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An oxygenating colloidal bioink for the engineering of biomimetic tissue constructs

Bio-Design and Manufacturing 2024年第3期7卷 240-261页

作者： Seol-Ha Jeong Jarno Hiemstra Patrick v.Blokzijl Rebeca Damian-Ferrara Danilo Martins dos Santos Jéssica H.L.da Fonseca Min-Ho Kang Jihyun Kim Dilara Yilmaz-Aykut Mei L.L.Cham-Pérez Jeroen Leijten Su Ryon shin Div.sion of Engineering in Medicine Department of MedicineBrigham and Women’s HospitalHarvard Medical SchoolBostonMA 02139USA Leijten Lab Department of Developmental BioEngineeringFaculty of Science and TechnologyTechnical Medical CentreUniversity of TwenteDrienerlolaan 57522 NB EnschedeThe Netherlands Nanotechnology National Laboratory for Agriculture(LNNA) Embrapa InstrumentaçãoSao CarlosSao Paulo 13560-970Brazil Department of Biomedical-Chemical Engineering The Catholic University of Korea43 Jibong-roBucheon-siGyeonggi-do 14662Republic of Korea Department of Biotechnology The Catholic University of Korea43 Jibong-roBucheon-siGyeonggi-do 14662Republic of Korea

Ensuring a sufficient oxygen supply is piv.tal for the success of bioprinting applications since it fosters tissue integration and natural *** in oxygen concentration among div.rse tissues necessitates the precise recreation of tissue-specific oxygen lev.ls in imprinted constructs to support the surv.v.l of targeted *** oxygen-releasing biomaterials,such as oxygen-generating microparticles(OMPs),hav. shown promise for enhancing the oxygen supply of microenv.ronments in injured tissues,whether this approach is scalable for large tissues and whether tissue-specific bioinks with v.rying OMP concentrations remain printable remain *** study addresses this critical gap by introducing an innov.tiv. class of engineered oxygenated bioinks that combine colloidal-based microgels with *** report that incorporating nanosized calcium peroxide(nCaO_(2))and manganese oxide nanosheets(nMnO_(2))into hydrophobic polymeric microparticles enables precise modulation of oxygen release while controlling hydrogen peroxide ***,the fabrication of oxygenating and cytocompatible colloidal gels is achiev.d using an aqueous two-phase *** study thoroughly ev.luates the fundamental characteristics of the resulting bioink,including its rheological behav.ors,printability,shape fidelity,mechanical properties,and oxygen release ***,this study demonstrates the macroscopic scalability and cytocompatibility of printed constructs produced v.a cell-laden oxygenating colloidal *** showcasing the effectiv.ness of extrusion-based bioprinting,this study underscores how it can be used to fabricate biomimetic tissues,indicating its potential for new *** findings presented here adv.nce the bioprinting field by achiev.ng scalability with both high cell v.ability and the possibility of mimicking specifically oxygenated *** work thereby offers a promising av.nue for the dev.lopment of functional tissues with e

关键词： 3D bioprinting Bioink Colloidal gels Extrusion printing Oxygen-generating microparticle

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Surface engineering of ZnO electrocatalyst by N doping towards electrochemical CO_(2) reduction

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Journal of Energy Chemistry 2024年第1期88卷 71-81,I0002页

作者： Rohini Subhash Kanase Getasew Mulualem Zewdie Maheswari Arunachalam Jyoti Badiger Suzan Abdelfattah Sayed Kwang-Soon Ahn Jun-Seok Ha Uk Sim Hyeyoung shin Soon Hyung Kang Department of Interdisciplinary Program for Photonic Engineering Chonnam National UniversityGwangju 61186Republic of Korea Graduate School of Energy Science and Technology(GEST) Chungnam National University99 Daehak-roYuseong-guDaejeon 34134Republic of Korea Department of Chemistry Education and Optoelectronic Conv.rgence Research Center Chonnam National UniversityGwangju 61186Republic of Korea Department of Adv.nced Chemicals and Engineering Chonnam National UniversityGwangju 61186Republic of Korea School of Chemical Engineering Yeungnam UniversityGyeongsan 38541Republic of Korea Department of Energy Engineering Korea Institute of Energy Technology(KENTECH)Naju 58217Republic of Korea

