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Multiscale microstructural consideration of enhanced shear strength in TiAl intermetallic/K4169 alloy composite joints prepared by vacuum brazing with(Ti,Zr)-Ni-based amorphous filler metal

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Journal of Materials Science & Technology 2024年第5期172卷 51-70页

作者： Liangliang Zhang Honggang Dong Peng Li baosheng wu Yueting Ma Libing Huang Chao Li Jiachen Li School of Materials Science and Engineering Dalian University of TechnologyDalian 116024China

TiAl intermetallic could be used to replace Ni-based alloy in assemblies to generate excellent specific strength.A(Ti,Zr)-Ni-based amorphous filler metal Ti_(21.25)Zr_(25)Ni_(25)Cu_(18.75)(at.%)was designed using a cluster-plus-glue-atom model to successfully vacuum braze K4169 and TiAl bimetallic *** various brazing temperatures and holding time,the quantitative relationships between lattice distortion,grain boundary,dislocation density,and hardness,elastic modulus,shear strength of the joints were ***,the fracture mechanism of the joints was *** brazed seam mainly consisted of solid diffusion reaction layers(ZonesⅠandⅢ)and filler metal residue zone(ZoneⅡ).When the brazing temperature increased to 1030℃,grain refinement occurred in the brazed ***Ⅰwas primarily composed of(Ni)ss[0-11]+TiNi[011]/(Cr,Fe,Ni)ss[0-11]/(Ti,Zr)Ni[0-1-1]+(Cr,Fe,Ni)ss[0-11].The(Ti,Zr)(Ni,Cu)[001]and(Ti,Zr)(Ni,Cu)[101]intermetallic compound-based solid solutions were formed in ZoneⅡ.And the lattice distortion of(Ti,Zr)(Ni,Cu)[101]and(Ti,Zr)(Ni,Cu)[001]was 32.05%and 14.82%,*** a result,the proportion of low angle grain boundaries(LAGBs)and deformed grains in ZoneⅡrose to 38.6%and 38.7%.In ZonesⅠandⅢ,the proportion of LAGBs reduced to 8%and 3.4%,*** the holding time increased,the long-range diffusion of Al in ZoneⅡcaused the(Ti,Zr)(Ni,Cu)[001]with cubic structure to transform into(Ti,Zr)(Ni,Cu,Al)[00-1]with hexagonal crystal system structure,where the lattice distortion was 4.42%and 10.49%for a and *** 1030℃/10 min,the average geometrically nec-essary dislocation densities(GNDs)in ZonesⅠ,ⅡandⅢwere 9.87×10^(14)m^(-2),8.55×10^(14)m^(-2)and 11.4×10^(14)m^(-2),***,the shear strength of joints reached 322 MPa due to the lattice distortion,dislocation strengthening and fine grain ***,the plastic and brittle hard phases were generated in ZoneⅡand displayed a mechanical interlocking structure tha

关键词： K4169/Ti_(21.25)Zr_(25)Ni_(25)Cu_(18.75)/TiAl composite joints Intermetallic compound-based solid solution Lattice distortion Elastic modulus

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黄河下游平滩流量的模拟方法

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水利学报 2024年第7期55卷 791-801页

作者：吴保生沈逸马子普郑珊清华大学水圈科学与水利工程全国重点实验室北京100084 清华大学水利部水圈科学重点实验室北京100084 清华大学水利水电工程系北京100084 天津大学建筑工程学院天津300072

在黄河流域水沙变异背景下,准确计算黄河下游平滩流量对于河道冲淤趋势预测与悬河治理十分重要。本文在比较分析已有多个黄河下游平滩流量计算方法基础上,首先建立了考虑非汛期水沙条件影响的平滩流量滞后响应模型,再提出了基于滞后响... 详细信息

