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An effective strategy to inhibit grain coarsening:Construction of multi-element co-segregated grain boundary complexion

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Journal of Advanced Ceramics 2024年第7期13卷 1060-1071页

作者： Le Fu Gabriel Arcuri wenjun Yu Bohan Wang Zihua Lei Ying Deng Kathryn Grandfield School of Material Science and Engineering Central South UniversityChangsha 410083China Canadian Centre for Electron Microscopy McMaster UniversityHamilton L8S 4L8Canada State Key Laboratory of New Ceramics and Fine Processing School of Materials Science and EngineeringTsinghua UniversityBeijing 100084China Department of Materials Science and Engineering McMaster UniversityHamilton L8S 4L8Canada

When exposed to moderate to high temperatures,nanomaterials typically suffer from severe grain coarsening,which has long been a major concern that prevents their wider ***,we proposed an effective strategy to inhibit grain coarsening by constructing grain boundary(GB)complexions with multiple codoped dopants,which hindered coarsening from both energetic and kinetic *** demonstrate the feasibility of this strategy,multiple selected dopants were doped into a ZrO_(2)-SiO_(2)nanocrystalline glass ceramic(NCGC)to form GB *** results showed that NCGC was predominantly composed of ZrO_(2)nanocrystallites(NCs)distributed in an amorphous SiO_(2)*** layers of GB complexions(~2.5 nm)were formed between adjacent ZrO_(2)NCs,and they were crystalline superstructures with co-segregated *** addition,a small amount of quartz solid solution was formed,and it adhered to the periphery of ZrO_(2)NCs and bridged the adjacent NCs,acting as a“bridging phase”.The GB complexions and the“bridging phase”synergistically enhanced the coarsening resistance of ZrO_(2)NCs up to 1000°*** findings are important for understanding GB complexions and are expected to provide new insights into the design of nanomaterials with excellent thermodynamic stability.

关键词： Zr_(2)-Si_(2) multi-element co-segregation grain boundary(GB)complexion grain coarsening atom probe tomography(APT)

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High-sensitivity intelligent packaging films harnessing rose anthocyanins and hydrophilic silica aerogel for visual food freshness monitoring

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Food Quality and Safety 2024年第1期8卷 179-189页

作者： wenjun Wu Luman Zheng Jiahao Yu Liming Liu Gulden Goksen Ping Shao Department of Food Science and Technology Zhejiang University of TechnologyZhejiangHangzhouChina Department of Food Technology Vocational School of Technical Sciences at Mersin Tarsus Organized Industrial ZoneTarsus UniversityMersinTurkey Eco-Industrial Innovation Institute ZJUT Zhejiang University of TechnologyZhejiangQuzhouChina

The enhancement of the sensitivity for anthocyanin-based indicator films in food freshness monitoring in real time is important for *** this study,hydrophilic silica aerogel(SiO2 NA)was incorporated into corn starch(CS)/chitosan(CH)/rose anthocyanins(RACNs)-encapsulated potato amylopectin nanoparticles(APNPs)composite film to increase the sensitivity for shrimp freshness *** microstructure of films revealed that the gas absorption capacity was improved by amorphous SiO2 NA via hydrogen *** pore size(1.74–5.60 times),pore volume(3.92–5.60 times),and specific surface area(2.21–2.34 times)of films increased with the addition of SiO2 *** sensing of NH3 and pH and the reversibility of films were also ***,the pH-responsive films containing SiO2 NA changed visibly in color from purple–red to orange–gray and finally to gray,enabling effective monitoring of shrimp freshness during storage at 4°***,anthocyanin-based indicator films with improved sensitivity by adding SiO2 NA were successfully designed for monitoring shrimp freshness.

关键词： Hydrophilic silica aerogel anthocyanins sensitivity pH-responsive shrimp freshness intelligent packaging

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Revealing the specific role of sulfide and nano-alumina in composite solid-state electrolytes for performance-reinforced ether-nitrile copolymers

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Journal of Energy Chemistry 2024年第4期91卷 628-636页

作者： Haoyang Yuan Changhao Tian Mengyuan Song wenjun Lin Tao Huang Aishui Yu Department of Chemistry Collaborative Innovation Center of Chemistry for Energy MaterialsShanghai Key Laboratory of Molecular Catalysis and Innovative MaterialsInstitute of New EnergyFudan UniversityShanghai 200438China Laboratory of Advanced Materials Fudan UniversityShanghai 200438China