The discov.ry of efficient,selectiv.,and stable electrocatalysts can be a key point to produce the largescale chemical fuels v.a electrochemical CO_(2) reduction(ECR).In this study,an earth-abundant and nontoxic ZnO-based electrocatalyst was dev.loped for use in gas-diffusion electrodes(GDE),and the effect of nitrogen(N)doping on the ECR activ.ty of ZnO electrocatalysts was ***,a ZnO nanosheet was prepared v.a the hydrothermal method,and nitridation was performed at different times to control the N-doping *** an increase in the N-doping content,the morphological properties of the nanosheet changed significantly,namely,the 2D nanosheets transformed into irregularly shaped ***,the ECR performance of Zn O electrocatalysts with different N-doping content was assessed in 1.0 M KHCO_(3) electrolyte using a gas-diffusion electrode-based ECR *** the ECR activ.ty increased after a small amount of N doping,it decreased for higher N doping *** them,the N:ZnO-1 h electrocatalysts showed the best CO selectiv.ty,with a faradaic efficiency(FE_(CO))of 92.7%at-0.73 v.*** hydrogen electrode(RHE),which was greater than that of an undoped Zn O electrocatalyst(FE_(CO)of 63.4%at-0.78 v.(RHE)).Also,the N:ZnO-1 h electrocatalyst exhibited outstanding durability for 16 h,with a partial current density of-92.1 mA cm^(-2).This improv.ment of N:ZnO-1 h electrocatalyst can be explained by density functional theory calculations,demonstrating that this improv.ment of N:ZnO-1 h electrocatalyst comes from(ⅰ)the optimized activ. sites lowering the free energy barrier for the rate-determining step(RDS),and(ⅱ)the modification of electronic structure enhancing the electron transfer rate by N doping.

关键词： ZnO N-doped ZnO Gas-diffusion electrode CO Selectiv.ty Electrochemical CO_(2)reduction

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In-situ study of the microstructure ev.lution during tension of a Mg-Y-Zn-Al alloy processed by rapidly solidified ribbon consolidation technique

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Journal of Magnesium and Alloys 2024年第5期12卷 2024-2040页

作者： Jeno Gubicza Kristián Máthis Péter Nagy Péter Jenei Zoltán Hegedus Andrea Farkas Jozef v.sely shin-ichi Inoue Daria Drozdenko Yoshihito Kawamura Department of Materials Physics Faculty of ScienceEotvos Loránd UniversityPázmány P.sétány 1/ABudapest H-1117Hungary Department of Physics of Materials Faculty of Mathematics and PhysicsCharles UniversityKe Karlovu 512116 Praha 2Czech Republic Deutsches Elektronen-Synchrotron DESY Notkestr.85Hamburg 22603Germany Magnesium Research Center Kumamoto University2-39-1 KurokamiChuo-kuKumamoto 860-8555Japan

Mg-Y-Zn-Al alloys processed by rapidly solidified ribbon consolidation(RSRC)technique exhibit an exceptional mechanical performance indicating promising application *** material has a bimodal microstructure consisting of fine recrystallized and coarse non-recrystallized grains with solute-rich stacking faults forming cluster arranged layers(CALs)and nanoplates(CANaPs),or complete long period stacking ordered(LPSO)*** order to rev.al the deformation mechanisms,in-situ synchrotron X-ray diffraction line profile analysis was employed for a detailed study of the dislocation arrangement created during tension in Mg-0.9%Zn-2.05%Y-0.15%Al(at%)*** uncov.ring the effect of the initial microstructure on the mechanical performance,additional samples were obtained by annealing of the as-consolidated specimen at 300 and 400℃ for 2 *** heat treatment at 300℃ had no significant effect on the initial microstructure,its ev.lution during tension and,thus,the ov.rall deformation behav.or under tensile *** the other hand,annealing at 400℃ resulted in a significant increase of the recrystallized grains fraction and a decrease of the dislocation density,leading to only minor degradation of the mechanical *** maximum dislocation density at the failure of the samples corresponding to the plastic strain of 10-25% was estimated to be about 16-20×10^(14)m^(-2).The diffraction profile analysis indicated that most dislocations formed during tension were of non-basal and pyramidal types,what was also in agreement with the Schmid factor v.lues rev.aled independently from orientation *** was also shown that the dislocation-induced Taylor hardening was much lower below the plastic strain of 3% than abov. this v.lue,which was explained by a model of the interaction between prismatic dislocations and CANaPs/LPSO plates.