在黄河流域水沙变异背景下,准确计算黄河下游平滩流量对于河道冲淤趋势预测与悬河治理十分重要。本文在比较分析已有多个黄河下游平滩流量计算方法基础上,首先建立了考虑非汛期水沙条件影响的平滩流量滞后响应模型,再提出了基于滞后响应模型和能量法的平滩流量模拟方法,结果表明:(1)小浪底运行后非汛期水沙条件发生了重要改变,已有研究提出的三种黄河下游平滩流量计算方法中,滑动平均法、滞后响应模型、能量法均无法有效模拟2000年后的黄河下游河道平滩流量。(2)建立了考虑非汛期水沙条件影响的滞后响应模型,以反映小浪底水库运行以来非汛期来水来沙条件的影响,虽然提高了平滩流量的模拟精度,但平滩流量平衡值的计算公式中部分参数差异较大,结构形式不稳定。(3)借鉴能量法的优点,改进了平滩流量平衡值计算公式,改进后的平滩流量计算方法不仅可反映全年来水来沙的影响,而且可同时反映以床沙中值粒径为代表的床面阻力的影响,新方法不仅具有一定的理论基础,而且提高了平滩流量的模拟精度。

关键词：黄河下游平滩流量来水来沙床沙中值粒径滞后响应能量法

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小浪底水库运用以来黄河下游时空冲淤规律与模拟

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Journal of Geographical Sciences 2024年第3期34卷 591-609页

作者：沈逸吴保生王彦君覃超郑珊 State Key Laboratory of Hydroscience and Engineering Tsinghua UniversityBeijing100084China Key Laboratory of Hydrosphere Sciences of the Ministry of Water Resources Tsinghua UniversityBeijing100084China Department of Hydraulic Engineering Tsinghua UniversityBeijing100084China Key Laboratory of River Regulation and Flood Control of Ministry of Water Resources Yangtze River Scientific Research InstituteWuhan430010China State Key Laboratory of Water Resources and Hydropower Engineering Science Wuhan UniversityWuhan430072China

This study focuses on the Lower Yellow River(LYR),which has experienced continuous erosion since the operation of Xiaolangdi Reservoir in 1999,and its spatiotemporal variation process is *** on the single-step mode of the Delayed Response Model(DRM),we proposed a calculation method for simulating the accumulated erosion and deposition volume in the *** coefficient of determination R^(2)between the calculated and measured values from 2000 to 2020 is ***,the LYR is undergoing continuous erosion,however the erosion rate is gradually slowing down,and the difference between the equilibrium and calculated values of accumulated erosion and deposition volume gradually decreases,which means riverbed erosion has a tendency towards ***,we derive a formula to simulate the spatial distribution of the main channel accumulated erosion volume per unit river length in the LYR based on the non-equilibrium suspended sediment transport *** coefficient of determination R^(2)between the fitted values and measured values from 2003 to 2015 is approximately 0.98-0.99,with a relative error of approximately 6.2%.The findings in this research suggest that under the current background of decreasing sediment inflow and continuous erosion in the LYR,it takes approximately 3.0 years for the riverbed to achieve half of the erosion and deposition adjustment and approximately 13.0 years to achieve 95%of the ***,the spatial distribution of accumulated main channel erosion volume in the LYR tends to become uniform with the continuous development of *** results could provide a valuable reference for analysing the complex spatiotemporal variation process in the LYR.

关键词： Lower Yellow River erosion and deposition adjustment Delayed Response Model non-equilibrium sediment transport equation

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黄河下游河道冲淤分布模式及冲淤特征

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水利学报 2024年第4期55卷 468-480页

作者：马子普吴保生沈逸薛源覃超汪舸清华大学水圈科学与水利工程全国重点实验室北京100084

为揭示黄河下游河道的沿程冲淤分布模式及分布特征,对黄河下游1952—2021年间共70年的河段实测冲淤量数据进行了系列统计分析。研究表明:(1)黄河下游河道存在7种沿程冲淤分布模式,其中全线冲刷、全线淤积、上冲下淤、上淤下冲等4种为基... 详细信息

