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Chinese Chemical Letters 2010年第4期21卷 426-428页

作者： Zhang, yuan yuan Zeng, Xing Yan Nie, Kui zhong, Zhi Cheng wang, yu Liang wang, yu zhong Sichuan Univ Dept Chem Chengdu 610064 Peoples R China Sichuan Univ Dept Chem Engn Chengdu 610065 Peoples R China Southwest Univ Coll Anim Sci & Technol Chongqing 400715 Peoples R China

A series of ethyl 6-alkoxy-7-phenyl-4-hydroxy-3-quinolinecarboxylates were designed and *** structures were confirmed by ~1H NMR,^(13)C NMR,IR and *** biological activities were primarily evaluated against Eimeria tenella according to Anticoccidial Index(ACI) method in *** results showed that compounds 5e,5f and 5i exhibited anticoccidial activities against *** at 27 mg kg^(-1).

关键词： Ethyl 6-alkoxy-7-phenyl-4-hydroxy-3-quinolinecarboxylate Synthesis Anticoccidial activity Eimeria tenella

SYNERGISTIC EFFECTS OF NOVOLAC-BASED CHAR FORMER WITH A PHOSPHORUS/NITROGEN-CONTAINING FLAME RETARD ANT IN POLYAMIDE 6

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Chinese Journal of Polymer Science 2012年第1期30卷 72-81页

作者： Wei-cheng Xiong Li Chen De-yi wang Fei Song yu-zhong wang Center for Degradation an-d Flame--Retardant Polymeric Materials College of-Chemistry State Key Laboratory of Polymer Materials Engineering National Engineering Laboratory of Eco-Friendly Polymeric Materials （Sichuan） Sichuan University Chengdu 610064 China

The synergistic effect of phosphorus oxynitride（PON） with a novolac-based char former modified by salification （NA-metal salt） on the flame retardance of polyamide 6（PA6） was *** this purpose,various flame-retardant PA6 systems were melt-compounded with PON,PON/NA,PON/NA-V_2O_5 and PON/NA-Fe_2O_3,and their flame retardance was evaluated by measuring the limiting oxygen index（LOI） values and UL-94 vertical burning *** results showed that,compared with the PA6/PON/NA system,the combination of two char formers（NA-V_2O_5,NA-Fe_2O_3） with PON could obviously improve the char formation and flame retardance of *** flame retardance and cone calorimetric analyses showed the stronger synergism as well as the better flame retardant performance of PON/NA-Fe_2O_3 flame retardant system. The effects of different char formers on the flame retardance and thermal stability of this system were also discussed.

关键词： Polyamide Flame retardance Novolac resin Synergistic effect

Protective effects of pLNCX-SOD gene transfection on hepatocyte injury induced by obstructive jaundice in rats

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Hepatobiliary & Pancreatic Diseases International 2007年第2期6卷 194-198页

作者： Gong, Peng wang, zhong-yu wang, Hong-Jiang Dalian Med Univ Dept Gen Surg First Affiliated Hosp Dalian 116011 Peoples R China

BACKGROUND: Hydrophobic bile acids lead to the generation of oxygen free radicals in mitochondria. Accordingly, this study is to investigate if gene delivery of superoxide dismutase (SOD) will reduce hepatocyte injury caused by experimental cholestasis. METHODS: The recombinant of pLNCX-SOD gene packaged with lipofection of AMINE was transfected into hepatocytes in vitro, which stably expressed the SOD gene. RESULTS: After transfection, hepatocytes enhanced the protective effect against injury to bile and the toxicity of serum in obstructive jaundice. The inhibition of bile at the concentration of 2% (v: v, bile: DMEM 1: 50) decreased obviously from (78.80 +/- 12.35)% to (43.35 +/- 9.69)% in 12 hours, from (82.55 +/- 11.27)% to (-26.64 +/- 7.66)% in 24 hours, and from (83.83 +/- 18.69)% to (-19.27 +/- 14.38)% in 48 hours, compared with that of the untransfected cells (P < 0.01). The inhibition of serum at the obstructive jaudice concentration of 2.5% was obviously decreased from (89.72 +/- 1.52)% to (14.68 +/- 14.33)% in 12 hours, from (92.2 +/- 11.27)% to (41.39 +/- 7.66)% in 24 hours, and from (94.25 +/- 8.96)% to (22.71 +/- 4.38)% in 48 hours (P < 0.01). CONCLUSION: Hepatocytes transfected with the pLNCX-SOD gene could obviously be resistant to the toxicity of bile and serum from rat with obstructive jaundice.