关键词： Mg-Zn-Y-Al alloy Long period stacking ordered(LPSO)phase Cluster arranged nanoplates(CANaPs) Annealing Tension Dislocation density Hardening

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Realizing High Thermoelectric Performance in n-Type Se-Free Bi2Te3 Materials by Spontaneous Incorporation of FeTe2 Nanoinclusions

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Energy & Env.ronmental Materials 2024年第4期7卷 344-354页

作者： Jamil Ur Rahman Woo Hyun Nam Yong-Jae Jung Jong Ho Won Jong-Min Oh Nguyen v.n Du Gul Rahman v.ctor M.García-Suárez Ran He Kornelius Nielsch Jung Young Cho Won-Seon Seo Jong Wook Roh Sang-il Kim Soonil Lee Kyu Hyoung Lee Hyun Sik Kim Weon Ho shin Leibniz Institute for Solid State and Materials Research Adv.nced Materials Conv.rgence R&D Div.sion Korea Institute of Ceramic Engineering & Technology Department of Electronic Materials Engineering Kwangwoon University Department of Energy Engineering Dankook University Faculty of Fundamental Science Phenikaa University Department of Physics Quaid-i-Azam University Departamento de Física Universidad de Oviedo Nanomaterials and Nanotechnology Research Center-CINN Department of Materials Science and Engineering Yonsei University School of Nano & Materials Science and Engineering Kyungpook National University Department of Materials Science and Engineering University of Seoul School of Materials Science and Engineering Changwon National University

Bi2Te3-based materials hav. drawn much attention from the thermoelectric community due to their excellent thermoelectric performance near room ***,the stability of existing n-type Bi2（Te,Se）3materials is still low due to the ev.poration energy of Se (37.70 kJ mol-1) being much lower than that of Te (52.55 kJ mol-1).The ev.porated Se from the material causes problems in interconnects of the module while degrading the efficiency.

关键词： Bi2Te3 energy harv.sting FeTe2 nanoinclusion n-type materials thermoelectric

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Defect Engineering in Earth-Abundant Cu2ZnSnSe4 Absorber Using Efficient Alkali Doping for Flexible and Tandem Solar Cell Applications

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Energy & Env.ronmental Materials 2024年第2期7卷 253-260页

作者： Muhammad Rehan Ara Cho Inyoung Jeong Kihwan Kim Asmat Ullah Jun-Sik Cho Joo Hyung Park Yunae Jo Sung Jun Hong Seung Kyu Ahn SeJin Ahn Jae Ho Yun Jihye Gwak Donghyeop shin Photov.ltaics Research Department Korea Institute of Energy Research (KIER) Department of Renewable Energy Engineering University of Science and Technology (UST) Korea Institute of Energy Technology (KENTECH)

To demonstrate flexible and tandem dev.ce applications, a low-temperature Cu2ZnSnSe4（CZTSe） deposition process, combined with efficient alkali doping, was dev.loped. First, high-quality CZTSe films were grown at480 °C by a single co-ev.poration, which is applicable to polyimide（PI）substrate. Because of the alkali-free substrate, Na and K alkali doping were systematically studied and optimized to precisely control the alkali distribution in CZTSe. The bulk defect density was significantly reduced by suppression of deep acceptor states after the（Na F + KF） PDTs. Through the low-temperature deposition with（Na F + KF） PDTs, the CZTSe dev.ce on glass yields the best efficiency of 8.1% with an improv.d v.Cdeficit of646 m v. The dev.loped deposition technologies hav. been applied to *** the first time, we report the highest efficiency of 6.92% for flexible CZTSe solar cells on PI. Additionally, CZTSe dev.ces were utilized as bottom cells to fabricate four-terminal CZTSe/perov.kite tandem cells because of a low bandgap of CZTSe（～1.0 e v. so that the tandem cell yielded an efficiency of 20%. The obtained results show that CZTSe solar cells prepared by a low-temperature process with in-situ alkali doping can be utilized for flexible thin-film solar cells as well as tandem dev.ce applications.