为揭示黄河下游河道的沿程冲淤分布模式及分布特征,对黄河下游1952—2021年间共70年的河段实测冲淤量数据进行了系列统计分析。研究表明:(1)黄河下游河道存在7种沿程冲淤分布模式,其中全线冲刷、全线淤积、上冲下淤、上淤下冲等4种为基本模式。上淤下冲模式的冲淤临界位置在孙口附近,上冲下淤模式的冲淤临界位置在游荡性河段。各模式对河道整体冲淤的贡献率存在较大差异,两边冲中间淤模式对冲刷量的贡献率最大,全线淤积模式对淤积量的贡献率最大;(2)1952年以来,黄河下游河道沿程冲淤分布模式的变化过程可分为1952—1959年、1960—1985年、1986—1999年、2000年后共4个阶段;(3)各河段冲淤量大小以0点为中心近似呈偏态分布,冲淤量在多年尺度下具有沿程减小的趋势性特征以及“冲久必淤、淤久必冲”的周期性特征;(4)各河段整体冲淤发生年数差别不大,反映了河道冲淤的平衡趋向性;70年内淤积于黄河下游河床底部的泥沙有一半左右被冲走,花园口到孙口河段的累计冲淤量接近下游总冲淤量的8成,孙口以下河段很小;(5)全线冲刷模式为小浪底水库运用后下游河道的主要冲淤模式,小花段前期淤积的泥沙基本被冲完,夹高段、高孙段及孙艾段仅冲走了前期淤积泥沙的二到三成。研究结果总结了黄河下游河道的沿程冲淤分布模式,分析了冲淤分布特征,有助于深化对下游河道冲淤现象的整体认识。

关键词：黄河下游冲淤量沿程分布模式全线冲刷全线淤积

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Ti_(43.76)Zr_(12.50)Cu_(37.49-x)Ni_(6.25)Co_(x)非晶钎料真空钎焊TC4钛合金/316L不锈钢

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焊接学报 2024年第1期45卷 47-57,I0006页

作者：韩文倩董红刚马月婷李鹏吴宝生张亮亮大连理工大学大连116024

根据双团簇模型设计并制备了Ti-Zr-Cu-Ni-Co系非晶钎料,用于真空钎焊TC4钛合金和316L不锈钢,分析了钎料中Co元素含量对钎焊接头界面微观组织形貌、力学性能及断裂行为的影响规律.结果表明,钎焊接头可划分为TC4/扩散区(Ⅰ区)/钎缝中心区... 详细信息

根据双团簇模型设计并制备了Ti-Zr-Cu-Ni-Co系非晶钎料,用于真空钎焊TC4钛合金和316L不锈钢,分析了钎料中Co元素含量对钎焊接头界面微观组织形貌、力学性能及断裂行为的影响规律.结果表明,钎焊接头可划分为TC4/扩散区(Ⅰ区)/钎缝中心区(Ⅱ区)/界面区(Ⅲ区)/316L,界面典型微观组织结构为TC4/β-Ti+Ti_(2)Cu/(Ti,Zr)_(2)(Cu,Ni)+Ti_(2)Cu+Ti_(2)(Cu,Ni)+TiFe/(Fe,Cr)_(2)Ti+α-(Fe,Cr)+τ+γ-(Fe,Ni)+σ/316L,随着Co元素含量的增加,接头剪切强度先升高后降低再升高,当Co元素含量为1.56%时达到最大310 MPa,不添加Co元素时,接头断裂于钎缝中心区(Ⅱ区);当Co元素含量为1.56%~6.24%时,接头断裂于靠近316L母材的界面区(Ⅲ区)附近,断裂模式为典型的解理断裂.

关键词：真空钎焊非晶钎料钛合金/不锈钢异种金属微观组织剪切强度

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Vacuum brazing TiAl intermetallic to K4169 alloy using amorphous filler metals Ti_(56.25–x)Zr_(x)Ni_(25)Cu1_(8.75)

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Journal of Materials Science & Technology 2023年第23期154卷 217-231页

作者： Liangliang Zhang Honggang Dong Peng Li Shuai Li baosheng wu Yueting Ma Libing Huang Chao Li Jiachen Li Yuesen Yang School of Materials Science and Engineering Dalian University of Technology Dalian 116024 China School of Mechanical Engineering North China University of Water Resources and Electric Power Zhengzhou 450045 China

