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International Journal of Minerals,Metallurgy and Materials 2025年第1期32卷 80-91页

作者： Junjie shi Changle Hou Jingjing Dong Dong Chen Jianzhong Li Key Laboratory for Ecological Metallurgy of Multimetallic Mineral(Ministry of Education) Northeastern UniversityShenyang 110819China School of Metallurgy Northeastern UniversityShenyang 110819China

With the continuous increase in the disposal volume of spent lithium-ion batteries(LIBs),properly recycling spent LIBs has become essential for the advancement of the circular *** study presents a systematic analysis of the chlorination roasting kinetics and proposes a new two-step chlorination roasting process that integrates thermodynamics for the recycling of LIB cathode *** activation energy for the chloride reaction was 88.41 kJ/mol according to thermogravimetric analysis–derivative thermogravimetry data obtained by using model-free,model-fitting,and Z(α)function(αis conversion rate).Results indicated that the reaction was dominated by the first-order(f1)model when the conversion rate was less than or equal to 0.5 and shifted to the second-order(f2)model when the conversion rate exceeded *** conditions were determined by thoroughly investigating the effects of roasting temperature,roasting time,and the mass ratio of NH_(4)Cl to LiCoO_(2).Under the optimal conditions,namely 400℃,20 min,and NH_(4)Cl/LiCoO_(2)mass ratio of 3:1,the leaching efficiency of Li and Co reached 99.43% and 99.05%,*** of the roasted products revealed that valuable metals in LiCoO_(2)transformed into CoCl_(2) and ***,the reaction mechanism was elucidated,providing insights for the establishment of a novel low-temperature chlorination roasting technology based on a crystal structure *** technology can guide the development of LIB recycling processes with low energy consumption,low secondary pollution,high recovery efficiency,and high added value.

关键词： spent lithium-ion battery thermodynamics chlorination roasting kinetics circular economy

Mechanism of wavy vortex and sign laws in flow past a bluff body:vortex-induced vortex

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Acta Mechanica Sinica 2019年第1期35卷 1-14,I0001页

作者： L.M.Lin S.Y.shi x.f.Zhong Y.x.Wu Key Laboratory for Mechanics in fluid Solid Coupling Systems Institute of MechanicsChinese Academy of SciencesBeijing 100190China School of Engineering Sciences University of Chinese Academy of SciencesBeijing 100049China

As reported in a previous work by Lin et al.(Acta Meeh Sin, 2018. https://***/10.1007/s 10409-018-0758-z), an interesting phenomenon was discovered based on the analysis of wavy vortex and vorticity distribution in the shear layers and near wake of a peak-perforated conic shroud, and two sign laws were summarized. In the present paper, the theory of a vortex-induced vortex is introduced to explore mechanisms in a wavy vortex and applicable sign laws for uniform and incompressible flow past a fixed bluff body. Based on the analysis of the nearest-wall How, two vortex-induced models for streamwise and vertical vortex pairs, respectively, are proposed under two boundary cases, denoting the induced vorticity introduced or distributed on and near the walls. As a result, the first sign law, for only streamwise and vertical components of vorticity, and the second sign law, for three components of vorticity, are obtained under their own particular conditions. The first sign law reveals the intrinsic physical relationship between streamwise and vertical vorticities, independent of the distribution of spanwise vortices in the whole flow field. It is also confirmed that the spanwise vortices, as well as the shear layers and wake width, distributed wavily across the span, are attributed to the introduced streamwise or vertical vortices. The two sign laws for vorticity are independent of the disturbed spanwise wavelength and the Reynolds number. Through the analysis of flow past the conic shroud, the two sign laws are successfully used to summarize typical spacial distributions of vorticity in three flow regions: on and near the front cylinder surfaces, the separated shear layers and the near wake.

关键词： Wavy vortex Sign law Vortex-induced vortex Wake Bluff body

A pathway to improve low-cycle fatigue life of face-centered cubic metals via grain boundary engineering

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Journal of Materials Science & Technology 2022年第18期113卷 82-89页

作者： x.J.Guan Z.P.Jia S.M.Liang f.shi x.W.Li Department of Materials Physics and Chemistry School of Materials Science and EngineeringNortheastern UniversityShenyang 110819China State Key Laboratory of Rolling and Automation Northeastern UniversityShenyang 110819China Key Laboratory for Anisotropy and Texture of Materials Ministry of EducationNortheastern UniversityShenyang 110819China

To probe a pathway to improve the low-cycle fatigue life of face-centered cubic(fCC)metals via grain boundary engineering(GBE),the tension-tension fatigue tests were carried out on the non-GBE and GBE Cu-16 at.%Al alloys at relatively high stress *** results indicate that the cyclic strain localiza-tion and cracking at grain boundaries(GBs)can be effectively suppressed,especially at increased stress amplitude,by an appropriate GBE treatment that can result in a higher resistance to GB cracking and a greater capability of compatible ***,the sensitivity of fatigue life to stress amplitude can be weakened by GBE,and the low-cycle fatigue life of Cu-16 at.%Al alloys is thus distinctly improved.

