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Phase evolution and relaxor to ferroelectric phase transition boosting ultrahigh electrostrains in (1-x)(Bi_(1/2)Na_(1/2))TiO_(3)-x(Bi_(1/2)K_(1/2))TiO_(3) solid solutions

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Journal of Materiomics 2022年第2期8卷 335-346页

作者： Ruiyi Jing Leiyang Zhang Qingyuan Hu DOAlikin vya shur Xiaoyong Wei Lin Zhang Gang Liu Haibo Zhang Li Jin Electronic Materials Research Laboratory Key Laboratory of the Ministry of Education&International Center for Dielectric ResearchSchool of Electronic Science and EngineeringFaculty of Electronic and Information EngineeringXi'an Jiaotong UniversityXi'an710049China School of Natural Sciences and Mathematics Ural Federal UniversityEkaterinburg620000Russia MIT Media Lab Massachusetts Institute of TechnologyCambridgeMA02139USA School of Materials and Energy Southwest UniversityChongqing400715China School of Materials Science and Engineering State Key Laboratory of Material Processing and Die&Mould TechnologyHuazhong University of Science and TechnologyWuhan430074China

Owing to the complex composition architecture of these solid solutions,some fundamental issues of the classical(1-x)(Bi_(1/2)Na_(1/2))TiO_(3) -x(Bi_(1/2)K_(1/2))TiO_(3)(BNT-xBKT)binary system,such as details of phase evolution and optimal Na/K ratio associated with the highest strain responses,remain unresolved.In this work,we systematically investigated the phase evolution of the BNT-xBKT binary solid solution with x ranging from 0.12 to 0.24 using not only routine X-ray diffraction and weak-signal dielectric characterization,but also temperature-dependent polarization versus electric field(P-E)and current versus electric field(I-E)curves.Our results indicate an optimal Na/K ratio of 81/19 based on high-field polarization and elec-trostrain characterizations.As the temperature increased above 100?C,the x¼0.19 composition pro-duces ultrahigh electrostrains(>0.5%)with high thermal stability.The ultrahigh and stable electrostrains were primarily due to the combined effect of electric-field-induced relaxor-to-ferroelectric phase tran-sition and ferroelectric-to-relaxor diffuse phase transition during heating.More specifically,we revealed the relationship between phase evolution and electrostrain responses based on the characteristic tem-peratures determined by both weak-field dielectric and high-field ferroelectric/electromechanical property characterizations.This work not only clarifies the phase evolution in BNT-xBKT binary solid solution,but also paves the way for future strain enhancement through doping strategies.

关键词： Phase evolution BNT BKT Electrostrain Relaxor ferroelectric Phase diagram

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Enhanced antiferroelectric-like relaxor ferroelectric characteristic boosting energy storage performance of(Bi_(0.5)Na_(0.5))TiO_(3)-based ceramics via defect engineering

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Journal of Materiomics 2022年第3期8卷 527-536页

作者： Leiyang Zhang Ruiyi Jing Yunyao Huang Qingyuan Hu DOAlikin vya shur Jinghui Gao Xiaoyong Wei Ling Zhang Gang Liu Yan Yan Li Jin Electronic Materials Research Laboratory Key Laboratory of the Ministry of Education&International Center for Dielectric ResearchSchool of Electronic Science and EngineeringXi'an Jiaotong UniversityXi'an710049China School of Natural Sciences and Mathematics Ural Federal UniversityEkaterinburg620000Russia State Key Laboratory of Electrical Insulation and Power Equipment School of Electrical EngineeringXi'an Jiaotong UniversityXi'an710049China Chengdu Hongke Electronic Technology Co. LtdChengdu610100China School of Materials and Energy Southwest UniversityChongqing400715China