关键词： obstructive jaundice retrovirus superoxide dismutase hepatocyte

STUDY ON THE EFFECTS OF TLCP ON PYROLYSIS OF PET AND ITS RETARDANT MECHANISM

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Chinese Journal of Polymer Science 2008年第1期26卷 111-116页

作者： Deng, Yi wang, yu-zhong Zong, Zhi-jing Liu, Xiu-hua Du, Xiao-hua China Acad Engn Phys Mianyang 621900 Peoples R China Sichuan Univ Ctr Degradable & Flame Retardant Polymer Mat Chengdu 610064 Peoples R China

The flame retardancy of aromatic thermotropic liquid crystal phosphorus-containing copolyester,TLCP,on PET was *** results show that the presence of TLCP promotes char formation of the substrate and enhances thermal stability of char,hence delay its *** pictures show that the char formed from PET/TLCP is more compact, therefore is more resistant to fire and heat than that from pure *** gas analysis by I.R measurements indicates that TLCP would decompose to produce phosphor...

关键词： Thermotropic liquid crystal copolymer Flame retardant PET

Non-traumatic diaphragmatic hernia of the liver in an adult:a case report

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Hepatobiliary & Pancreatic Diseases International 2007年第2期6卷 219-221页

作者： Luo, Hai-Feng Lei, Ting wang, Hong-Jiang Tan, Guang wang, zhong-yu Dalian Med Univ Dept Gen Surg First Affiliated Hosp Dalian 116011 Peoples R China Dalian Med Univ Dept Thorac Surg First Affiliated Hosp Dalian 116011 Peoples R China

BACKGROUND: Diaphragmatic hernia of the liver is a rare clinical entity, usually found after trauma in adults. This study was undertaken to elucidate a misdiagnosis of non-traumatic diaphragmatic hernia of the liver in an adult. METHOD: The clinical data of one patient with non-traumatic diaphragmatic hernia of the liver was analyzed. RESULTS: A tumor in the right lower thorax was revealed by chest X-ray and computed tomography. Non-traumatic diaphragmatic hernia of the liver was not identified until the operation. Pathological analysis confirmed the finding. The patient recovered well. CONCLUSIONS: Non-traumatic diaphragmatic hernia of the liver in an adult is a rare right-sided diaphragmatic hernia, which can move up into the chest cavity. It should be distinguished from lung cancer. The diagnosis and evaluation of non-traumatic diaphragmatic hernia of the liver can help optimize surgical management.

关键词： diaphragmatic hernia thorax liver management

New tumor-associated antigen SC6 in pancreatic cancer

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World Journal of Gastroenterology 2005年第48期11卷 7671-7675页

作者： Min-Pei Liu Xiao-zhong Guo Jian-Hua Xu Di wang Hong-yu Li zhong-Min Cui Jia-Jun Zhao Li-Nan Ren Department of Experimental Medicine Northern Hospital Shenyang Liaoning Province China