关键词： Cu-Al alloy Grain boundary engineering fatigue life Crack nucleation Stress amplitude

Changes in fine root biomass of Picea abies forests:predicting the potential impacts of climate change

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Journal of Plant Ecology 2018年第4期11卷 595-603页

作者： Z.Y.Yuan x.R.shi f.Jiao f.P.Han State Key Laboratory of Soil Erosion and Dryland farming on the Loess Plateau Institute of Soil and Water ConservationNorthwest A&F UniversityYanglingShaanxi 712100China Institute of Soil and Water Conservation Chinese Academy of Science and Ministry of Water ResourceYanglingShaanxi 712100China

Aims the impact of global warming on belowground processes,espe-cially on fine root production,is poorly understood in comparison with its aboveground *** Here,we compiled 227 measurements to assess the influence of temperature and precipitation on fine root biomass of Norway spruce(Picea abies[L.]Karst)forest ecosystems in the Eurasia boreal *** findings We found that fine root biomass decreased significantly with *** was a biomass increase of 0.63 Mg ha−1 and 0.32 Mg ha−1 for fine rootsf mean annual *** was an increase of 0.5 and 0.1 Mg ha−1 per 100 mm year−1 precipitation for the two size classes of fine *** the adaption of root production can match the pace of global warming and water is not a limiting factor for plant growth,fine root biomass would be expected to increase by 40-140%in response to the predicted increase in tem-perature(3-10°C)over the next *** analyses highlighted the strongly positive influences of temperature and precipitation on belowground function,suggesting that predicted future climate change could substantially enhance belowground biomass in the boreal region where the greatest warming is *** potential increase of belowground biomass,coupled with aboveground biomass,may provide a better understanding of climate-ecosystem feedbacks.

关键词： boreal forest carbon climate change fine roots latitudinal gradient mean annual temperature and precipitation Norway spruce Picea abies production and biomass

Toward developing Ti alloys with high fatigue crack growth resistance by additive manufacturing

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Journal of Materials Science & Technology 2023年第1期132卷 166-178页

作者： f.Wang L.M.Lei x.fu L.shi x.M.Luo Z.M.Song G.P.Zhang Shenyang National Laboratory for Materials Science Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China School of Materials Science and Engineering University of Science and Technology of ChinaShenyang 110016China AECC Commercial Aircraft Engine Co. Ltd.Shanghai 201306China

fatigue crack growth behaviors were investigated by three-point bending tests for TA19 alloy fabricated by laser metal deposition and four kinds of heat-treated *** crack growth resistance of the TA19 samples in the near-threshold regime and Paris regime was evaluated through the experimental characterization and theoretical analysis of the interaction between fatigue crack andα/βphase inter-face,columnar prior-βgrain boundary and colony *** results show that in the near-threshold regime,the fatigue crack propagation threshold and resistance increase with the increase of widths of lamellarαp phases and colonies,and the decrease of the number ofαlaths with an angle(ϕ)relative to the applied stress direction ranging from 75°to 90°.In the Paris regime,the fatigue cracking path can be deflected at colony boundaries or columnar prior-βgrain *** larger the deflection angle,the more tortuous the cracking path and the lower the fatigue crack growth *** angle(γ)of the columnar prior-βgrain growth direction relative to the build direction affects not onlyϕof differentαvariants,but also the fatigue cracking path deflection angle(θij)at columnar prior-βgrain *** optimal combination ofγ=0°-15°-0°-15°for several adjacent columnar prior-βgrains is derived from the theoretical analysis,and that can effectively avoidϕbeing in the range from 75°to 90°and makeθij as large as *** findings provide a guide for the selection of scanning strategies and process parameters to additively manufacture Ti alloys with high fatigue damage tolerance.