3Lead-free(BiasNaus)TiO_(3)(BNT)-based relaxor ferroelectric(RFE)ceramics have attracted a lot of atten-tion due to their high power density and rapid charge-discharge apabilities,as well as their potential application in pulse power capacitors.However,because of the desire for smaller electronic devices,their energy storage performance(ESP)should be enhanced even further.We describe a defect engineering strategy for enhancing the antiferroelectric-like RFE feature of BNT-based ceramics by unequal substi-tution of rare-earth La^(3+)in this paper.The ESP of La^(3+)-doped samples is raised by 25%with the same synthetic procedure and thidkness,due to an inrease in the critical electric field(E-field)and saturated E-field during polarization response,which is induced by a modifiation in the energy barrier between the lattice torsion.More impressively,an ultrahigh recoverable energy storage density Wrec of 8.58J/cm^(3)and a high energy storage efficiengyηof 945%are simultaneously attained in 3 at.%La^(3+)-substituted 0.6(Bi_(0.5)Na_(0.4)K_(0.1))_(1-1.5x)La_(x)TiO_(3)-0.4[2/3SrTiO_(3)-1/3Bi(Mg_(2/3)Ni_(1/3))O_(3)]RFE ceamics with good temperatue stability(W_(rec)=4.6±0.2 J/cm^(3)and higher n of 290%from 30℃to 120℃),frequency stability,and fatigue resistance.The significant inrease in ESP achieved through defect engineering not only proves the effectiveness of our strategy,but also presents a novel dielectric material with potential applications in pulse power apacitors.

关键词： BNT Energy storage performance Relaxor ferroelectric Antiferroelectric-like

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Superior piezoelectric performance with high operating temperature in bismuth ferrite-based ternary ceramics

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Journal of Materials Science & Technology 2024年第2期169卷 172-181页

作者： Yunyao Huang Leiyang Zhang Ruiyi Jing Yang Yang Vladimir shur Xiaoyong Wei Li Jin Electronic Materials Research Laboratory Key Laboratory of the Ministry of EducationSchool of Electronic Science and EngineeringXi’an Jiaotong UniversityXi’an 710049China Faculty of Materials and Manufacturing Key Laboratory of Advanced Functional MaterialsEducation Ministry of ChinaBeijing University of TechnologyBeijing 100124China School of Natural Sciences and Mathematics Ural Federal UniversityEkaterinburg620000Russia

Due to the thermal depolarization effect,adequate piezoelectric performance with high operating temperature is regarded to be challenging to accomplish concurrently in piezoceramics for applications in specific piezoelectric devices.In this work,we synthesized(0.8−x)BiFeO_(3)-x PbTi_(3)-0.2Ba(Zr_(0.25)Ti_(0.75))O_(3)(abbreviated as BFO-x PT-BZT)ternary solid solutions with 0.15≤x≤0.30 by conventional solid-state reaction method.The MPB composition with a coexisting state of rhombohedral-tetragonal phases exhibits enhanced electromechanical properties,including Curie temperature of 380℃,large-signal equivalent piezoelectric coefficient d^(∗)_(33)of 395 pm V^(-1),small-signal piezoelectric coefficient d_(33)of 302 pC N^(-1),and electromechanical coupling factor k_(p)of 50.2%,which is comparable to commercial PZT-5A ceramics,indicating potential in high-temperature applications.Furthermore,in-situ X-ray diffraction(XRD)and piezoelectric force microscopic(PFM)techniques demonstrate that multiphase coexistence and complex nanodomains promote piezoelectric response via synergism.The x=0.24 composition exhibits the highest in-situ d_(33)of 577 pC N^(-1)and good temperature stability in 30−280℃,indicating that BZT-modified BFO-PT ceramics are promising candidates for high-temperature piezoelectric devices.