A series of Ti_(56.25-x)Zr_(x)Ni_(25)Cu1_(8.75)(x=0–25,at.%) filler metals were designed based on a cluster-plus-glue-atom model to vacuum braze TiAl intermetallic to K4169 alloy. The impact of Zr content on the interfacial microstructure and shear strength of joints was examined. And the relationship between the interfacial lattice structure and the fracture behavior of the joint was investigated. The findings reveal a sectionalized characteristic with three reaction zones (Zone I, Zone II and Zone III) in the microstructure of the TiAl intermetallic to K4169 alloy joint. As the Zr content in filler metals increased, the diffusion of Ti transitioned from long-distance to short-distance in Zone I, changing the initial composition from TiNi_(3) /TiNi/NiNb/(Cr, Fe, Ni)SS to NiCrFe/(Cr, Fe, Ni)SS /TiNi. In Zone II, the initial composition altered from TiNi_(3) /TiNi to TiNi/Ti_(2) Ni/TiNi_(3) /TiCu/TiNi. The interface between Zones II and III altered from a non-coherent and semi-coherent interface of TiNi/TiAl/Ti_(3) Al with significant residual stress to a semi-coherent interface of TiNi/TiNi_(3) /TiAl_(2) /Ti_(3) Al with a gradient distribution. The shear strength of the joint initially decreased and then increased. When the Zr content of filler metal was 25 at.%, the shear strength of the joint reached 288 MPa. The crack initiation position changed from non-coherent TiNi/TiAl interface with high angle grain boundaries (HAGBs) and lattice mismatch of 65.86 at.% to a semi-coherent Ti3 Al/TiAl2 interface with a lattice mismatch of 20.07 at.% when the Zr content increased. The brittle fracture was present on the fracture surfaces of all brazed joints.

关键词： Vacuum brazing TiAl intermetallic to K4169 alloy brazed joint Ti-Ni based amorphous filler metal EBSD Lattice mismatch

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Effect of Three-High Rotary Piercing Process on Microstructure,Texture and Mechanical Properties of Magnesium Alloy Seamless Tube

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Acta Metallurgica Sinica(English Letters) 2024年第6期37卷 953-968页

作者： Xiaofeng Ding Zehao wu Tong Li Jianxun Chen Yuanhua Shuang baosheng Liu Heavy Machinery Engineering Research Center of Education Ministry Taiyuan University of Science and TechnologyTaiyuan030024China College of Materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan030024China

Mg alloy seamless tubes(MASTs)were prepared through three-high rotary piercing process,effect of billet temperature,feed angle and plug advance on microstructure,texture and mechanical properties of tubes were *** effect on the deformation mechanism and improving mechanical properties mechanism of this process for MASTs were *** results show that the grain size could be refined to 11.3-31.1%of the initial grain size and the microstructure was more uniform due to the accumulation of *** formation of high strain gradient at the grain boundary activated the non-basal *** piercing process could change the grain orientation of as-extruded billet and eliminate the initial basal texture to produce new favorable *** the process could accelerate the continuous dynamic recrystallization *** piercing,yield strength of pierced tubes decreased by 6.7%,ultimate tensile strength(UTS)and elongation increased by 32.4 and 45%,respectively,at optimal *** plate-shapedβ_(1)-Mg_(17)Al_(12) orientation transformed from basal plates to prismatic plates,facilitating the increase in UTS and *** decrease size of nanoscale precipitates could reduce the cracking *** critical resolved shear stress ratios of pyramidal(10−11)slip and(11−22)slip to basal slip for the sample including prismatic plates both decreased compared to that including basal *** could enhance the ductility of tube ***,grain boundary sliding could contribute to a better ductility via coordinating deformation and reducing stress concentration during piercing process.

关键词： Mg alloy tube Rotary piercing Microstructure Texture Mechanical properties

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Fluvial Processes in the Meandering Reach of the Lower Wei River During the Course of Degradation

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四川大学学报（工程科学版） 2005年第S1期37卷 46-51页

作者： Xia, Junqiang Wang, Guangqian wu, baosheng Dept. of Hydraulic Eng. Tsinghua Univ. Beijing 100084 China

This paper presents an analysis of the changes of the longitudinal and lateral profiles in the meander- ing reach of the Lower Wei River over the period from October 1973 to October 1976 during the course of *** results indicated that retrogressive erosion and subsequent downstream erosion occurred in the reach due to the lowering in the Tongguan elevation and the inflowing water carrying low sediment con- *** the end of the degradation,the main channel widths of the majority ...