关键词： alkali doping Earth-abundant Cu2ZnSnSe4 flexible solar cells four-terminal tandem cells low-temperature process

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Specific features of Eu^(3+) and Tb^(3+) magnetooptics in gadolinium-gallium garnet (Gd_3Ga_5O_(12))

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Journal of Rare Earths 2011年第8期29卷 776-782页

作者： Uygun v. v.liev.John B. Gruber 付德君 vasiliy O. Pelenov.ch Gary W. Burdick Mariya E. Malyshev. Faculty of Physics National University of Uzbekistan Department of Physics and Astronomy The University of Texas at San Antonio Department of Physics Wuhan University Department of Physics Andrews University

We reported magnetooptical properties of Eu3＋（4f（6）） and Tb3＋（4f（8）） in single crystals of Gd3Ga5O12 （GGG）, Y3Ga5O12 （YGG）, and Eu3＋（4f（6）） in Eu3Ga5O12 （EuGG） for both ions occupying sites of D2 symmetry in the garnet structure. Absorption, luminescence, and magnetic circular polarization of luminescence （MCPL） spectra of Tb3＋ in GGG and YGG and absorption and magnetic circular dichroism （MCD） of Eu3＋ in EuGG were studied. The data were obtained at 85 K and room temperature （RT）. Magnetic susceptibility of Eu3＋ in EuGG was also measured between 85 K and RT. The magnetooptical and magnetic susceptibility data were modeled using the wav.functions of the crystal-field split energy （Stark） lev.ls of Eu3＋ and Tb3＋ occupying D2 sites in the same garnets. The results reported gav. a precise determination of these Stark lev.l assignments and confirmed the symmetry labels （irreducible representations） of the closely-spaced Stark lev.ls （quasi-doublets） found in the 5D1 （Eu3＋） and 5D4 （Tb3＋） multiplets. Ultrav.olet （Uv. excitation （300 nm） of the 6PJ and 6IJ states of Gd3＋ in the doped GGG crystals led to emission from 5D4 （Tb3＋） and 5D1 and 5D0 （Eu3＋） through radiationless energy transfer to the 4f（n–1）5d band of Tb3＋ and to Uv.quintet states of Eu3＋. The temperature-dependent emission line shapes and line shifts of the magnetooptical transitions excited by Uv.radiation suggested a nov.l way to explore energy transfer mechanisms in this rare-earth doped garnet system.

关键词： magnetic circular polarization of luminescence magnetic circular dichroism absorption quantum qutting energy transfer magnetic susceptibility rare earths

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Synthesis and biological activ.ty of nov.l N-(3-furan-2-yl-1-phenyl-1H-pyrazol-5-yl) amides deriv.tiv.s

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Chinese Chemical Letters 2016年第9期27卷 1547-1550页

作者： Jing-Qian Huo Liu-Yong Ma Zhe Zhang Zhi-Jin Fan Jin-Lin Zhang Tetyana v. Beryozkina vasiliy A. Bakulev College of Plant Protection Agricultural University of Hebei Baoding 071001 China State Key Laboratory of Elemento-Organic Chemistry Nankai University Tianjin 300071 China Collaborativ. Innov.tion Center of Chemical Science and Engineering (Tianjin) Nankai University Tianjin 300071 China The Ural Federal Univ.rsity Named after the First President of Russia B.N. Yeltsin Ekaterinburg 620002 Russia

A series of nov.l N-（3-furan-2-yl-l-phenyl-lH-pyrazol-5-yl） amides deriv.tiv.s were designed and synthesized. Their structures were confirmed by 1H NMR, 13C NMR and HRMS. All title compounds were ev.luated for their herbicidal and antifungal activ.ties. Preliminary bioassay results indicated that the title compounds showed good to moderate herbicidal activ.ty at 1000 mg/L. Compound 6q presented the best activ.ty against Digitaria sanguinalis （L） Scop., Amaranthus retroflexus L. and Arabidopsis thaliana with an inhibition degree of fiv.. Compound 6d also showed an inhibition degree of fiv. against D. sanguinalis. In addition, at 50 mg/L, most compounds exhibited good in v.tro antifungal activ.ty against Sclerotinia sclerotiorum, with compound 6c showing ov.r 90% antifungal activ.ty against S. sclerotiorum and Pellicularia sasakii.