关键词： High-temperature piezoelectrics Morphotropic phase boundary In-situ technique Domain structure BFO

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Moderate Fields, Maximum Potential: Achieving High Records with Temperature‑Stable Energy Storage in Lead‑Free BNT‑Based Ceramics

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Nano-Micro Letters 2024年第5期16卷 184-200页

作者： Wenjing Shi Leiyang Zhang Ruiyi Jing Yunyao Huang Fukang Chen Vladimir shur Xiaoyong Wei Gang Liu Hongliang Du Li Jin Electronic Materials Research Laboratory Key Laboratory of the Ministry of EducationSchool of Electronic Science and EngineeringXi’an Jiaotong UniversityXi’an 710049People’s Republic of China School of Materials and Energy Southwest UniversityChongqing 400715People’s Republic of China School of Natural Sciences and Mathematics Ural Federal UniversityEkaterinburg 620000Russia Multifunctional Electronic Ceramics Laboratory College of EngineeringXi’an International UniversityXi’an 710077People’s Republic of China

The increasing awareness of environmental concerns has prompted a surge in the exploration of leadfree,high-power ceramic capacitors.Ongoing efforts to develop leadfree dielectric ceramics with exceptional energystorage performance(ESP)have predominantly relied on multicomponent composite strategies,often accomplished under ultrahigh electric fields.However,this approach poses challenges in insulation and system downsizing due to the necessary working voltage under such conditions.Despite extensive study,bulk ceramics of(Bi_(0.5)Na_(0.5))TiO_(3)(BNT),a prominent lead-free dielectric ceramic family,have seldom achieved a recoverable energy-storage(ES)density(Wrec)exceeding 7 J cm^(−3).This study introduces a novel approach to attain ceramic capacitors with high ESP under moderate electric fields by regulating permittivity based on a linear dielectric model,enhancing insulation quality,and engineering domain structures through chemical formula optimization.The incorporation of SrTiO_(3)(ST)into the BNT matrix is revealed to reduce the dielectric constant,while the addition of Bi(Mg_(2/3)Nb_(1/3))O_(3)(BMN)aids in maintaining polarization.Additionally,the study elucidates the methodology to achieve high ESP at moderate electric fields ranging from 300 to 500 kV cm^(−1).In our optimized composition,0.5(Bi_(0.5)Na_(0.4)K_(0.1))TiO_(3)–0.5(2/3ST-1/3BMN)(B-0.5SB)ceramics,we achieved a Wrec of 7.19 J cm^(−3) with an efficiency of 93.8%at 460 kV cm^(−1).Impressively,the B-0.5SB ceramics exhibit remarkable thermal stability between 30 and 140℃ under 365 kV cm^(−1),maintaining a Wrec exceeding 5 J cm^(−3).This study not only establishes the B-0.5SB ceramics as promising candidates for ES materials but also demonstrates the feasibility of optimizing ESP by modifying the dielectric constant under specific electric field conditions.Simultaneously,it provides valuable insights for the future design of ceramic capacitors with high ESP under constraints of limited electric field.

关键词： BNT Energy storage Lead-free Relaxor ferroelectrics Capacitors

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Improved energy storage performance of bismuth sodium titanate-based lead-free relaxor ferroelectric ceramics via Bi-containing complex ions doping

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Rare Metals 2023年第5期42卷 1472-1482页

作者： Wen-Jing Shi Lei-Yang Zhang Yu-Le Yang D.O.Alikin V.Ya.shur Xiao-Yong Wei Hong-Liang Du Li Jin Electronic Materials Research Laboratory Key Laboratory of the Ministry of Education and International Center for Dielectric ResearchSchool of Electronic Science and EngineeringXi’an Jiaotong UniversityXi’an710049China School of Natural Sciences and Mathematics Ural Federal UniversityEkaterinburg620000Russia Multifunctional Electronic Ceramics Laboratory College of EngineeringXi’an International UniversityXi’an710077China

