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Microstructural evolution and superelastic properties of ultrafine-graine d NiTi-base d shape memory alloy via sintering of amorphous ribbon precursor

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Journal of Materials Science & Technology 2023年第7期138卷 80-92页

作者： w.S.Cai h.Z.Lu h.Z.Li Z.Liu h.B.Ke w.h.wang C.Yang National Engineering Research Center of Near-net-shape Forming for Metallic Materials Guangdong Provincial Key Laboratory for Processing and Forming of Advanced Metallic MaterialsSouth China University of TechnologyGuangzhou 510640China Songshan Lake Materials Laboratory Dongguan 523808China Institute of Physics Chinese Academy of SciencesBeijing 100190China

NiTi-based shape memory alloys(SMAs)are considered as cutting-edge intelligent functional materials.however,it remains a great challenge to obtain ultrafine-grained(UFGed)bulk materials with mm-scale size as well as outstanding superelastic properties.here,UFGed bulk Ti_(35)Zr_(15)Ni_(35)Cu_(15)NiTi-based SMA is successfully prepared via spark plasma sintering of amorphous ribbon precursor at different sintering temperatures,and microstructural evolution and superelastic properties are symmetrically investigated.It is found that its grain size ranges from UFG to micro-grain with increased sintering temperature regard-less of the predominant B2 matrix in all bulk samples.Interestingly,the orientation relationships between B2 matrix and nano-scale fcc(Ti,Zr)_(2)Ni precipitate evolve from coherent to incoherent.Consequently,the UFGed samples exhibit perfect superelasticity with the high recoverable strain of∼5.8%,the stable recov-ery rate above 99%,and the great critical stress inducing martensitic transformation higher than 1 GPa,far superior to the corresponding ones of suction-cast micro-grained TiZrNiCu SMAs.Fundamentally,the perfect superelasticity is attributed to the good resistance to dislocation slip or grain boundary slip by residual nano-scale amorphous phase or secondary phase of coherent and semi-coherent fcc(Ti,Zr)_(2)Ni precipitate.In addition,the gentle superelastic plateau is associated to the favorable transfer stress and the strong ability to accommodate dislocation movement,which is generated by the coherent interface between nano-scale fcc(Ti,Zr)_(2)Ni and UFGed B2 matrix.These results suggest that spark plasma sintering of amorphous alloy precursor is a feasible route to obtaining excellent superelasticity in NiTi-based SMAs.

关键词： Shape memory alloy Amorphous alloy Microstructure Superelasticity

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Interface dominated deformation transition from inhomogeneous to apparent homogeneous mode in amorphous/amorphous nanolaminates

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Journal of Materials Science & Technology 2022年第4期99卷 178-183页

作者： Z.Q.Chen M.C.Li J.S.Cao F.C.Li S.w.Guo B.A.Sun h.B.Ke w.h.wang Songshan Lake Materials Laboratory Dongguan 523808PR China Institute of Physics Chinese Academy of SciencesBeijing 100190PR China Institute of Materials Engineering Nanjing UniversityNantong 226019PR China School of Physics Science and Technology Xinjiang UniversityXinjiang 830046PR China School of Physical Sciences University of Chinese Academy of SciencesBeijing 100049PR China State Key Laboratory for Mechanical Behavior of Material Xi'an Jiaotong UniversityXi’an 710049PR China

The amorphous/amorphous nanolaminates(A/ANLs)have aroused great attentions owing to their tunable structure and enhanced mechanical properties.however,the plastic deformation mechanism of A/ANLs have yet been clarified.here,we systematically examined the mechanical properties and deformation behavior of series of NiNb/ZrCuNi Al A/ANLs via nanoindentaion test.It was found that both the amount and morphology of amorphous/amorphous interface(A/AIs)played crucial roles in the plastic deformation of A/ANLs.Less and straighter A/AIs facilitated multiple shear banding deformation,of which the hardness increased with decreasing layer thickness,as the A/AIs hindered the propagation of shear bands(SBs).whilst,more and wavier A/AIs promoted homogeneous deformation,of which the hardness stayed at a much lower value and was relatively irrelevant with the layer thickness,for the promoted activation of shear transformation zones by A/AIs.Our results provide guidance for modifying the mechanical properties of amorphous alloys with interface engineering design.

