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Chinese Chemical Letters 2007年第1期18卷 89-90页

作者： Ming Hui xiang xian bo shi Na Li Ke An Li College of Chemistry and Molecular Engineering Peking University Beijing 100871 China

Tris （2, 2′-bipyridine） ruthenium （Ⅱ）（Ru（bpy）3^2＋） dichloride was successfully immobilized into the galleria of layered gamma zirconium phosphate （γ-ZrP） preintercalated by butyl amine（BA）. The compou... 详细信息

关键词： Tris (2, 2′-bipyridine) ruthenium Zirconium phosphate Immobilization Luminescence

Effect of Rare Earth and Cooling Process on Microstructure and Mechanical Properties of an Ultra-Cleaned X80 Pipeline Steel

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Acta Metallurgica Sinica(English Letters) 2021年第5期34卷 639-648页

作者： He Duan Yi-Yin Shan Ke Yang xian-bo shi Wei Yan Yi Ren Institute of Metal Research Chinese Academy of SciencesShenyang110016China School of Materials Science and Engineering University of Science and Technology of ChinaShenyang110016China State Key Laboratory of Metal Materials and Application for Marine Equipment Anshan114009China

In order to explore the eff ect of a small amount of rare earth addition in ultra-cleaned pipeline steel and the influence of the cooling process on the tensile and impact properties,three API X80 pipeline steels were fabricated by varying RE addition and the cooling process at the same *** microstructures with different features for a low C high Nb microalloyed high-strength pipeline steel and the corresponding mechanical properties were *** results showed that even in the ultra-cleaned steel with O and S contents less than 10 ppm,the addition of RE would still cause an increase in the volume fraction of inclusions consisting of complicated RE oxysulfide and RE *** inclusions formed in the 112 ppm RE steel were harmful to the low temperature toughness,while few inclusions formed in the 47 ppm RE steel had almost no influence on the low temperature *** two RE additions had no effect on strength of the *** the finishing cooling temperature was increased and the cooling rate was decreased within a certain range,the volume fractions of polygonal ferrite and quasi-polygonal ferrite as well as the number density and size of martensite–austenite islands were *** such combined effect,the strength of the steels had almost no *** the finishing cooling temperature was increased from 481 to 584℃and the cooling rate was reduced from 20 to 13℃/s,for the steel with 112 ppm addition of RE,there was an obvious decrease in the low temperature *** reduced value(about 33 J)of the USE of steel consisted of two parts including the influence(about 18 J)of more inclusions formed due to 112 ppm addition of RE and the eff ect(about 15 J)of the lower high-angle grain boundaries.

关键词： Low temperature toughness Cooling process High-angle grain boundaries(HAGBs) Ductile–brittle transition temperature(DBTT) Rare earth Inclusions

HIC and SSC Behavior of High-Strength Pipeline Steels

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Acta Metallurgica Sinica(English Letters) 2015年第7期28卷 799-808页

作者： xian-bo shi Wei Yan Wei Wang Lian-Yu Zhao Yi-Yin Shan Ke Yang Institute of Metal Research Chinese Academy of Sciences University of Chinese Academy of Sciences Petro China Pipeline Company

In this study,hydrogen-induced cracking（HIC） and sulfide stress corrosion cracking（SSC） behaviors of highstrength pipeline steels in four different strength grades（X70,X80,X90 and X100） with the microstructure of acicular ferrite were *** results showed that both of X70 and X80 steels exhibited better HIC resistance,and their susceptibility to HIC increased with the strength *** parameters,including cracking length ratio,cracking thickness ratio（CTR） and cracking sensitivity ratio,were all increased,and among these,the CTR increased most,with the increase in the strength *** was found to initiate and grow along the hard boundaries such as large size martensite/austenite（M/A） islands and bainitic *** addition,the density of hydrogen-induced blister on the steel surface was increased with the decrease in p H value for the same-grade pipeline *** susceptibilities of X80,X90 and X90-C were revealed to subsequently decrease,which was related to the large size M/A islands.