Lead-free dielectric ceramics can be used to make quick charge-discharge capacitor devices due to their high power density.Their use in advanced electronic systems,however,has been hampered by their poor energy storage performance(ESP),which includes low energy storage efficiency and recoverable energy storage density(Wrec).In this work,we adopted a combinatorial optimization strategy to improve the ESP in(Bi_(0.5)Na_(0.5))TiO_(3)(BNT)-based relaxor ferroelectric ceramics.To begin,the Bi-containing complex ions Bi(Mg_(2/3)Nb_(1/3))O_(3)(BMN)were introduced into a BNT-based matrix in order to improve the diffuse phase transition,increase Bi-O bond coupling,avoid macro domain development,and limit polarization response hysteresis.Second,the viscous polymer process was employed to reduce sample thickness and porosity,resulting in an apparent increase in breakdown strength in(1-x)[0.7(Bi_(1/2)Na_(1/2))TiO_(3)]-0.3SrTiO_(3)-xBi(Mg_(2/3)Nb_(1/3))O_(3)(BS-xBMN)ceramics.Finally,in x=0.20 composition,an amazing Wrecof 5.62 J·cm^(-3)and an ultra-high efficiency of 91.4%were simultaneously achieved at a relatively low field of 330 kV·cm^(-1),together with remarkable temperature stability in the temperature range of 30-140℃(3.5 J·cm^(-3)±5%variation).This research presents a new lead-free dielectric material with superior ESP for use in pulsed power capacitors.

关键词： Relaxor ferroelectric Energy storage performance(ESP) Viscous polymer process (Bi_(0.5)Na_(0.5))TiO_(3)(BNT)

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Ultra-slim electrostrains with superior temperature-stability in leadfree sodium niobate-based ferroelectric perovskite

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Journal of Materiomics 2022年第6期8卷 1230-1238页

作者： Ruiyi Jing Qingyuan Hu Leiyang Zhang Yuan Sun Jiagang Wu D.O.Alikin V.Ya shur Xiaoyong Wei Hongliang Du Yunfei Chang Li Jin Electronic Materials Research Laboratory Key Laboratory of the Ministry of Education&International Center for Dielectric ResearchSchool of Electronic Science and EngineeringXi'an Jiaotong UniversityXi'an710049China Functional Materials and Acousto-Optic Instruments Institute School of Instrumentation Science and EngineeringHarbin Institute of TechnologyHarbin150080China Department of Materials Science Sichuan UniversityChengdu610065China School of Natural Sciences and Mathematics Ural Federal UniversityEkaterinburg620000Russia Multifunctional Electronic Ceramics Laboratory College of EngineeringXi'an International UniversityXi'an710077China

Large electrostrains with high temperature stability and low hysteresis are essential for applications in high-precision actuator devices.However,achieving simultaneously all three of the aforementioned features in ferroelectric ceramics remains a considerable challenge.In this work,we firstly report a high unipolar electrostrain(0.12%at 60 kV/cm)in(1ex)NaNbO_(3)-x[(Ba0.85Ca0.15)(Zr_(0.1)Ti_(0.9))O_(3)](NN-xBCZT)ferroelectric polycrystalline ceramics with excellent thermal stability(variation less than 10%in the temperature range of 30-160℃)and ultra-low hysteresis(<6%).Secondly,the high-field electrostrain response is dominated by the intrinsic electrostrictive effect,which may account for more than 80%of the electrostrain.Furthermore,due to the thermal stability of the polarization in the pure tetragonal phase,the large electrostrain demonstrates extraordinarily high stability from room temperature to 140℃.Finally,in-situ piezoelectric force microscopy reveals ultra-highly stable domain structures,which also guarantee the thermal stability of the electrostrain in(NN-xBCZT ferroelectrics ceramics.This study not only clarifies the origin of thermally stable electrostrain in NN-xBCZT ferroelectric perovskite in terms of electrostrictive effect,but also provides ideas for developing applicable ferroelectric ceramic materials used in actuator devices with excellent thermal stability.

