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Improvement of elevated-temperature strength and recrystallization resistance via Mn-containing dispersoid strengthening in Al-Mg-Si 6082 alloys

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Journal of Materials Science & Technology 2020年第4期39卷 135-143页

作者： chen Li Kun Liu x.-grant chen Department of Applied Science University of Québec at ChicoutimiChicoutimiQC G7H 2B1Canada

The precipitation behavior of Mn-containing dispersoids in Al-Mg-Si 6082 alloys with different Mn contents(0,0.5 and 1.0 wt%)during various heat treatments(300–500℃)was *** effects of dispersoids on elevated-temperature strength and recrystallization resistance during hot-rolling and post-rolling annealing were *** results showed that the dispersoids in the Mn-containing alloys(0.5 and 1.0%)began to precipitate at 350℃and reached the optimum conditions after 2–4 h at 400℃.However,the dispersoids coarsened with increasing holding time at temperatures above450℃.After the peak precipitation treatment at 400℃for 2 h,the yield strength at 300℃increased from 28 MPa(base alloy free of Mn)to 55 MPa(alloy with 0.5%Mn)and 70 MPa(alloy with 1%Mn),respectively,demonstrating a significant dispersoid strengthening effect at elevated *** addition,the dispersoids were thermally stable at 300℃for up to 1000 h holding owing to its relative high precipitation temperature(350–400℃),leading to the superior constant mechanical performance at elevated temperature during the long service *** hot rolling and post-rolling annealing,the presence of a large amount of dispersoids results in the higher Zener drag PZcompared with base alloy and then significantly improved the recrystallization *** alloy containing 0.5%Mn exhibited the highest recrystallization resistance among three experimental alloys studied during the post-rolling process,likely resulted from the lower coarsening rate of dispersoids and the lower dispersoids free zone.

关键词： Al-Mg-Si 6082 alloy Mn addition Dispersoid precipitation Elevated-temperature strength Recrystallization resistance

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Effects of Mn content on recrystallization resistance of AA6082 aluminum alloys during post-deformation annealing

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Journal of Materials Science & Technology 2020年第17期52卷 189-197页

作者： xiaoming Qian Nick Parson x.-grant chen Department of Applied Science University of Quebec at ChicoutimiSaguenay G7H 2B1Canada Arvida Research and Development Centre Rio Tinto AluminumSaguenay G7S 4K8Canada

The microstructural evolutions under as-homogenized and as-deformed conditions and after the postdeformation annealing of AA6082 aluminum alloys with different Mn content(0.05 wt.%-1 wt.%)were studied by optical,scanning electron,and transmission electron *** results showed that the presence of a large amount ofα-Al(Mn,Fe)Si dispersoids induced by Mn addition significantly improved the recrystallization *** the base alloy free of Mn,static recrystallization occurred after 2 h of annealing,and grain growth commenced after 4 h of annealing,whereas in Mn-containing alloys,the recovered grain structure was well-retained after even 8 h of *** alloy with 0.5%Mn exhibited the best recrystallization resistance,and a further increase of the Mn levels to 1%resulted in a gradual reduction of the recrystallization resistance,the reason for which was that recrystallization occurred only in the dispersoid-free zones(DFZs)and the increased DFZ fraction with Mn content led to an increase in the recrystallization *** variation in the dispersoid number density and a coarsening of dispersoids during annealing have a limited influence on the static recrystallization in Mn-containing alloys.

关键词： AA6082 alloys Mn effects Recrystallization resistance Dispersoid precipitation Post-deformation annealing

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Fabrication of Superhydrophobic Surfaces on Aluminum Alloy Via Electrodeposition of Copper Followed by Electrochemical Modification

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Nano-Micro Letters 2011年第3期3卷 160-165页

作者： Ying Huang D.K.Sarkar x-grant chen University Research Center on Aluminum (CURAL) University of Qubec at Chicoutimi

Superhydrophobic aluminum surfaces have been prepared by means of electrodeposition of copper on aluminum surfaces, followed by electrochemical modification using stearic acid organic molecules. Scanning electron microscopy(SEM) images show that the electrodeposited copper films follow "island growth mode" in the form of microdots and their number densities increase with the rise of the negative deposition potentials. At an electrodeposition potential of-0.2 V the number density of the copper microdots are found to be 4.5×104cm^(-2)that are increased to 2.9×105cm^(-2)at a potential of-0.8 V. Systematically, the distances between the microdots are found to be reduced from 26.6 μm to 11.03 μm with the increase of negative electrochemical potential from-0.2 V to-0.8 V. x-ray diffraction(xRD) analyses have confirmed the formation of copper stearate on the stearic acid modified copper films. The roughness of the stearic acid modified electrodeposited copper films is found to increase with the increase in the density of the copper microdots. A critical copper deposition potential of-0.6 V in conjunction with the stearic acid modification provides a surface roughness of 6.2 μm with a water contact angle of 157?, resulting in superhydrophobic properties on the aluminum substrates.

