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Characterization and Selection of Microcrystalline Cellulose from Oil Palm Empty Fruit Bunches for Strengthening Hydrogel Films

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Journal of Renewable Materials 2024年第3期12卷 513-537页

作者： Susi Susi Makhmudun Ainuri wagiman wagiman Mohammad Affan Fajar Falah Department of Agroindustrial Technology Faculty of AgricultureUniversitas Lambung MangkuratJl A Yani Km 36BanjarbaruSouth Kalimantan70714Indonesia Doctoral Programme of Agroindustrial Technology Faculty of Agricultural TechnologyUniversitas Gadjah MadaJl Flora No.1BulaksumurYogyakarta55281Indonesia Department of Agroindustrial Technology Faculty of Agricultural TechnologyUniversitas Gadjah MadaJl Flora No.1BulaksumurYogyakarta55281Indonesia

Microcrystalline cellulose(MCC)is one of the cellulose derivatives produced as a result of the depolymerization of a part of cellulose to achieve high *** implemented in other polymers,high crystallinity correlates with greater strength and stiffnes,but it can reduce the water-holding *** acid concentration and hydrolysis time will affect the acquisition of crystallinity and water absorption capacity,both of which have significance as properties of hydrogel *** study aimed to evaluate the properties and select the MCC generated from varying the proportion of hydrochloric acid(HCl)and the appropriate hydrolysis time as a filler for film *** was produced by hydrolyzing cellulose of oil palm empty fruit bunches(OPEFB)with the HCl solution at varied concentrations and *** results show that the longer hydrolysis times and higher HCl concentrations increase crystallinity and density while lowering yield and water *** extensive acid hydrolysis reduces the amorphous area significantly,allowing the depolymerization to occur and extend the crystalline *** morphological properties of the MCC,which are smaller but compact,indicate the presence of disintegrating and diminishing structures.A 2.5 N HCl concentration and a 45-min hydrolysis time succeed in sufficient crystallinity as well as maintaining good water absorption *** treatment produced MCC with absorption capacity of 4.03±0.26 g/g,swelling capacity of 5.03±0.26 g/g,loss on drying of 1.44%±0.36,bulk and tapped density of 0.27±0.031 g/cm^(3) and 0.3±0.006 g/cm^(3),respectively,with a crystallinity index of 88.89%±4.76 and a crystallite size of 4.23±0.70 *** MCC generated could potentially be utilized as a hydrogel film filler,since a given proportion will be able to maintain the strength of the hydrogel,not readily dissolve but absorb water significantly.

关键词： Acid hydrolysis hydrogel OPEFB microcrystalline cellulose water absorption

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