关键词： Hydrogen-induced cracking Sulfide stress corrosion cracking High-strength pipeline steel Martensite/austenite island (M/A)

Strength, strain capacity and toughness of five dual-phase pipeline steels

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Journal of Iron and Steel Research International 2021年第6期28卷 752-761页

作者： Yi Ren xian-bo shi Zhen-guo Yang Yi-yin Shan Wei Ye Gui-xi Cai Ke Yang State Key Laboratory of Metal Material for Marine Equipment and Application Anshan 114009LiaoningChina CAS Key Laboratory of Nuclear Materials and Safety Assessment Institute of Metal ResearchChinese Academy of SciencesShenyang 110016LiaoningChina Institute of Metal Research Chinese Academy of SciencesShenyang 110016LiaoningChina

The effect of microstructures on strength,strain capacity and low temperature toughness of a micro-alloyed pipeline steel was *** various dual-phase microstructures,namely,acicular ferrite and a small amount of(around 2 vol.%)polygonal ferrite(AF+PF),polygonal ferrite and bainite(PF+B),polygonal ferrite and martensite/austenite islands(PF+M/A),polygonal ferrite and martensite(PF+M)and elongated polygonal ferrite and martensite(ePF+M),have been *** results show that AF+PF microstructure has high yield strength and excellent low temperature toughness,whereas its yield ratio is the *** ferrite-based dual-phase steels,PF+B,PF+M/A and PF+M microstructures show better strain capacity and low temperature *** strain capacity and low temperature toughness of ePF+M microstructure are the worst due to its high *** relationship between microstructure,strength,strain capacity and toughness has been *** on the results,the optimum microstructure for a better combination of strength,strain capacity and toughness is suggested to be the one having appropriate polygonal ferrite as second phase in an acicular ferrite matrix.

关键词： Pipeline steel Dual-phase microstructure Strength Strain capacity Toughness

Effect of Microstructure on Hydrogen Induced Cracking Behavior of a High Deformability Pipeline Steel

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Journal of Iron and Steel Research International 2015年第10期22卷 937-942页

作者： xian-bo shi Wei YAN Wei WANG Lian-yu ZHAO Yi-yin SHAN Ke YANG Institute of Metal Research Chinese Academy of Sciences University of Chinese Academy of Sciences Petro China Pipeline Company

The hydrogen induced cracking （HIC） behavior of a high deformability pipeline steel was investigated with three different dual-phase microstructures, ferrite and bainite （F＋B）, ferrite and martensite/austenite islands （F＋M/A） and ferrite and martensite （F＋M）, respectively. The HIC test was conducted in hydrogen sulfide （H2S）-saturated solution. The results showed that the steels with F＋B and F＋M/A dual-phase microstructures had both higher deformability and better HIC resistance, whereas the harder martensite phase in F＋M microstructure was responsible for the worst HIC resistance. The band-like hard phase in dual-phase mi- crostructure was believed to lead to increasing susceptibility to HIC.

关键词： pipeline steel high deformability dual-phase microstructure mechanical property hydrogen induced cracking

Effect of Cu Addition in Pipeline Steels on Microstructure,Mechanical Properties and Microbiologically Influenced Corrosion

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Acta Metallurgica Sinica(English Letters) 2017年第7期30卷 601-613页

作者： xian-bo shi Wei Yan Mao-Cheng Yan Wei Wang Zhen-Guo Yang Yi-Yin Shan Ke Yang Institute of Metal Research Chinese Academy of SciencesShenyang 110016China University of Chinese Academy of Sciences Beijing 100049China

In the present study, Cu-modified pipeline steels were fabricated to mitigate MIC by the antimicrobial ability of Cu element. The microstructure, mechanical properties and the antimircobial performance of the Cu-modified steel were systematically investigated. The Cu-modified steels showed good antimicrobial performance with remarkable strength enhancement by nanoscale Cu-rich precipitates and good impact toughness without changing the original base microstructures after the optimal aging treatment of 500 °C/1 h.

关键词： Pipeline steel Cu addition Mechanical properties Microstructure Antimicrobial performance

Chemical modification of barite for improving the performance of weighting materials for water-based drilling fluids

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Petroleum Science 2024年第1期21卷 551-566页

作者： Li-Li Yang Ze-Yu Liu shi-bo Wang xian-bo He Guan-Cheng Jiang Jie Zhang MOE Key Laboratory of Petroleum Engineering State Key Laboratory of Petroleum Resources and ProspectingChina University of Petroleum(Beijing)Changping DistrictBeijing102249China MOE Key CNPC Drilling Research Institute Changping DistrictBeijing102206China

With increasing drilling depth and large dosage of weighting materials,drilling fluids with high solid content are characterized by poor stability,high viscosity,large water loss,and thick mud cake,easier leading to reservoir damage and wellbore *** this paper,micronized barite(MB)was modified(mMB)by grafting with hydrophilic polymer onto the surface through the free radical polymerization to displace conventional API barite *** suspension stability of water-based drilling fluids(WBDFs)weighted with API barite:mMB=2:1 in 600 g was significantly enhanced compared with that with API barite/WBDFs,exhibiting the static sag factor within 0.54 and the whole stability index of *** viscosity and yield point reached the minimum,with a reduction of more than 40%compared with API barite only at the same *** multi-stage filling and dense accumulation of weighting materials and clays,filtration loss was decreased,mud cake quality was improved,and simultaneously it had great reservoir protection performance,and the permeability recovery rate reached 87%.In addition,it also effectively improved the lubricity of *** sticking coefficient of mud cake was reduced by 53.4%,and the friction coefficient was ***,mMB can serve as a versatile additive to control the density,rheology,filtration,and stability of WBDFs weighted with API barite,thus regulating comprehensive performance and achieving reservoir protection *** work opened up a new path for the productive drilling of extremely deep and intricate wells by providing an efficient method for managing the performance of high-density WBDFs.