Composite solid-state electrolytes represent a critical pathway that balances the interface compatibility and lithium-ion conductivity in all-solid-state *** quest for stable and highly ion-conductive combinations between polymers and fillers is vital,but blind attempts are often made due to a lack of understanding of the mechanisms involved in the interaction between polymers and ***,we employ in-situ polymerization to prepare a polymer based on an ether-nitrile copolymer with high cathode stability as the foundation and discuss the performance enhancement mechanisms of argyrodite and *** 1%content of sulfide interacting with the polymer at the two-phase interface,the local enhancement of lithium-ion migration capability can be achieved,avoiding the reduction in capacity due to the low ion conductivity of the passivation layer during *** capacity retention after 50cycles at 0.5 C increases from 83.5%to 94.4%.Nano-alumina,through anchoring the anions and interface inhibition functions,eventually poses an initial discharge capacity of 136.8 m A h g^(-1)at 0.5 C and extends the cycling time to 1000 h without short-circuiting in lithium metal *** the combined action of dual fillers on the composite solid-state electrolyte,promising insights are provided for future material design.

关键词： Composite solid-state electrolytes Lithium metal anode Dual fillers Interfacial ionic conduction Inert nano-alumina

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Prediction of the thermal conductivity of Mg–Al–La alloys by CALPHAD method

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International Journal of Minerals,Metallurgy and Materials 2024年第1期31卷 129-137页

作者： Hongxia Li wenjun Xu Yufei Zhang Shenglan Yang Lijun Zhang Bin Liu Qun Luo Qian Li State Key Laboratory of Advanced Special Steels&Shanghai Key Laboratory of Advanced Ferrometallurgy&School of Materials Science and Engineering Shanghai UniversityShanghai 200444China National Engineering Research Center for Magnesium Alloys Chongqing UniversityChongqing 400044China State Key Laboratory of Powder Metallurgy Central South UniversityChangsha 410083China College of Materials Science and Engineering Chongqing UniversityChongqing 400044China National Key Laboratory of Advanced Casting Technologies Chongqing UniversityChongqing 400044China

Mg-Al alloys have excellent strength and ductility but relatively low thermal conductivity due to Al *** accurate prediction of thermal conductivity is a prerequisite for designing Mg-Al alloys with high thermal ***,databases for predicting temperature-and composition-dependent thermal conductivities must be *** this study,Mg-Al-La alloys with different contents of Al2La,Al3La,and Al11La3phases and solid solubility of Al in the α-Mg phase were *** influence of the second phase(s) and Al solid solubility on thermal conductivity was *** results revealed a second phase transformation from Al_(2)La to Al_(3)La and further to Al_(11)La_(3)with the increasing Al content at a constant La *** degree of the negative effect of the second phase(s) on thermal diffusivity followed the sequence of Al2La>Al3La>Al_(11)La_(3).Compared with the second phase,an increase in the solid solubility of Al in α-Mg remarkably reduced the thermal *** the basis of the experimental data,a database of the reciprocal thermal diffusivity of the Mg-Al-La system was established by calculation of the phase diagram (CALPHAD)*** a standard error of±1.2 W/(m·K),the predicted results were in good agreement with the experimental *** established database can be used to design Mg-Al alloys with high thermal conductivity and provide valuable guidance for expanding their application prospects.

关键词： magnesium alloy thermal conductivity thermodynamic calculations materials computation

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Lateral root elongation in maize is related to auxin synthesis and transportation mediated by N metabolism under a mixed NO_(3)^(–) and NH_(4)^(+) supply

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Journal of Integrative Agriculture 2024年第3期23卷 1048-1060页

作者： Peng Wang Lan Yang Xichao Sun wenjun Shi Rui Dong Yuanhua Wu Guohua Mi Key Laboratory of Tobacco Biology and Processing of Ministry of Agriculture and Rural Affairs Tobacco Research InstituteChineseAcademy of Agricultural SciencesQingdao 266101China Department of Plant Nutrition College of Resources and Environmental SciencesChina Agricultural UniversityBeijing 100193China College of Resources Hunan Agricultural UniversityChangsha 410128China Agro-Environmental Protection Institute Ministry of Agriculture and Rural AffairsTianjin 300191China

A mixed nitrate (NO_(3)^(–)) and ammonium (NH_(4)^(+)) supply can promote root growth in maize (Zea mays),however,the changes in root morphology and the related physiological mechanism under different N forms are still ***,maize seedlings were grown hydroponically with three N supplied in three different forms (NO_(3)^(–)only,75/25 NO_(3)^(–)/NH_(4)^(+)and NH_(4)^(+)only).Compared with sole NO_(3)^(–)or NH_(4)^(+),the mixed N supply increased the total root length of maize but did not affect the number of axial *** main reason was the increased total lateral root length,while the average lateral root (LR) length in each axle was only slightly *** addition,the average LR density of 2nd whorl crown root under mixed N was also *** with sole nitrate,mixed N could improve the N metabolism of roots (such as the N influx rate,nitrate reductase (NR) and glutamine synthase (GS)enzyme activities and total amino content of the roots).Experiments with exogenously added NR and GS inhibitors suggested that the increase in the average LR length under mixed N was related to the process of N assimilation,and whether the NR mediated NO synthesis participates in this process needs further ***,an investigation of the changes in root-shoot ratio and carbon (C) concentration showed that C transportation from shoots to roots may not be the key factor in mediating lateral root elongation,and the changes in the sugar concentration in roots further proved this ***,the synthesis and transportation of auxin in axial roots may play a key role in lateral root elongation,in which the expression of ZmPIN1B and ZmPIN9 may be involved in this *** study preliminarily clarified the changes in root morphology and explored the possible physiological mechanism under a mixed N supply in maize,which may provide some theoretical basis for the cultivation of crop varieties with high N efficiency.