关键词： Electrostrain Electrostriction NaNbO_(3) Polarization

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Ferroelectric-to-relaxor transition and ultrahigh electrostrictive effect in Sm^(3+)-doped Pb(Mg_(1/3)Nb_(2/3))O_(3)-PbTiO_(3)ferroelectrics ceramics

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Journal of Materials Science & Technology 2023年第34期165卷 75-84页

作者： Yunyao Huang Leiyang Zhang Wenjing Shi Qingyuan Hu Vladimir shur Xiaoyong Wei Li Jin Electronic Materials Research Laboratory Key Laboratory of the Ministry of EducationSchool of Electronic Science and EngineeringXi’an Jiaotong UniversityXi’an 710049China School of Natural Sciences and Mathematics Ural Federal UniversityEkaterinburg 620000Russia

Rare-earth Sm^(3+)-doped Pb(Mg_(1/3)Nb_(2/3))O_(3)-0.25PbTiO_(3)(PMN-0.25PT)ferroelectric ceramics with doping amounts between 0%-3%were developed via a conventional solid-state method.The doping effect of Sm^(3+)ions on the PMN-0.25PT matrix was systematically investigated on the basis of the phase structure,temperature-dependent dielectric,ferroelectric,and electrotechnical properties.Due to the disruption of long-range ferroelectric order,the addition of Sm^(3+)ions effectively lowers the Tm(temperature corresponding to maximum permittivity)of the samples,leading to enhanced relaxor ferroelectric(RFE)characteristic and superior electric field-induced strain(electrostrain)properties at room temperature.Intriguingly,a considerable large-signal equivalent piezoelectric coefficient d∗_(33)of 2376 pm/V and a very small hysteresis were attained in the PMN-0.25PT component doped with 2.5 mol.%Sm^(3+).The findings of piezoelectric force microscopy indicate that the addition of Sm^(3+)increases the local structural heterogeneity of the PMN-0.25PT matrix and that the enhanced electromechanical performance is due to the dynamic behavior of polar nanoregions.Importantly,strong temperature-dependent electrostrain and electrostrictive coefficient Q33 are observed in the critical region around Tm in all Sm^(3+)-modified PMN-0.25PT ceramic samples studied.This work elucidates the phase transition behavior of Sm^(3+)-doped PMN-0.25PT and reveals a critical region where electrostrictive properties can be greatly improved due to a strong temperature-dependent characteristic.

关键词： PMN-PT ceramics Sm^(3+)doping,Equivalent piezoelectric coefficient,Local structural heterogeneity,Electrostrictive effect

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Boosting the piezoelectric property of relaxor ferroelectric single crystal via active manipulation of defect dipole polarization

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Journal of Materiomics 2023年第1期9卷 166-173页

作者： Qingyuan Hu Huimin Liao Xin Liu Li Jin Kexin Song Yongyong Zhuang Zhuo Xu Vladimir Ya shur Xiaoyong Wei Electronic Materials Research Laboratory Key Laboratory of the Ministry of Education&International Center for Dielectric ResearchSchool of Electronic ImformationXi'an Jiaotong UniversityXi'an710049China School of Natural Sciences and Mathematics Ural Federal UniversityEkaterinburg620000Russia

To further enhance the property of piezoelectric materials is of great significance to improve the overall performance of electro-mechanical devices.Here in this work,we propose a thermal annealing and high temperature poling approach to achieve significantly enhanced piezoelectricity in Pb(In_(1/2)Nb_(1/2))O_(3)single bondPb(Mg_(1/3)Nb_(2/3))O_(3)single bondPbTiO_(3)(PIN-PMN-PT)crystals with a morphotropic phase boundary(MPB)composition.The main idea of our approach is to realize a more sufficiently polarized crystal via active manipulation of defects and orientation of defect polarization.Manipulation of defect dipoles by the high temperature poling is proved by the piezo-response force microscopy.Finally,a d_(33)of 3300 pC/N and a SE of 0.25%are obtained,nearly 60%higher than that of conventionally poled crystals.Moreover,such a boosting of piezoelectric property is obtained under a maintained Curie temperature.Our research not only reveals the active control of defect dipole via modified poling method in the PIN-PMN-PT crystal,but also provides a feasible strategy to further improve the property of piezoelectric materials.