关键词： Drilling fluids Weighting materials Filtration control Reservoir protection Stability property

Families of Schmidt-number witnesses for high dimensional quantum states

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Communications in Theoretical Physics 2024年第8期76卷 44-51页

作者： xian shi College of Information Science and Technology Beijing University of Chemical TechnologyBeijing 100029China

Higher dimensional entangled states demonstrate significant advantages in quantum information processing tasks. The Schmidt number is a quantity of the entanglement dimension of a bipartite state. Here we build families of k-positive maps from the symmetric information complete positive operator-valued measurements and mutually unbiased bases, and we also present the Schmidt number witnesses, correspondingly. At last, based on the witnesses obtained from mutually unbiased bases, we show the distance between a bipartite state and the set of states with a Schmidt number less than k.

关键词： Schmidt number entanglement witness mutually unbiased bases

Design and high-power testing of offline conditioning cavity for CiADS RFQ high-power coupler

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Nuclear Science and Techniques 2024年第9期35卷 18-27页

作者： Ruo-Xu Wang Yuan He Long-bo shi Chen-Xing Li Zong-Heng Xue Tian-Cai Jiang xian-bo Xu Lie-Peng Sun Zhou-Li Zhang Institute of Modern Physics Chinese Academy of SciencesLanzhou 730000China Lanzhou University Lanzhou 730000China

To validate the design rationality of the power coupler for the RFQ cavity and minimize cavity contamination,we designed a low-loss offline conditioning cavity and conducted high-power *** offline cavity features two coupling ports and two tuners,operating at a frequency of 162.5 MHz with a tuning range of 3.2 *** the installation angle of the coupling ring and the insertion depth of the tuner helps minimize cavity *** performed electromagnetic structural and multiphysics simulations,revealing a minimal theoretical power loss of 4.3%.However,when the cavity frequency varied by110 kHz,theoretical power losses increased to10%,necessitating constant tuner adjustments during *** simulations indicated that increased cavity temperature did not affect frequency *** completion of the offline high-power conditioning platform,we measured the transmission performance,revealing a power loss of 6.3%,exceeding the theoretical *** utilized efficient automatic range scanning and standing wave resonant *** fully condition the power coupler,a 15°phase difference between two standing wave points in the condition-ing system was ***,the maximum continuous wave power surpassed 20 kW,exceeding the expected target.

关键词： RFQ cavity Power coupler Offline conditioning Resonant cavity

Combustion mechanism of benzene in iron ore sintering process:experimental and simulation

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Journal of Iron and Steel Research International 2024年第1期31卷 195-203页

作者： Zhi-gang Que Jin-ming shi xian-bin Ai Institute of Energy Research Jiangxi Academy of ScienceNanchang330096JiangxiChina Jiangxi Carbon Neutralization Research Center Nanchang330096JiangxiChina

Benzene is a typical component of volatile organic compounds(VOCs)in the iron ore sintering flue *** combustion behavior of benzene directly affects the emission of VOCs in iron ore sintering *** effects of temperature,benzene,and oxygen concentrations on the conversion ratio of benzene were investigated by experiments and numerical *** experiments were carried out in a tube reactor at temperatures of 773-1098 K,benzene concentrations of 0.01-0.03 vol.%,and oxygen concentrations of 10-21 vol.%.The numerical simulation was performed with the plug flow model in the CHEMKIN program based on a kinetic model that consists of 132 chemical species and 772 elementary step-like *** experimental results reveal that increasing the temperature and benzene concentration could signifi-cantly promote benzene *** is attributed to the increase in the reaction rates of all steps in the pathway for forming CO_(2)and H_(2)*** addition,due to the large equivalent ratio of oxygen to benzene,the conversion ratio of benzene remained constant at different oxygen *** simulation results were in good agreement with the experimental results and indicated that six elementary reactions dominated the formations of CO_(2)and H_(2)*** oxidations of C_(6)H_(5)O,CO,and C_(5)H_(4)O intermediates to CO_(2)were the limiting steps in the reaction pathways.

关键词： Benzene Volatile organic compound Iron ore sinter Combustion Simulation Temperature Oxygen