关键词： Amorphous alloys Nanolaminates Shear bands hardness Interface

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hardening and toughening effects of intermediate nanosized structures in a confined amorphous alloy film

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Journal of Materials Science & Technology 2022年第23期118卷 44-53页

作者： Z.Q.Chen M.C.Li X.Tong Y.Zhao J.Y.Xie S.w.Guo P.huang F.wang h.B.Ke B.A.Sun w.h.wang Songshan Lake Materials Laboratory Dongguan 523808China Institute of Physics Chinese Academy of SciencesBeijing 100190China Xinjiang Key Laboratory of Solid State Physics and Devices and School of Physical Science and Technology Xinjiang UniversityXinjiangUrumqi 830046China Key Laboratory of LCR Materials and Devices of Yunnan Province School of Materials and EnergyYunnan UniversityKunming 650091China State-Key Laboratory for Mechanical Behavior of Material Xi’an Jiaotong UniversityXi’an 710049China State Key Laboratory for Strength and Vibration of Mechanical Structures Xi’an Jiaotong UniversityXi’an 710049China National Demonstration Center for Experimental Mechanics Education Xi’an Jiaotong UniversityXi’an 710049China

The plastic deformation of amorphous alloys is well known to be localized into shear bands(SBs),which are believed to stem from the atomic-scale flow defects,i.e.,shear transformation zones(STZs).Yet,the bridge between the mesoscopic SBs and the atomic-scale STZs remains poorly understood.In this work,through thermally activating pronouncedβrelaxations in the well-designed crystalline-layer confined amorphous(CLCA)Ni w alloy films,we experimentally captured and observed an intermediate nanosized structure termed as“nano shear bands”(NSBs)with a typical size of 1–2 nm in thickness and5–10 nm in length.The influences of such NSB structures on the macroscale deformation behavior were systematically investigated.It was found that NSBs lead to both hardening and toughening effects for the CLCA films,as they promote multiple and controlled shear banding deformation,which results in enhanced crystallization.The intermediate NSB structure could connect the microstructural characteristics and macroscopic plasticity in amorphous alloys and may provide new insights for understanding the microscopic deformation mechanism of amorphous alloys as well as tuning/designing their properties.

关键词： Amorphous alloys Nano shear band hardening Toughening Crystallization

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A Diagram for Glass Transition and Plastic Deformation in Model Metallic Glasses

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Journal of Materials Science & Technology 2014年第6期30卷 546-550页

作者： X.Q.Gao w.h.wang h.Y.Bai Institute of Physics Chinese Academy of Sciences

In this paper, we report a strain rate related glass transition in model SrCaYbMg（Li）Zn（Cu） metallic glasses at room temperature. A critical strain rate, equivalent to glass transition temperature, is found for the strain rate induced glassy state to liquid-like viscoplastic state translation. The results show that the observation time, equivalent to temperature and stress, is a key parameter for the transition between the glass and supercooled liquid states. A three-dimension glass transition diagram involved in time, temperature and stress in metallic glasses is established.

关键词： homogeneous plastic flow Glass transition Metallic glass

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Microstructure change in Fe-based metallic glass and nanocrystalline alloy induced by liquid nitrogen treatment

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Journal of Materials Science & Technology 2021年第10期69卷 1-6页

作者： M.C.Ri D.w.Ding Y.h.Sun w.h.wang Institute of Physics Chinese Academy of SciencesBeijing100190China Songshan Lake Materials Laboratory Dongguan523808China

The effects of acyclic liquid nitrogen(LN)treatment in a temperature range of-196℃to 50℃on the thermal and magnetic stability of Fe78Si9B13 and Fe73.5Si13.5B9Nb3Cu1 glassy ribbons have been studied.The intrinsic heterogeneities of the metallic glasses can be activated through cryogenic thermal cycling,making irreversible structural changes after the treatment and inducing rejuvenation to the materials.The microstructural changes of both Fe-based metallic glass(MG)and nanocrystalline alloy induced by LN treatment were investigated.The experimental results show that the LN treatment could effectively rejuvenate the Fe-Si-B MGs and change their thermomechanical and magnetic properties.Based on the partially-crystallinity and well-known magnetic constants,the increase of the energy at the order of 10m J/g and magnetic domain wall movement and rotation at the order of 5-6μm and 0.5°-0.8°are found for FINEMET-type amorphous alloy after LN treatment.It is also found that LN treatment can contribute a little stored energy to the magnetic domain wall movement and magnetic domain rotation.