关键词： Superhydrophobic aluminum surface Water contact angle Copper microdots Surface roughness Electrochemical modification

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Effect of Si,Cu and Fe on mechanical properties of cast semi-solid 206 alloys

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Transactions of Nonferrous Metals Society of China 2010年第9期20卷 1555-1560页

作者： A.LEMIEUx J.LANGLAIS D.BOUCHARD x.grant chen Rio Tinto Alcan Arvida Research and Development Centre Rio Tinto Alcan Laterrière Works NRC-Aluminium Technology Centre Université du Québec à Chicoutimi

The development of a modified 206 alloy whose composition was optimized to minimize hot tearing during semi-solid forming was reported. The effect of varying silicon, copper and iron contents was investigated using a design of experiment (DOE) approach. Semi-solid slurries were prepared using the SEED process and injected into a high pressure die casting press. The hot tearing sensitivity results were reported for different alloy variants. The microstructure evolution during the semi-solid preparation was presented along with actual die cast components. The effects of silicon, copper and iron on mechanical properties in the T7 condition were also analyzed. Beyond the benefit of reducing hot tearing, it is shown that the tensile and fatigue properties remain compatible with the automotive industry requirements.

关键词： semi-solid forming 206 aluminum alloy SEED process hot tearing mechanical properties

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Semi-solid processing of hypereutectic A390 alloys using novel rheoforming process

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Transactions of Nonferrous Metals Society of China 2010年第9期20卷 1743-1748页

作者： M.TEBIB J.B.MORIN F.A JERSCH x.grant chen Université du Québec à Chicoutimi cole polytechnique de Montréal

The feasibility of semi solid processing of hypereutectic A390 alloys using a novel rheoforming process was investigated. A combination of the swirl enthalpy equilibration device （SEED） process, isothermal holding using insulation and addition of solid alloy during swirling was introduced as a novel method to improve the processability of semi solid slurry. The effects of isothermal holding and the addition of solid alloy on the temperature gradient between the centre and the wall and on the formation of a（Al） particles were examined. In additional tests, phosphorus and strontium were added to the molten metal to refine the primary and eutectic silicon structure to facilitate semi solid processing. The results show that the combination of the SEED process with two additional processing steps can produce semi-solid A390 alloys that can be rheoprocessed. The microstructure reveals an adequate amount of non-dendritic a（Al） globules surrounded by liquid, which greatly improves the processability of semi-solid slurry.

关键词： semi-solid forming rheoforming process hypereutectic A390 alloys microstructure

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Effect of magnesium on dispersoid strengthening of Al-Mn-Mg-Si(3xxx) alloys

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Transactions of Nonferrous Metals Society of China 2016年第11期26卷 2793-2799页

作者：李震张展 x-grant GHEN Department of Applied Sciences University of Québec at Chicoutimi 555 boul. de l’Université

The effects of magnesium addition on the dispersoid precipitation as well as mechanical properties of 3xxx alloys wereinvestigated. The microstructures in as-cast and heat-treated conditions were evaluated by optical microscopy and transmissionelectron microscopy. The results reveal that Mg has a strong influence on the distribution and volume fraction of dispersoids duringprecipitation heat treatment. The microhardness and yield strength at ambient temperature increase with increasing Mg content. Thesolid solution and dispersoid strengthening mechanisms of materials after heat treatment are quantitatively analyzed. Dispersoidstrengthening for the alloys is the predominant strengthening mechanism after precipitation heat treatment. An analytical model isintroduced to predict the evolution of ambient-temperature yield strength.

关键词： aluminum alloy Mg dispersoid strengthening solid solution strengthening microstructure characterization mechanicalproperties

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均匀化前预处理对Al-Zn-Mg-Cu合金中含V相析出及再结晶的影响

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轻合金加工技术 2016年第3期44卷 24-30,42页

作者：郭占英丛福官赵刚 x.-grant chen 田妮东北大学材料各向异性与织构教育部重点实验室辽宁沈阳110819 魁北克大学希库蒂米分校应用科学学院东北轻合金有限责任公司黑龙江哈尔滨150060

用透射电子显微镜（TEM）及扫描电镜电子背散射（EBSD）技术,研究了均匀化前250℃~400℃的预处理对w（V）=0.11%的超高强Al-Zn-Mg-Cu合金中Al21V2弥散相析出行为及变形后再结晶抗力的影响,并计算了V在铝基体中的扩散常数和扩散距离。结... 详细信息