AIM: To examine the concentration of a new antigen SC6 (SC6-Ag) recognized by monoclonal antibody (MAb)in patients with pancreatic cancer and other malignant or benign diseases and to understand whether SC6-Ag has any clinical significance in distinguishing pancreatic cancer from other gastrointestinal ***: Six hundred and ninety-five serum specimens obtained from 115 patients with pancreatic cancer, 154 patients with digestive cancer and 95patients with non-digestive cancer were used and classified in this study. Serum specimens obtained from 140 patients with benign digestive disease and 89 patients with non-benign digestive disease served as controls. Ascites was tapped from 16 pancreatic cancer patients, 19 hepatic cancer patients, 16 colonic cancer patients, 10 gastric cancer and 6 severe necrotic pancreatitis patients. The samples were quantitated by solid-phase radioimmunoassay. The cut-off values (CV)of 41, 80, and 118 U/mL were ***: The average intra- and interassay CV detected by immunoradiometric assay of SC6-Ag was 5.4% and 8.7%, respectively. The sensitivity and specificity were 73.0% and 90.9% respectively. The levels in most malignant and benign cases were within the normal upper limit. Among the 16 pancreatic cancer cases, the concentration of SC6-Ag in ascites was over the normal range in 93.8% patients. There was no significant difference in the concentration of *** expression of SC6-Ag in sera was significantly related to tumor differentiation. The concentration of SC6-Ag was higher in patients before surgery than after surgery. The specificity of SC6-Ag and CA19-9 was significantly higher than that of ultrasound and computer tomography (CT) in pancreatic cancer patients. Higher positive predictive values were indicated in 92.3% SC6-Ag and 88.5% CA19-9, but lower in 73.8% ultrasound and 76.2% ***: The combined test of SC6-Ag and CA19-9 may improve the diagnostic rate of primary cancer. The detection of

关键词： Tumor antigen SC6 Pancreatic neoplasm Immunoradiometric assay

Application of camera calibrating model to space manipulator with multi-objective genetic algorithm

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Journal of Central South University 2016年第8期23卷 1937-1943页

作者：王中宇江文松王岩庆 Key Laboratory of Precision Opto-Mechatronics Technology of Ministry of Education (Beihang University) Beijing 100191 China Academy of Opto-Electronics Chinese Academy of Sciences Beijing 100094 China

The multi-objective genetic algorithm(MOGA) is proposed to calibrate the non-linear camera model of a space manipulator to improve its locational accuracy. This algorithm can optimize the camera model by dynamic balancing its model weight and multi-parametric distributions to the required accuracy. A novel measuring instrument of space manipulator is designed to orbital simulative motion and locational accuracy test. The camera system of space manipulator, calibrated by MOGA algorithm, is used to locational accuracy test in this measuring instrument. The experimental result shows that the absolute errors are [0.07, 1.75] mm for MOGA calibrating model, [2.88, 5.95] mm for MN method, and [1.19, 4.83] mm for LM method. Besides, the composite errors both of LM method and MN method are approximately seven times higher that of MOGA calibrating model. It is suggested that the MOGA calibrating model is superior both to LM method and MN method.

关键词： space manipulator camera calibration multi-objective genetic algorithm orbital simulation and measurement

Design and fabrication of superconducting HEB mixer

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Chinese Science Bulletin 2009年第12期54卷 2013-2017页

作者： wang JinPing LI YangBin KANG Lin wang yu zhong YangYin LIANG Min CHEN Jian CAO ChunHai XU WeiWei WU PeiHeng Research Institute of Superconductor Electronics (RISE) Deptartment of Electronic Science and Engineering Nanjing UniversityNanjing 210093 China

This paper describes the design and fabrication of superconducting hot electron bolometer (HEB) mixer based on ultra-thin superconducting NbN films. The high quality films were epitaxially grown on high resistance Si substrates. The device was fabricated by magnetron sputtering, electron beam lithography (EBL), reactive ion etching (RIE), lithography, and so on. The device's resistance-tempera-ture (R-T) curves and current-voltage (I-V) curves were studied. The results of THz response of the device are presented. Y-factor technique was used to measure the device's noise temperature. When the device was irradiated with a laser radiation of 2.5 THz, the obtained lowest noise temperature of the device was 2213 K.