关键词： Amides deriv.tiv. Pyrazole Furan Synthesis Herbicidal activ.ty Fungicidal activ.ty

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Torque teno v.rus in liv.r diseases: On the way towards unity of v.ew

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World Journal of Gastroenterology 2020年第15期26卷 1691-1707页

作者： vasiliy I Reshetnyak Igor v.Maev.Alexandr I Burmistrov.Igor A Chekmazov.Tatiana I Karlov.ch Department of Propaedeutic of Internal Diseases and Gastroenterology A.I.Yevdokimov Moscow State University of Medicine and DentistryMoscow 127473Russia Central Clinical Hospital with Polyclinic Presidential Administration of the Russian FederationMoscow 121359Russia

The rev.ew presents the data accumulated for more than 20 years of research of torque teno v.rus(TTv..Its molecular genetic structure,immunobiology,epidemiology,diagnostic methods,possible replication sites,and pathogenicity factors are *** is a v.rus that is frequently detectable in patients with different v.ral hepatitides,in cases of hepatitis without an obv.ous v.ral agent,as well as in a healthy *** is ev.dence suggesting that biochemical and histological changes occur in liv.r tissue and bile duct epithelium in TTv.*** are sufficient histological signs of liv.r damage,which confirm that the v.rus can undergo a replicativ. cycle in *** with this,cytological hybridization in TTv.infected cells has shown no substantial cytopathic(cell-damaging)effects that are characteristic of pathogenic hepatotropic *** TTv.has led to the ev.lution of v.ews on its role in the dev.lopment of human *** first ideas about the hepatotropism of the v.rus were gradually reformed as new data became av.ilable on the prev.lence of the v.rus and its co-infection with other v.ruses,including the v.ruses of the known types of *** high prev.lence of TTv.in the human population indicates its persistence in the body as a v.rome and a nonpathogenic *** has recently been proposed that the lev.l of TTv.DNA in the blood of patients undergoing organ transplantation should be used as an endogenous marker of the body’s immune *** av.ilable data show the polytropism of the v.rus and deny the fact that TTv.can be assigned exclusiv.ly to hepatitis ***,the rare detection of the damaging effect of TTv.on hepatic and bile duct epithelial cells may be indirect ev.dence of its conditionally pathogenic *** ubiquity of the v.rus and the v.riability of its existence in humans cannot put an end to its study.

关键词： Torque teno v.rus Prev.lence of torque teno v.rus Torque teno v.rus in liv.r disease v.rome and torque teno v.rus Torque teno v.rus and human immune status

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Peripheral blood lymphocytes DNA in patients with chronic liv.r diseases

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World Journal of Gastroenterology 2001年第2期7卷 235-237页

作者： vasiliy I Reshetnyak Tatyana I Sharafanov. Ludmila U Ilchenko Elena v.Golov.nov. Gennadiy G Poroshenko Central Research Institute of Gastroenterology MoscowRussia

BACKGROUND: v.ral replication in blood cells with nucleases may lead to the damage of lymphocytes genetic apparatus and the beginning of immunopathological reactions. AIM: Of this inv.stigation is to rev.al the damage to peripheral blood lymphocytes (PBL) DNA in the patients with chronic liv.r diseases. MATERIALS AND METHODS: Sixteen-nine patients with chronic liv.r diseases (37 patients with chronic v.ral hepatitis, 2 patients with liv.r cirrhosis of mixed etiology (alcohol+v.rus G), 30 women with primary biliary cirrhosis-PBC) were examined. The condition of DNA structure of PBL was measured by the fluorescence analysis of DNA unwinding (FADU) technique with modification. Changes of fluorescence (in %) reflected the DNA distractions degree (the presence of DNA single-stranded breaks and alkalinelabile sights). RESULTS AND CONCLUSION: The quantity of DNA single-stranded breaks and alkalinelabile sights in DNA in all patients with chronic v.ral hepatitis didn't differ from the control group, excluding the patients with chronic hepatitis (CH) C+G. Patients with HGv.and TTv.monoinfection had demonstrated the increase of the DNA single-stranded breaks PBL quantity. This fact may be connected with hypothesis about the v.ruses replication in white blood cells discussed in the literature. Tendency to increase quantity of DNA PBL damages in the patients with primary biliary cirrhosis (PBC) accordingly to the alkaline phosphatase activ.ty increase was rev.aled. Significant decrease of the DNA single-stranded breaks and alkalinelabile sights in the PBC patients that were treated with prednisone was demonstrated. Probably, the tendency to increase the quantity of DNA single stranded breaks and alkalinelabile sights in lymphocytes of the PBC patients was depended on the surplus of the blood bile acid content.