关键词： Metallic glasses Cryogenic thermal treatment Soft magnetic materials Rejuvenation Stored energy Domain wall

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Foreword

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Journal of Materials Science & Technology 2014年第6期30卷 I0001-I0002页

作者： w.h.wang Z.F.Zhang Institute of Physics Chinese Academy of Sciences at Beijing

As a new class of advanced materials, metallic glasses （also often referred as amorphous alloys） possess a combination of unique amorphous structure and remarkably impressive mechanical and physical properties, and are now at the cutting edge of research. The emergence of bulk metallic glasses （BMGs） provides more alloy compositions, large geometric size and diverse mechanical behaviors for some fundamental issues such as deformation and fracture mechanisms of glassy materials and potentiates possibly great applications. In particular, the BMG-s exhibit many unique mechanical properties, such as superior strength and hardness, excellent scratch and wear resistance, extremely high elastic limit, and diverse fracture toughness （varying significantly from approaching ideal brittleness like the oxide glasses for Mg-based BMGs to the highest known damage tolerance for Pd-based BMGs） and patterns （such as dimple structures, nanoscale periodic corrugations, and fiver patterns）. It has become possible to experimentally characterize the mechanical behaviors of metallic glasses and to explore their correlations with the processing conditions, structures and other properties, and accordingly in a more general sense, to understand the deformation, energy dissipation, and fracture mechanisms in the disordered glassy materials. The important and interesting mechanical properties and deformation mechanisms are currently the focus of intense research in the material science community, and the corresponding studies on them are progressing at a fast pace.

关键词： BMGs Foreword

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Effect of solute atom concentration and precipitates on serrated flow in Mg-3Nd-Zn alloy

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Journal of Materials Science & Technology 2018年第7期34卷 1236-1242页

作者： w.h.wang D.wu R.S.Chen X.N.Zhang State Key Laboratory of Metal Matrix Composites School of Materials Science and Engineering Shanghai Jiao Tong University The Group of Magnesium Alloys and Their Applications Institute of Metal Research Chinese Academy of Sciences

Influence of solute atom concentration and precipitates on serrated flow, i.e., Portevin-Le Chatelier effect, was studied in Mg-3Nd-Zn alloy by tensile test at 250℃ with a strain rate of l x 10^-3 s^-1 Microstructure and tensile property of the Mg-3Nd-Zn alloy in solution and aging conditions were also investigated. Results indicate that the serrated flow was weakened with aging time, and geometry of the serrations changed from sharp to rounded corner. Through analyzing the mechanism of the interactions between dislocations and solute atoms, it was identified that the precipitates did not only weaken the serrated flow due to the decrease in the concentration of solute atom, but also regulate the serration type by restraining the movement of dislocations during high temperature deformation.2017 Published by Elsevier Ltd on behalf of The editorial office of Journal of Materials Science ＆ Technology.

关键词： Magnesium alloy Serrated flow Precipitate heat treatment Deformation behavior

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Composition and size dependent torsion fracture of metallic glasses

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Journal of Materials Science & Technology 2021年第23期82卷 153-160页

作者： J.Dong J.Shen Y.h.Sun h.B.Ke B.A.Sun w.h.wang h.Y.Bai Institute of Physics Chinese Academy of SciencesBeijing100190PR China College of Materials Science and Opto Electronic Technology University of Chinese Academy of SciencesBeijing100049PR China Songshan Lake Materials Laboratory DongguanGuangdong523808PR China

The fracture of metallic glasses(MGs)of different compositions and sizes down to micrometers under torsion loading were systematically investigated.Contrary to the flat shear fracture along the circumferential plane as commonly supposed under torsion,we find that the torsion fracture of metallic glasses can deviate from flat shear plane,and the fracture angle is closely dependent on the composition and the size of MG samples.with a conversion method,we show that the torsion fracture of both millimeterand micrometer-sized MGs can be described by the ellipse fracture criterion as originally proposed for the tension fracture.The deviation from the circumferential shear plane under torsion is further shown to intrinsically relate to the fracture toughness of MGs.The tougher MG tends to have a smaller fracture angle with respect to the maximum shear plane,and vice versa,indicating a correlation between the fracture toughness and pressure/normal stress sensitivity in MGs.Our results provide new insights on the fracture mechanism and are helpful to design and control the deformation and fracture behavior of MGs under torsion loading.