用透射电子显微镜（TEM）及扫描电镜电子背散射（EBSD）技术,研究了均匀化前250℃~400℃的预处理对w（V）=0.11%的超高强Al-Zn-Mg-Cu合金中Al21V2弥散相析出行为及变形后再结晶抗力的影响,并计算了V在铝基体中的扩散常数和扩散距离。结果表明,铸锭均匀化处理过程形成Al21V2弥散相,并在晶界附近形成明显的无析出区,其宽度基本不受均匀化处理前预处理的影响;在普通均匀化处理前预处理能明显提高Al21V2弥散相的密度、减小其尺寸;在铝基体中,V在300℃及400℃的扩散常数分别为9.81×10-31m2/s、5.32×10-24m2/s。在300℃预处理合金能获得尺寸最小、密度最高的Al21V2弥散相,而且其热变形后再结晶抗力最大。

关键词：超高强Al-Zn-Mg-Cu合金均匀化 Al21V2相弥散相再结晶

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均匀化前预处理对7150铝合金中Al_3Zr相析出及再结晶的影响

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轻合金加工技术 2016年第2期44卷 21-27页

用透射电子显微镜（TEM）及电子背散射（EBSD）技术,研究了均匀化前进行250℃~400℃预处理对7150铝合金中Al3Zr相析出行为及变形后固溶处理过程再结晶抗力的影响。结果表明,7150铝合金是否进行均匀化前预处理,其经470℃24 h的均匀化后... 详细信息

用透射电子显微镜（TEM）及电子背散射（EBSD）技术,研究了均匀化前进行250℃~400℃预处理对7150铝合金中Al3Zr相析出行为及变形后固溶处理过程再结晶抗力的影响。结果表明,7150铝合金是否进行均匀化前预处理,其经470℃24 h的均匀化后其合金中Al3Zr析出相与Al基体均为共格关系。随均匀化前预处理温度降低,Al3Zr析出相的尺寸变小、密度提高;在250℃预处理,随预处理时间延长,最终Al3Zr析出相的尺寸变小、密度提高;当预处理温度超过300℃时,随预处理时间延长,Al3Zr析出相的尺寸变大、密度降低,但预处理时间超过24 h后其影响不明显。7150铝合金铸锭经470℃均匀化前预处理能显著提高其变形后再结晶抗力,经470℃2h固溶处理后,其组织为未再结晶的回复组织;而直接经470℃均匀化处理后的变形样品经470℃2h固溶处理后,其组织为部分再结晶组织。

关键词： 7150铝合金均匀化 Al3Zr弥散相高分辨TEM 再结晶

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轻质铝基熵合金:概述与未来趋势

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Science China Materials 2024年第1期67卷 31-46页

作者：崔立莹张展陈晓光 Department of Applied Science University of Quebec at Chicoutimi555boulevard de l’UniversiteSaguenay G7H 2B1QCCanada

新一代合金——高熵合金的出现,揭示了熵效应在合金设计中的重要意义.受这一概念的启发,轻质铝基熵合金这一概念被提出.随着对低密度结构材料的需求不断增加,这些新型合金在各种应用中具有巨大的潜力.本文综述了轻质铝基熵合金的发展背... 详细信息

新一代合金——高熵合金的出现,揭示了熵效应在合金设计中的重要意义.受这一概念的启发,轻质铝基熵合金这一概念被提出.随着对低密度结构材料的需求不断增加,这些新型合金在各种应用中具有巨大的潜力.本文综述了轻质铝基熵合金的发展背景、设计原理、制造方法、微观结构和力学性能、高温应用,及其发展前景.通过对当前研究的全面调查,本文重点研究分析了122种密度低于4.0 g cm-3的铝基熵合金.轻质铝基熵合金可以弥补传统铝和钛合金在机械性能和密度方面的差距.轻质铝基熵合金优异的热稳定性使其有望成为在高温下使用的结构材料.此外,本文还讨论了轻质铝基熵合金领域的未来发展趋势.机器学习作为有效计算工具,可以极大地提高合金的开发效率.

关键词：高温应用合金设计新型合金机器学习铝基计算工具高熵合金微观结构

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Targeting cholesterol trafficking to mitigate axonal degeneration in hereditary spastic paraplegia

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Neural Regeneration Research 2025年第5期20卷 1397-1398页

作者： Zhenyu chen xue-Jun Li Department of Biomedical Sciences University of Illinois College of Medicine RockfordRockfordILUSA Department of Bioengineering University of Illinois at ChicagoChicagoILUSA

Axonal degeneration underlies many debilitating diseases including hereditary spastic paraplegia(HSP),a genetically and clinically diverse group of disorders characterized by spasticity and weakness of the lower *** is one significant cause of chronic neurodisability due to the lack of effective treatments and a wide range of onset ages from early childhood to 70 years.

关键词： degeneration diseases hereditary

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