关键词： maize NO_(3)^(–)/NH_(4)^(+)ratio lateral root elongation N assimilation indole-3-acetic acid

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A First-principles Study on the Adhesion Strength,Interfacial Stability,and Electronic Properties of Mg/Mg_(2)Y Interface

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Acta Metallurgica Sinica(English Letters) 2024年第3期37卷 537-550页

作者： Yunxuan Zhou wenjun Tian Quan Dong Hailian Wang Jun Tan Xianhua Chen Kaihong Zheng Fusheng Pan College of Materials Science and Engineering National Engineering Research Center for Magnesium AlloysChongqing UniversityChongqing 400044China State Key Laboratory of Mechanical Transmission Chongqing UniversityChongqing 400044China Institute of New Materials Guangdong Academy of SciencesGuangzhou 510650China

The interfacial microstructures and configurations directly affect the comprehensive properties of the composites,but their interfacial adhesion mechanism is complicated to expound by experimental *** this work,based on the stacking sequence of the Mg/Mg_(2)Y interface models,nine different Mg/Mg_(2)Y interface configurations with top site,bridge site,and hollow site(HCP)under Mg1,Mg_(2),and Y terminations were successfully constructed and systematically explored by first-principles *** results showed that the Mg_(2)Y(0001)surface with Y termination is the most stable when the yttrium chemical potential()is less than-1.09 eV;otherwise,Mg_(2)Y(0001)surface with Mg1 termination is the most *** seven-layer Mg(0001)and eleven-layer Mg_(2)Y(0001)slabs are employed to reflect the bulk-like interior ***,the Mg(0001)/Mg_(2)Y(0001)with the Y-HCP stacking has the largest interface thermodynamic stability with the value of 2.383 J/m^(2) in all interface configurations owing to its largest work of *** addition,the interfacial energy of Y-HCP stacking is significantly smaller than those of Mg1-HCP when is approximately less than-0.55 eV,showing that it is more *** thermodynamic stability of Mg/Mg_(2)Y with Y-HCP is due to Mg-Y chemical bonds formed between Mg and Y ***,the Mg/Mg_(2)Y interfaces are strong interfaces based on the Griffith fracture theory.

关键词： Mg/Mg_(2)Y interface Interface stability Work of adhesion Electronic structure First-principles calculations

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Transient synthesis of carbon-supported high-entropy alloy sulfide nanoparticles via flash Joule heating for efficient electrocatalytic hydrogen evolution

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Nano Research 2024年第4期17卷 3379-3389页

作者： Yuntian Liao Rongtao Zhu wenjun Zhang Haiyang Zhu Yang Sun Jiale Chen Zhenhua Dong Ronghuan Lv School of Chemical Engineering and Technology China University of Mining and TechnologyXuzhou 221116China

High entropy alloys(HEA)are frequently employed as catalysts in electrocatalytic hydrogen ***,the traditional high entropy alloy synthesis methods are time-consuming,energy-intensive,and environmentally polluting,which limits their application in the hydrogen evolution reaction(HER).This study leveraged the capabilities of flash Joule heating(FJH)to synthesize carbon-supported high-entropy alloy sulfide nanoparticles(CC-S-HEA)on carbon cloth(CC)with good self-standing properties within 300 *** carbon thermal shock generated by the Joule heating could pyrolyze the sulfur source into gas,resulting in numerous pore structures and defects on CC,forming an S-doped carbon substrate(CC-S).Then the S atoms were used to stably anchor the metal atoms on CC-S to form high-density uniformly dispersed HEA *** electrochemical test results demonstrated that CC-S-HEA prepared at 60 V flash voltage had HER performance comparable to Pt/*** density functional theory(DFT)calculation indicated that the S atoms on CC-S accelerated the electron transfer between the carbon substrate and HEA ***,the unique electronic structure of CC-S-HEA was beneficial to H*adsorption and promoted catalytic *** simplicity and versatility of FJH synthesis are of great significance for optimizing the synthesis of HEA and improving the quality of HEA products,which provides a broad application prospect for the synthesis of nanocatalysts with efficient HER performance.