关键词： Metallic glasses Torsion fracture Pressure sensitivity Fracture toughness

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Unusually thick shear-softening surface of micrometer-size metallic glasses

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The Innovation 2021年第2期2卷 174-182页

作者： J.Dong Y.huan B.huang J.Yi Y.h.Liu B.A.Sun w.h.wang h.Y.Bai Institute of Physics Chinese Academy of SciencesBeijing 100190China College of Materials Science and Opto-Electronic Technology University of Chinese Academy of SciencesBeijing 100049China State Key Laboratory of Nonlinear Mechanics(LNM) Institute of MechanicsChinese Academy of SciencesBeijing 100190China Institute of Materials School of Materials Science and EngineeringShanghai UniversityShanghai 200444China Songshan Lake Materials Laboratory DongguanGuangdong 523808China

The surface of glass is crucial for understanding many fundamental processes in glassy solids.A common notion is that a glass surface is a thin layer with liquid-like atomic dynamics and a thickness of a few tens of nanometers.here,we measured the shear modulus at the surface of both millimeter-size and micrometer-size metallic glasses(MGs)through high-sensitivity torsion techniques.we found a pronounced shear-modulus softening at the surface of MGs.Compared with the bulk,the maximum decrease in the surface shear modulus(G)for the micro-scale MGs reaches~27%,which is close to the decrease in the G upon glass transition,yet it still behaves solid-like.Strikingly,the surface thickness estimated from the shear-modulus softening is at least 400 nm,which is approximately one order of magnitude larger than that revealed from the glass dynamics.The unusually thick surface is also confirmed by measurements using X-ray nano-computed tomography,and this may account for the brittle-to-ductile transition of the MGs with size reductions.The unique and unusual properties at the surface of the micrometer-size MGs are physically related to the negative pressure effect during the thermoplastic formation process,which can dramatically reduce the density of the proximate surface region in the supercooled liquid state.

关键词： glass surface shear modulus torsion metallic glasses

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Study of BESIII trigger efficiencies with the 2018 J/ψ data

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Chinese Physics C 2021年第2期45卷 48-55页