关键词： Piezoelectric property Relaxor ferroelectric single crystals Defects Defect polarization

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Creation of periodical domain structure by local polarization reversal in planar waveguide produced by soft proton exchange in LiNbO_(3)

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Journal of Advanced Dielectrics 2023年第6期13卷 39-44页

作者： Evgeniy Savelyev Andrey Akhmatkhanov Boris Slautin Herve Tronche Florent Doutre Tommaso Lunghi Pascal Baldi Vladimir shur Institute of Natural Sciences and Mathematics Ural Federal University 620002 EkaterinburgRussia Institut de Physique de Nice Universite Cote d’AzurCNRS06108 Nice Cedex 2France

The paper presents the results of an experimental study of the local polarization reversal and creation of domains by a biased tip of scanning probe microscope(SPM)in lithium niobate single crystals of congruent composition with a surface layer modified by soft proton exchange(SPE).The depth dependence of Ht ions concentration in the SPE-modified layer measured by confocal Raman microscopy demonstrates a sufficient composition gradient.The creation of isolated domains and stripe domain structures has been done by two switching modes:(1)point switching by field application in separated points and(2)line scanning switching by motion of the biased tip being in contact with the sample surface.For point switching for pulse durations less than 10 s,the logarithmic dependence of the domain diameter on the pulse duration was observed.The change of the dependence to a linear one for pulse duration above 10 s has been attributed to the transition from the stochastic step generation at the domain wall to the deterministic one at the domain vertexes.The periodical structure of stripe domains was created in SPE CLN planar waveguides by scanning at elevated temperature.The revealed switching regime suppresses electrostatic interaction of neighboring domains and leads to a significant improvement of the domain structure regularity.The creation of the stable periodical domain structure with submicron periods in SPE CLN planar waveguides was demonstrated.

关键词： Scanning probe microscopy piezoelectric force microscopy periodical poling composition gradient

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Formation of self-assembled nanodomain structures in single crystals of uniaxial ferroelectrics lithium niobate, lithium tantalate and strontium–barium niobate

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Journal of Advanced Dielectrics 2014年第1期4卷 87-94页

作者： V.Ya.shur V.A.Shikhova P.S.Zelenovskiy D.V.Pelegov L.I.Ivleva J.Dec Ferroelectric Laboratory Institute of Natural Sciences Ural Federal University51 Lenin Ave.Ekaterinburg 620000Russia General Physics Institute of the Russian Academy of Sciences 38 Vavilov Str. Moscow 119991Russia Institute of Materials Science University of Silesia4 Uniwersytecka Str.Katowice PL-40-007Poland

The formation and evolution of the self-assembled nanodomain structures during polarization reversal have been comparatively analyzed in single crystals of various uniaxial ferroelectrics:LiNbO_(3)(LN),LiTaO_(3)(LT)and Sr_(x)Ba_(1-x)Nb_(2)O_(6)(SBN).Several experimental methods have been used for visualization of the micro-and nanodomain patterns.The static domain images have been obtained by optical microscopy and piezoresponse force microscopy.The Raman confocal microscopy allowed us to obtain the domain images in the bulk.The equilibrium slow switching with effective screening resulted in growth of polygon-shaped microdomains:hexagons in LN,triangles in LT and squares in SBN,which corresponds to crystal symmetry.Switching in nonequilibrium conditions(noneffective screening of depolarization field)brings to appearance of similar nanodomain structures in all studied crystals as a result of different processes:(1)formation of nanodomain ensembles,(2)discrete switching,(3)incomplete merging and(4)spontaneous backswitching.

关键词： Nanodomain structures self-assembling lithium niobate lithium tantalate strontium-barium niobate.

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