL）. Numerical results were presented for comparison to those given by the finite difference method and experimental results, allowing a critical evaluation of the technique performance. The influence of variation of mean axial tension induced by elongation of flexible cylinder was evaluated, which was shown to be not negligible in numerical simulation of VIV of a long flexible cylinder.

关键词： Vortex-Induced Vibration (VIV) nonlinear wake oscillator flexible cylinder integral transform

Study on Enzymatic Hydrolysis of Gadus morrhua Skin Collagen and Molecular Weight Distribution of Hydrolysates

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Agricultural Sciences in China 2009年第6期8卷 723-729页

作者： HUO jian-xin ZHAO Zheng Jinzhong University Jinzhong 030600 P.R. China College of Food Engineering ＆ Biotechnology Tianjin University of Science ＆ Technology Tianjin 300457 P.R.China

Process parameters on enzymatic hydrolysis and molecular weight （MW） distribution of collagen hydrolysates from Gadus morrhua skin were investigated. The optimal process parameters were obtained by the single-factor and orthogonal experiments. The molecular weight distribution of hydrolysates was determined using both Sephadex G25 partition and high speed liquid chromatography electricity spray mass spectrum （HPLC-ESI-MS）. Collagen hydrolysates were first gained by an alkaline protease ＂alcalase＂ for 3 h at temperature （50~C）, pH （10.0）, substrate concentration （75 g L-~）, and E/S （3%）. The molecular weight distribution of collagen hydrolysates ranged from 300 to 1 500 Da, and most of peptides were under 1 200 Da. Sephadex G25 partition and HPLC-ESI-MS should be successfully employed to determine the molecular weight distribution of collagen hydrolysates.

关键词： collagen hydrolysates Gadus morrhua molecular weight distribution alkaline protease

Effect of Initial Concentration on Adsorption-Desorption Characteristics and Desorption Hysteresis of Hexachlorobenzene in Soils

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Pedosphere 2010年第1期20卷 104-110页

作者： GAO Hong-jian jianG xin School of Resources and Environmental Science Anhui Agricultural University Hefei 230036 (China) State Key Lab of Soil and Sustainable Agriculture Institute of Soil Science Chinese Academy of Sciences Nanjing 210008 (China)

Adsorption and desorption are important processes that influence the transport, transformation, and bioavailability of hexachlorobenzene (HCB) in soils. To examine the adsorption-desorption characteristics of HCB, equilibrium batch experiments were carried out using two soils (red soil and paddy soil) with different initial HCB concentrations (0.25, 0.50, 0.75, 1.00, 1.50, 2.50, 3.50, and 5.00 mg L-1 ) by using 0.01 mol L-1 calcium chloride as the background solution. The successive desorption experiments (48, 96, 144, 192, and 240 h) were conducted after each adsorption equilibrium experiment. The results revealed that adsorption and desorption isotherms of HCB on two soils were nonlinear, which can be best described by the Freundlich equation with the square of the correlation coefficient (r 2 ) ranging from 0.97 to 0.99. Desorption of HCB from the two soils exhibited hysteresis at all HCB concentrations because the Freundlich desorption coefficients were always higher than the Freundlich adsorption coefficients. The hysteretic effect was enhanced with increasing initial HCB concentration, and positive hysteresis was observed at different concentrations.

关键词： Freundlich equation sorption coefficients sorption isotherms

Homology Cycles and Dependent Cycles of Hypergraphs

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Acta Mathematicae Applicatae Sinica 2018年第2期34卷 237-248页

作者： jian-fang WANG xin XU Academy of Mathematics and Systems Science Chinese Academy of Sciences Beijing 100190 China School of Sciences North China University of Technology Beijing 100144 China

In this paper, some new concepts for hypergraphs are introduced. Based on the previous results, we do further research on cycle structures of hypergraphs and construct a more strictly complete cycle structure system o... 详细信息

关键词： hypergraph semilattice cycle maximal cycle homology cycle

DIAGNOSTIC VALUE OF WHOLE BODY DIFFUSION WEIGHTED IMAGING FOR SCREENING PRIMARY TUMORS OF PATIENTS WITH METASTASES

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Chinese Medical Sciences Journal 2008年第3期23卷 145-150页

作者： Tai-fu gu xin-lan Xiao Fei Sun jian-hua Yin Hai Zhao Department of Radiology the Second Affiliated Hospital of Nanchang University Nanchang 330006 MR Modality General Electric Healthcare China Beijing 100172

Objective To evaluate the values of whole body diffusion weighted imaging （DWI） in screenmg pnmary unknown tumor in patients with metastases. Methods Totally, 34 patients with metastases of primary unknown tumors were scanned with whole body DWI, and conventional magnetic resonance （MR） imaging was performed if suspected lesions were detected. All the metastases including 27 cases of osseous metastases, 2 brain metastases, 2 liver metastases, 1 pulmonary multiple metastasis, 1 neck metastasis and 1 malignant ascites, were diagnosed by computed tomography, single photon emission computed tomography, or MR imaging. For the proven primary tumors diagnosed by biopsy or pathology of surgical specimens, apparent diffusion coefficient （ADC） values of the primary and metastatic lesions were measured respectively. The sensitivity and specificity of this technique for screening primary tumors were cvaluated. Results We found 24 cases with suspected primary lesions, in which 23 lesions were proved to be primary tumors, and 1 was proved to be benign lesion. And no definite primary lesion was found in 10 cases on whole body DWI, but in which 1 case was diagnosed with primary tumor by biopsy later, and the other 9 cases remained unknown within follow-up of over halfa year. The difference was not significant in ADC values between primary and metastatic lesions （P〉0.05）. The sensitivity and specificity of whole body DWI for searching primary tumors was 95.8% and 90.0%, respectively. Conclusion Combined with conventional MR scanning, whole body DWI can help to search primary lesions of patients with metastases.