关键词： high entropy alloy flash Joule heating carbon thermal shock hydrogen evolution reaction density functional theory

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Biochemistry and transcriptome analysis reveal condensed tannins alleviate liver injury induced by regulating cholesterol metabolism pathway

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Food Science and Human Wellness 2024年第2期13卷 909-919页

作者： Xiangxin Li Yijing Pu Bangdi Liu Xiaoming Fang wenjun Peng Weibo Jiang Wenli Tian Institute of Apicultural Research Chinese Academy of Agricultural SciencesBeijing 100093China College of Food Science and Nutritional Engineering China Agricultural UniversityBeijing 100083China Academy of Agricultural Planning and Engineering Ministry of Agriculture and Rural AffairsBeijing 100125China

Free cholesterol has been considered to be a critical risk factor of nonalcoholic fatty liver disease(NAFLD).It remains unknown whether dietary intake of condensed tannins(CTs)have distinguishable effects to alleviate liver damage caused by a high cholesterol *** C57BL/6 mice were fed a high cholesterol diet for 6 weeks,and given CTs treatment at a dosage of 200 mg/(kg·day)at the same *** results indicated that compared with mice fed a normal diet,a high cholesterol diet group resulted in significant weight loss,dysregulation of lipid metabolism in blood and liver,and oxidative stress in the liver,but CTs treatment dramatically reversed these negative *** and eosin(H&E)staining and frozen section observation manifested that CTs treatment could effectively reduce the deposition of liver cholesterol and tissue necrosis caused by high cholesterol *** alleviated liver injury mainly by regulating the expression of related genes in cholesterol metabolism pathway and AMPK *** results confirmed that CTs have remarkable cholesterol lowering and anti-liver injury effects in vivo.

关键词： Condensed tannins High cholesterol Liver injury Antioxidants Transcriptomic analysis

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Long Short-Term Memory Spiking Neural Networks for Classification of Snoring and Non-snoring Sound Events

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Chinese Journal of Electronics 2024年第3期33卷 793-802页

作者： Rulin ZHANG Ruixue LI Jiakai LIANG Keqiang YUE wenjun LI Yilin LI Electronics and Information College Hangzhou Dianzi University

Snoring is a widespread occurrence that impacts human sleep *** is also one of the earliest symptoms of many sleep *** is accurately detected,making further screening and diagnosis of sleep problems *** is frequently ignored because of its underrated and costly detection *** a result,this research offered an alternative method for snoring detection based on a long short-term memory based spiking neural network(LSTM-SNN) that is appropriate for large-scale home detection for *** designed acquisition equipment to collect the sleep recordings of 54 subjects and constructed the sleep sound database in the home *** Mel frequency cepstral coefficients(MFCCs) were extracted from these sound signals and encoded into spike trains by a threshold encoding *** were classified automatically as non-snoring or snoring sounds by our LSTM-SNN *** used the backpropagation algorithm based on an alternative gradient in the LSTM-SNN to complete the parameter *** categorization percentage reached an impressive 93.4%,accompanied by a remarkable 36.9% reduction in computer power compared to the regular LSTM model.

关键词： Costs Databases Computational modeling Backpropagation algorithms Sleep apnea Encoding Recording

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Activation of dislocations in Mg with solute Y

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Journal of Magnesium and Alloys 2024年第3期12卷 1045-1053页

作者： Alireza Maldar Leyun Wang Boyu Liu wenjun Liu Zhaohui Jin Bijin Zhou Xiaoqin Zeng National Engineering Research Center of Light Alloy Net Forming Shanghai Jiao Tong UniversityShanghai 200240China State Key Laboratory for Mechanical Behavior of Materials Xi’an Jiaotong UniversityXi’an 710049China Advanced Photon Source Argonne National LaboratoryIL 60439USA Shenyang National Laboratory for Materials Science Institute of Metal ResearchChinese Academy of Sciences72 Wenhua RoadShenyang 110016China School of Mechanical Engineering Suzhou University of Science and TechnologySuzhou 215009China

Mg-Y cast alloy shows excellent ductility(elongation to failure>15%)compared with pure Mg and commercial Mg cast *** monitoring the microstructure evolution during an in situ tensile test of a Mg-2.5 wt%Y alloy,we identify the activation of prismaticslip,which is rare in *** X-ray micro-beam Laue diffraction(μ-Laue)and transmission electron microscopy revealed the morphology of prismaticslip bands and individual*** functional theory and molecular dynamics calculations indicate that solute Y can significantly reduce the stacking fault energy(SFE)alongdirection on prismatic plane in Mg lattice and thus facilitate the nucleation ofdislocations during *** presence of freedislocations in the Mg lattice can also lead to nucleation of{10–12}twins even under unfavorable geometric conditions.

关键词： alloy microstructure ductility

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