作者： M.Ablikim M.N.Achasov P.Adlarson S.Ahmed M.Albrecht R.Aliberti A.Amoroso M.R.An Q.An X.h.Bai Y.Bai O.Bakina R.Baldini Ferroli I.Balossino Y.Ban K.Begzsuren N.Berger M.Bertani D.Bettoni F.Bianchi J.Bloms A.Bortone I.Boyko R.A.Briere h.Cai X.Cai A.Calcaterra G.F.Cao N.Cao S.A.Cetin J.F.Chang w.L.Chang G.Chelkov D.Y.Chen G.Chen h.S.Chen M.L.Chen S.J.Chen X.R.Chen Y.B.Chen Z.J Chen w.S.Cheng G.Cibinetto F.Cossio X.F.Cui h.L.Dai X.C.Dai A.Dbeyssi R.E.de Boer D.Dedovich Z.Y.Deng A.Denig I.Denysenko M.Destefanis F.De Mori Y.Ding C.Dong J.Dong L.Y.Dong M.Y.Dong X.Dong S.X.Du Y.L.Fan J.Fang S.S.Fang Y.Fang R.Farinelli L.Fava F.Feldbauer G.Felici C.Q.Feng J.h.Feng M.Fritsch C.D.Fu Y.Gao Y.Gao Y.Gao Y.G.Gao I.Garzia P.T.Ge C.Geng E.M.Gersabeck A Gilman K.Goetzen L.Gong w.X.Gong w.Gradl M.Greco L.M.Gu M.h.Gu S.Gu Y.T.Gu C.Y Guan A.Q.Guo L.B.Guo R.P.Guo Y.P.Guo A.Guskov T.T.han w.Y.han X.Q.hao F.A.harris h hüsken K.L.he F.h.heinsius C.h.heinz T.held Y.K.heng C.herold M.himmelreich T.holtmann Y.R.hou Z.L.hou h.M.hu J.F.hu T.hu Y.hu G.S.huang L.Q.huang X.T.huang Y.P.huang Z.huang T.hussain w.Ikegami Andersson w.Imoehl M.Irshad S.Jaeger S.Janchiv Q.Ji Q.P.Ji X.B.Ji X.L.Ji h.B.Jiang X.S.Jiang J.B.Jiao Z.Jiao S.Jin Y.Jin T.Johansson N.Kalantar-Nayestanaki X.S.Kang R.Kappert M.Kavatsyuk B.C.Ke I.K.Keshk A.Khoukaz P.Kiese R.Kiuchi R.Kliemt L.Koch O.B.Kolcu B.Kopf M.Kuemmel M.Kuessner A.Kupsc M.G.Kurth w.Kühn J.J.Lane J.S.Lange P.Larin A.Lavania L.Lavezzi Z.h.Lei h.Leithoff M.Lellmann T.Lenz C.Li C.h.Li Cheng Li D.M.Li F.Li G.Li h.Li h.Li h.B.Li h.J.Li J.L.Li J.Q.Li J.S.Li Ke Li L.K.Li Lei Li P.R.Li S.Y.Li w.D.Li w.G.Li X.h.Li X.L.Li Z.Y.Li h.Liang h.Liang h.Liang Y.F.Liang Y.T.Liang L.Z.Liao J.Libby C.X.Lin B.J.Liu C.X.Liu D.Liu F.h.Liu Fang Liu Feng Liu h.B.Liu h.M.Liu huanhuan Liu huihui Liu J.B.Liu J.L.Liu J.Y.Liu K.Liu K.Y.Liu Ke Liu L.Liu M.h.Liu P.L.Liu Q.Liu Q.Liu S.B.Liu Shuai Liu T.Liu w.M.Liu X.Liu Y.Liu Y.B.Liu Z.A.Liu Z.Q.Liu X.C.Lou F.X.Lu h.J.Lu J.D.Lu J.G.Lu X.L.Lu Y.Lu Y.P.Lu C.L.Luo M.X.Luo b P.w.Luo T.Luo X.L.Luo S Institute of high Energy Physics Beijing 100049China Beihang University Beijing 100191China Beijing Institute of Petrochemical Technology Beijing 102617China Bochum Ruhr-University D-44780 BochumGermany Carnegie Mellon University PittsburghPennsylvania 15213USA Central China Normal University Wuhan 430079China China Center of Advanced Science and Technology Beijing 100190China COMSATS University Islamabad Lahore CampusDefence RoadOff Raiwind Road54000 LahorePakistan Fudan University Shanghai 200443China GIBudker Institute of Nuclear Physics SB RAS(BINP) Novosibirsk 630090Russia GSI helmholtzcentre for heavy Ion Research Gmbh D-64291 DarmstadtGermany Guangxi Normal University Guilin 541004China Guangxi University Nanning 530004China hangzhou Normal University Hangzhou 310036China helmholtz Institute Mainz Johann-Joachim-Becher-Weg 45D-55099 MainzGermany henan Normal University Xinxiang 453007China henan University of Science and Technology Luoyang 471003China huangshan College Huangshan 245000China hunan Normal University Changsha 410081China hunan University Changsha 410082China Indian Institute of Technology Madras Chennai 600036India Indiana University BloomingtonIndiana 47405USA (A)INFN Laboratori Nazionali di Frascati I-00044FrascatiItaly(B)INFN Sezione di PerugiaI-06100PerugiaItaly(C)University of PerugiaI-06100PerugiaItaly (A)INFN Sezione di Ferrara I-44122FerraraItaly(B)University of FerraraI-44122FerraraItaly Institute of Modern Physics Lanzhou 730000China Institute of Physics and Technology Peace Ave54BUlaanbaatar 13330Mongolia Jilin University Changchun 130012China Johannes Gutenberg University of Mainz Johann-Joachim-Becher-Weg 45D-55099 MainzGermany Joint Institute for Nuclear Research 141980 DubnaMoscow regionRussia Justus-Liebig-Universitaet Giessen IIPhysikalisches InstitutHeinrich-Buff-Ring 16D-35392GiessenGermany KVI-CART University of GroningenNL-9747 AA GroningenThe Netherlands Lanzhou University Lanzhou 730000China Liaoning Normal Unive

Using a dedicated data sample taken in 2018 on the J/ψpeak,we perform a detailed study of the trigger efficiencies of the BESIII detector.The efficiencies are determined from three representative physics processes,namely Bhabha scattering,dimuon production and generic hadronic events with charged particles.The combined efficiency of all active triggers approaches 100%in most cases,with uncertainties small enough not to affect most physics analyses.

关键词： BESIII trigger efficiency Bhabha dimuon hadronic events

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