关键词： Ti alloy fatigue crack growth Additive manufacturing Phase interface Grain boundary

Improving Intergranular Stress Corrosion Cracking Resistance in a fe–18Cr–17Mn–2Mo–0.85N Austenitic Stainless Steel Through Grain Boundary Character Distribution Optimization

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Acta Metallurgica Sinica(English Letters) 2022年第11期35卷 1849-1861页

作者： f.shi L.Yan J.Hu L.f.Wang T.Z.Li W.Li x.J.Guan C.M.Liu x.W.Li Department of Materials Physics and Chemistry School of Materials Science and EngineeringNortheastern UniversityShenyang 110819China State Key Laboratory of Rolling and Automation Northeastern UniversityShenyang 110819China Key Laboratory for Anisotropy and Texture of Materials(Ministry of Education) Northeastern UniversityShenyang 110819China

The grain boundary character distribution(GBCD) optimization and its effect on the intergranular stress corrosion cracking(IGSCC) resistance in a cold-rolled and subsequently annealed fe-18 Cr-17 Mn-2 Mo-0.85 N high-nitrogen nickel-free austenitic stainless steel were systematically *** results show that stacking faults and planar slip bands appearing at the right amount of deformation(lower than 10%) are beneficial cold-rolled microstructures to the GBCD *** proportion of special boundaries gradually increases in the subsequent stages of recrystallization and grain growth,accompanying with the growth of twin-related domain in the experimental *** this way,the fraction of low ∑ coincidence site lattice(CSL) boundaries can reach as high as 82.85% for the specimen cold-rolled by 5% and then annealed at 1423 K for 72 *** GBCD optimization,low ∑ CSL boundaries and the special triple junctions(J2,J3) of high proportion can greatly hinder the nitride precipitation along grain boundaries and enhance the capability for intergranular crack arrest,thus improving the IGSCC resistance of the experimental steel.

关键词： High-nitrogen austenitic stainless steel Grain boundary character distribution Coincidence site lattice(CSL)grain boundary Electron backscatter diff raction(EBSD) Intergranular stress corrosion cracking

STUDY ON Ni_(25)Ti_(50)Cu_(25) SHAPE MEMORY PARTICLE/Al MATRIx COMPOSITE

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Acta Metallurgica Sinica(English Letters) 1996年第6期9卷 589-594页

作者： L.S.Cui M.Qi P.shi f.x.Chen D.Z.Yang Department of Materials Engineering Dalian University of TechnologyDalian 116024China

Ni_(25)Ti_(50)Cu_(25) shape memory particle/Al matrix composite was prepared by hot pressing and further *** Ni_(25)Ti_(50)Cu_(25) particles embeded in Al matrix still keep B19 and B19 structure,and have a good thermal-elastic martensitic transition with 6K thermal hysteresis,the phase transition temperatures remaining constant during cycling. The scratching force of Ni_(25)Ti_(50)Cu_(25) particle is two times that of Al matrix,When the scratching force is larger than 4.2N, the Ni_(25)Ti_(50)Cu_(25) particle is separated from Al matrix.

关键词： Ni_(25)Ti_(50)Cu_(25) shape memory particle Al matrix composite thermal-elastic martensitic transformation.

Joint Distribution of Wave Periods and Rate of Change of Wave Surface Elevation

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China Ocean Engineering 1999年第2期14卷 225-229页

作者： shi, HD Sun, f Ocean Univ Qingdao Dept Civil Engn Qingdao 266003 Peoples R China

The rate of change of wave surface elevation is of much importance in ocean engineering, especially for the determination of the limitation of wave breaking. This paper gives a kind of joint distribution of wave periods and the rate of change of wave surface elevation by means of calculation of the two-order to four-order moment of the frequency spectrum based on the linear wave theory. for the first time, the distribution density function of wave periods determined by peaks is provided, and the conclusion is drawn that the rate of change of wave surface elevation obeys the Rayleigh distribution.

关键词： rate of change wave surface elevation joint distribution wave period

STUDY ON DYNAMIC J-INTEGRAL Of MECHANICAL HETEROGENEOUS WELDED JOINT

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Acta Metallurgica Sinica(English Letters) 2004年第6期17卷 934-939页

作者： f.Q.Tian D.Y.He x.Y.Li Y.W.shi D.Zhang InstituteofCompositeMaterials ShanghaiJiaotongUniversityShanghai200030China SchoolofMaterialsScienceandEngineering BeijingPolytechnicUniversityBeijing100022China

Welded joint is a mechanical heterogeneous body, and mechanical heterogeneity has great effect on dynamic fracture behaviour of welded joints. In the present investigation, dynamic response curve and dynamic J-integral of practical undermatched welded joint and whole base and whole weld three-point-bend (TPB) models containing longitudinal crack are com- puted. Dynamic J-integral is evaluated using virtual crack extension (VCE) method and the computation is performed using MARC finite element code. Because of the effect of inertia, dynamic load response curve of computed model waves periodically. Dynamic J-integral evaluated by VCE method is path independent. The effect of inertia has little influence on dynamic J-integral curve. The value of dynamic J-integral of undermatched welded joint is lower than that of whole base metal and higher than that of whole weld metal. The results establish the foundation of safety evaluation for dynamic loaded welded structures.

关键词： virtual crack extension welded joint dynamic response curve dynamic J-integral