关键词：超导制造混合器反应离子刻蚀测辐射热计反应装置薄膜外延生长光刻技术

Controllable Synthesis of Co304 from Nanosize to Microsize with Large-Scale Exposure of Active Crystal Planes and Their Excellent Rate Capability in Supercapacitors Based on the Crystal Plane Effect

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Nano Research 2011年第7期4卷 695-704页

作者： yu wang Ziyi zhong Yang Chen Cheng Theng Ng Jianyi Lin Institute of Chemical and Engineering Sciences 1 Pesek Road Jurong Island Singapore 627833

Co3O4 nanorods, nanobelts, nanosheets and cubic/octahedral nanoparticles have been successfully synthesized with tunable size from the nanoscale to the microscale, accompanied by a variation in the nature of the exposed crystal planes. The products are formed by thermal treatment of Co（CO3）05（OH）-0.11H2O nanorod, nanobelt, nanosheet and nanocubic/nanooctahedral precursors at 250 ℃. Detailed characterization, including X-ray diffraction （XRD）, scanning electron microscopy （SEM）, transmission electron microscopy （TEM）, X-ray photoelectron spectroscopy （XPS）, and nitrogen adsorption and desorption isotherms, revealed that the as-prepared nanorods, nanobelts, and nanosheet Co3O4 samples are single crystalline and mesoporous in nature with a predominance of exposed high-energy （11-0） crystal planes. They exhibited excellent electrochemical properties in supercapacitors, showing higher capacitance and better rate capability than conventional cubic/octahedral COBO4 nanoparticles having exposed low-energy （100） and （111） planes. No decay in capacitance was observed when the scan rate was increased from 5 mV/s to 100 mV/s, or from I A/g to 10 A/g. The maximum value of the specific capacitance was calculated to be 162.8 F/g and the capacitance retention reached as high as 90%. Their excellent performance in supercapacitors is believed to result from the large-area exposure of active （110） crystal planes. The Co3O4 nanosheets showed the best performance due to their larger surface area and ability to provide a better pathway for charge transfer, and are promising electrode materials for application in practical supercapacitors.

关键词： Co3O4 mesoporous single crystal energy storage supercapacitors

Metal-organic frameworks with dinuclear metal centers for synergistically boosting CO2 photoreduction

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Science China Chemistry 2025年第1期68卷 201-208页

作者： Hui-Feng wang Wen-Jie Shi yu-Xin Yang Bao-Xia Dong Tong-Bu Lu Di-Chang zhong School of Chemistry and Chemical Engineering Yangzhou University Institute for New Energy Materials and Low Carbon Technologies School of Materials Science and Engineering Tianjin University of Technology

Dinuclear metal synergistic catalysis （DMSC） has been proved powerful in boosting CO2reduction,while this has not been achieved in heterogeneous catalysts with long-range order *** this study,we,by introduction of metal catalytic centers into an indium-based metal-organic framework （MOF）,obtained a series of isostructural In-MOFs,including three MOFs with mononuclear metal catalytic center （M-In）,three MOFs with dinuclear homometallic catalytic centers （MM-In）,and three MOFs with dinuclear heterometallic catalytic centers (MM’-In,M/M’=Co（II）,Ni（II）,Zn（II）).It was found that all these MOFs can serve as catalysts for photochemical CO2reduction to *** with M-In,the catalytic activities of MM-In were obviously enhanced,and that of MM’-In was further significantly *** example,the CO yield of Co Zn-In reaches a record value of 12,700μmol g-1h-1,which is 4.0,8.1,9.4,and 18.6-fold higher than that of Co Co-In,Zn Zn-In,Co-In,and Zn-In,***,the catalytic activities of Co Ni-In and Ni Zn-In also show different fold increase than those of corresponding dinuclear homometallic and mononuclear metallic *** results of control experiments and theoretical calculation reveal that the higher catalytic activities of MM-In over M-In can be ascribed to the DMSC effect,and the higher catalytic activity of MM’-In over MM-In can be ascribed to the strengthened DMSC *** work reveals the relationship between DMSC effect and bimetal centers in CO2reduction,which provides new insights into the DMSC and paves a new way to design highly active catalysts for photochemical CO2reduction.

关键词： metal-organic frameworks dinuclear metal centers synergistic catalysis CO2 reduction photocatalysis