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Effect of annealing on the microstructures and Vickers hardness at room temperature of intermetallics in Mo-Si system

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Rare Metals 2004年第2期23卷 176-181页

作者： YANG Haibo LI Wei SHAN Aidang wu jiansheng key laboratory of ministry of education for high temperature materials and tests & department of material science and engieering, shanghai jiao tong university, shanghai 200030, china 上海交通大学教育部高温材料及高温测试开放实验室上海 200030

The microstructures and Vickers hardness at room temperature of arc-meltingprocessed intermetallics of Mo_5Si_3-MoSi_2 hypoeutectic alloy and hypereutectic alloy annealed at1200℃ for different time were investigated. Lamellar structure consisted of Mo_5Si_3 (D8m) phaseand MoSi_2 (C11_b) phase was observed in all the alloys. For Mo_5Si_3-MoSi_2 hypoeutectic alloy, thelamellar structure was found only after annealing and developed well with fine spacing on the orderof hundred nanometers after annealing at 1200℃ for 48 h. But when the annealing time was up to 96h, the well-developed lamellar structure was destroyed. For Mo_5Si_3-MoSi_2 hypereutectic alloy, thelamellar structure was found both before and after annealing. However the volume fraction andspacing of the lamellar structure did not change significantly before and after annealing. Theeffects of the formation, development and destruction of lamellar structure on Vickers hardness ofalloys were also investigated. When Mo_5Si_3-MoSi_2 hypoeutectic alloy annealed at 1200℃ for 48 h,the Vickers hardness was improved about 19% compared with that without annealing and formation oflamellar structure. The highest Vickers hardness of Mo5Si3-MoSi_2 hypereutectic was increasing about18% when annealing at 1200℃ for 48 h.

关键词： material experiment lamellar structure microstructure vickers hardness anneal intermetallics Mo-Si system

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Investigation on Thermal Insulation and Mechanical Strength of Lightweight Aggregate Concrete and Porous Mortar in Cold Regions

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Journal of Renewable materials 2022年第12期10卷 3167-3183页

作者： Jianan wu Ke Xue Zhaowei Ding Lei Lang Kang Gu Xiaolin Li Mingli Zhang Desheng Li Ningbo City College of Vocational Technology NingboChina College of Water Conservancy and Hydropower Engineering Sichuan Agricultural UniversityYa’anChina State key laboratory of Ocean Engineering Shanghai Jiao Tong UniversityShanghaiChina College of Civil Engineering and Architecture Jiaxing UniversityJiaxingChina department of Civil Engineering Lanzhou University of TechnologyLanzhouChina department of Civil Engineering College of ScienceNanjing University of Science and TechnologyNanjingChina

Thermal insulation is an important indicator to evaluate the construction material in cold region *** we know,adding the industrial waste as lightweight aggregate or creating the pore inside the cement-based composite could make the texture loose,and the thermal insulating capacity of the material would be improved with this *** these methods,the industrial by-product and engineering waste could be cycled in an efficient ***,after service the fragmented cement composites paste could be used as aggregate in the thermal insulating concrete *** the porous texture is not favorable for the mechanical strength and long-term durability in a cold *** balance the above three requirements from two opposite directions,different processing methods were applied to create the thermal insulation concrete/***,the organic/inorganic lightweight aggregate,including the Expanded Polystyrene(EPS),Expanded Perlite(EP),and Ceramsite(CRMST)particles,were applied to create the Lightweight Aggregate Concrete(LWAC).As the comparative tests,the expanded Superabsorbent Polymer(SAP)hydrogel and Air-Entraining Agent(AEA)were also introduced to create the porous *** above concrete/mortar was tested in the normal state and under the Freeze-Thaw cycle to explore the engineering performance in cold *** the experimenting process,the thermal insulation,mechanical strength,and frost resistance of these cement-based composites were investigated,and an optimal thermal insulation concrete/mortar was determined.

关键词： Thermal insulation mechanical strength cement-based composite freeze-thaw cycle frost resistance

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