关键词： diffusion weighted imaging primary tumor neoplasm metastasis whole body

Recovery of greenhouse gas as cleaner fossil fuel contributes to carbon neutrality

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Green Energy & Environment 2023年第2期8卷 351-353页

作者： xin Zhang jian-Rong Li Beijing Key Laboratory for Green Catalysis and Separation and Department of Chemical Engineering Faculty of Environment and LifeBeijing University of TechnologyBeijing 100124China

Under the context of carbon neutrality of China,it is urgent to shift our energy supply towards cleaner fuels as well as to reduce the greenhouse gas ***,coal is the main fossil fuel energy source of *** country is striving hard to replace it with methane,a cleaner fossil *** China has rich geological resources of methane as coal bed methane(CBM)reserves,it is quite challenging to utilize them due to low *** CBM is however mainly emitted directly to atmosphere during coal mining,causing waste of the resource and huge contribution to greenhouse *** recent work by Yang et *** a potential solution to extract low concentration methane selectively from CBM through using MOF materials as *** kind of materials and associated separation technology are promising to reduce greenhouse gas emission and promote the methane production capability,which would contribute to carbon neutrality in dual pathways.

关键词： Carbon neutrality Coal bed methane Metal–organic frameworks Greenhouse gas Fossil fuel

LOW DOSE PIRFENIDONE SUPPRESSES TRANSFORMING GROWTH FACTOR BETA-1 AND TISSUE INHIBITOR OF METALLOPROTEINASE-1, AND PROTECTS RATS FROM LUNG FIBROSIS INDUCED BY BLEOMYCIN

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Chinese Medical Sciences Journal 2006年第3期21卷 145-151页

作者： xin-lun Tian Wei Yao Zi-jian guo Li gu Yuan-jue Zhu Department of Respiratory Medicine Peking Union Medical College Hospital Chinese Academy of Medical Sciences ＆Peking Union Medical College Beijing 100730

Objective To investigate the optimal dosage of pirfenidone for the treatment of pulmonary fibrosis induced by bleomycin in Wistar rats, and the alteration of expressions of transforming growth factor beta-1 （ TGF-β1 ）, tissue inhibitor of metalloproteinase-1 （ TIMP-1 ）, and matrix metalloproteinase-13 （ MMP-13 ） in lung tissue. Methods Male Wistar rats were endotracheally instilled with bleomycin or normal saline. Pirfenidone （25-800 mg · kg^-l · d^-1 ）, dexamethasone （3 mg/kg）, or 1% carboxymethylcellulose sodium were given daily by feed 2 days before instillation of bleomycin. Groups T7 and T14 were fed pirfenidone 50 mg · kg^-1 · d^-1 at 7 days or 14 daYs after bleomycin instillation. Lungs were harvested at 28 days after bleomycin instillation. Patholological changes in luffg tissues were evaluated with HE staining. Lung collagen was stained by sirius red and measured by content of hydroxypro- line. Expression of proteins of TGF-β1 TIMP-1, and MMP-13 were detected by Western blotting. Results At doses of 25, 50, and 100 mg· kg^- 1 · d ^- 1, pirfenidone had significant anti-fibrotic effects for bleomy- cin-induced rat pulmonary fibrosis, and these effects were most significantly attenuated at the dosage of 50 mg · kg^-1 ·d^ -1（ HE： P 〈 0. 01, P 〈 0.01, and P = 0.064; sirius red： P 〈0.05, P 〈 0.01, and P 〈 0.05 ; hydroxyproline： P = 0.595, P 〈 0.01, and P = 0.976）. Pirfenidone at a dosage of 50 mg · kg^- l · d^-1 inhibited protein expression of TGF-131 and TIMP-1 in lung tissue in the early phase （0.79 and 0.75 times of control group）, but had no effect on ex- nr^eelnn nf MMP-13. Conclusion Low dose pirfenidone, especially at dosage of 50 mg · kg^-1 · d^-1, has significant anti-fibrotic effects on bleomycin-induced rat pulmonary fibrosis. Pirfenidone partially inhibits the enhancement of the expression of TGF-131 and TIMP-β1 in lung tissue.

关键词： pulmonary fibrosis bleomycin pirfenidone transforming growth factor beta-1 tissue inhibitor of metalloproteinase-1

First Enantioselective Synthesis of Isoamericanol A and Isoamericanin A

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Chinese Chemical Letters 2001年第6期12卷 485-486页

作者： Wen xin gu An xin WU Xue Gong SHE xin Fu PAN Department of Chemistry National Laboratory of Applied Organic ChemistryLanzhou UniversityLanzhou 730000

The first enantioselective synthesis approach to two chiral 1,4-benzodioxane neolignans isoamericanol A and isoamericanin A was reported.

关键词： Enantioselective synthesis 1 4-benzodioxane neolignans