关键词： the Lower Wei River fluvial processes batse level of erosion channel widening channel undercut

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Microstructures,corrosion behavior and mechanical properties of as-cast Mg-6Zn-2X(Fe/Cu/Ni)alloys for plugging tool applications

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International Journal of Minerals,Metallurgy and Materials 2024年第4期31卷 697-711页

作者： baosheng Liu Jiali Wei Shaohua Zhang Yuezhong Zhang Pengpeng wu Daqing Fang Guorui Ma School of Materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan 030024China State Key Laboratory for Mechanical Behavior of Materials Xi’an Jiaotong UniversityXi’an 710049China Intelligent Equipment Research and Development Center Zhuhai Institute of Advanced Technology Chinese Academy of SciencesZhuhai 519080China Advanced Materials Research Institute Zhuhai Dingmei Medical Technology Co.Ltd.Zhuhai 519000China

Mg-6Zn-2X(Fe/Cu/Ni)alloys were prepared through semi-continuous casting,with the aim of identifying a degradable magnesium(Mg)alloy suitable for use in fracturing balls.A comparative analysis was conducted to assess the impacts of adding Cu and Ni,which result in finer grains and the formation of galvanic corrosion *** electronic microscopy examination revealed that precipitated phases concentrated at grain boundaries,forming a semi-continuous network structure that facilitated corrosion penetration in Mg-6Zn-2Cu and Mg-6Zn-2Ni *** corrosion was observed in Mg-6Zn-2Fe,while galvanic corrosion was identified as the primary mechanism in Mg-6Zn-2Cu and Mg-6Zn-2Ni *** the tests,the Mg-6Zn-2Ni alloy exhibited the highest corrosion rate(approximately 932.9 mm/a)due to its significant potential *** testing showed that Mg-6Zn-2Ni alloy possessed suitable ultimate compressive strength,making it a potential candidate material for degradable fracturing balls,effectively addressing the challenges of balancing strength and degradation rate in fracturing applications.

关键词： magnesium alloys microstructure micro-galvanic corrosion mechanical properties

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Monsoon boosted radiation of the endemic East Asian carps

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Science China(Life Sciences) 2023年第3期66卷 563-578页

作者： Chenguang Feng Kun Wang Wenjie Xu Liandong Yang Kunyuan Wanghe Ning Sun baosheng wu Feixiang wu Lei Yang Qiang Qiu Xiaoni Gan Yiyu Chen Shunping He State Key Laboratory of Freshwater Ecology and Biotechnology Institute of HydrobiologyChinese Academy of SciencesWuhan 430072China School of Ecology and Environment Northwestern Polytechnical UniversityXi'an 710072China Key Laboratory of Adaptation and Evolution of Plateau Biota of Chinese Academy of Sciences Northwest Institute of Plateau BiologyChinese Academy of SciencesXining 810008China University of Chinese Academy of Sciences Beijing 100039China Key Laboratory of Vertebrate Evolution and Human Origins of Chinese Academy of Sciences Institute of Vertebrate Paleontology and PaleoanthropologyChinese Academy of SciencesBeijing 100044China Florida Museum of Natural History University of FloridaGainesvilleFL 32611USA National Natural Science Foundation of China Beijing 100085China Center for Excellence in Animal Evolution and Genetics Kunming Institute of ZoologyChinese Academy of SciencesKunming 650223China

Major historical events often trigger the rapid flourishing of a few lineages,which in turn shape established biodiversity *** did this process occur and develop?This study provides a window into this *** endemic East Asian carps(EEAC)dominated the ichthyofauna of East Asia and exhibited a high degree of adaptation to monsoonal river-lake ecosystems.A series of evidence,including ecogeography,phylogenetics,and macroevolution,suggests that the EEAC is a lineage that arose with the East Asian monsoon and thrived intimately with subsequent monsoon *** further deduce the evolution of the EEAC and find that a range of historical events in the monsoon setting(e.g.,marine transgression and regression and glacial-interglacial cycle)have further reshaped the distribution patterns of EEAC’s *** genomics analyses reveal that introgressions during the initial period of EEAC radiation and innovations in the regulation of the brain and nervous system may have aided their adaptation to river-lake ecosystems in a monsoon setting,which boosted ***,this study strengthens knowledge of the evolutionary patterns of freshwater fishes in East Asia and provides a model case for understanding the impact of major historical events on the evolution of biota.

关键词： adaptive radiation Xenocyprididae east Asian monsoon genomes macroevolution phylogenomics

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