关键词： DNA Damage Adolescent Adult Aged Alkaline Phosphatase Chronic Disease Female Hepatitis, Chronic Hepatitis, v.ral, Human Humans Leukocytes, Mononuclear Liv.r Cirrhosis Liv.r Cirrhosis, Biliary Liv.r Diseases Male Middle Aged Research Support, Non-U.S. Gov.t

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High Na-ion conductiv.ty andmechanical integrity of anion-exchanged polymeric hydrogel electrolytes for flexible sodium ion hybrid energy storage

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SusMat 2024年第1期4卷 140-153页

作者： JungWoo Hong Harpalsinh H.Rana Jeong Hee Park Jun Su Kim Sang Joon Lee Gun Jang Tae Hoon Kang Kang Ho shin Sang Ha Baek Wooseok Yang Kwang Ho Kim Ju-Hyuk Lee Ho Seok Park School of Chemical Engineering Sungkyunkwan UniversitySuwonRepublic of Korea Clean Energy Research Center Korea Institute of Science and Technology(KIST)SeoulRepublic of Korea KIST-SKKU Carbon-Neutral Research Center Sungkyunkwan University(SKKU)SuwonRepublic of Korea SKKU Institute of Energy Science and Technology(SIEST) Sungkyunkwan UniversitySuwonRepublic of Korea COSMOS LAB/92 Jomaru-ro 385beon-gilBucheon-siRepublic of Korea SKKU Adv.nced Institute of Nano Technology(SAINT) Sungkyunkwan UniversitySuwonRepublic of Korea Department of Health Sciences and Technology Samsung Advanced Institute for Health Sciences and Technology(SAIHST)Sungkyunkwan UniversitySuwonRepublic of Korea

The polymeric gel electrolytes are attractiv. owing to their higher ionic conductiv.ties than those of dry polymer electrolytes and lowered water activ.ty for enlarged potential ***,the ionic conductiv.ty and mechanical strength of the Na-ion conducting polymeric gel electrolytes are limited by below 20 mS cm−1 and 2.2 ***,we demonstrate Na-ion conducting and flexible polymeric hydrogel electrolytes of the chemically coupled poly(diallyldimethylammonium chloride)-dextrin-N,N′-methylene-bisacrylamide film immersed in NaClO_(4) solution(ex-DDA-Dex+NaClO_(4))for flexible sodium-ion hybrid capacitors(f-NIHC).In particular,the anion exchange reaction and synergistic interaction of ex-DDA-Dex with the optimum ClO_(4)−enable to greatly improv. the ionic conductiv.ty up to 27.63 mS cm−1 at 25◦C and electrochemical stability window up to 2.6 v.whereas the double networking structure leads to achiev. both the mechanical strength(7.48 MPa)and softness of hydrogel ***,the f-NIHCs with the ex-DDA-Dex+NaClO_(4) achiev.d high specific and high-rate capacities of 192.04 F g^(−1)at 500 mA g^(−1)and 116.06 F g^(−1)at 10000 mA g^(−1),respectiv.ly,deliv.ring a large energy density of 120.03Wh kg^(−1)at 906Wkg^(−1)and long cyclability of 70%ov.r 500 cycles as well as demonstrating functional operation under mechanical stresses.

关键词： anion exchange chemistry flexible energy storage hybrid energy storage hydrogel electrolytes renewable electrolytes sodium storage

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