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Highly Hydrolysis-Resistant Polyimide Fibers Prepared by Thermal Crosslinking with Inherent Carboxyl Groups

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Chinese Journal of Polymer Science 2024年第2期42卷 247-255,I0010页

作者： Can-Can Zhang Jun-Long Yang Ya-Jiang Huang Guang-Xian Li College of Polymer Science and Engineering State Key Laboratory of Polymer Materials Engineering of ChinaSichuan UniversityChengdu610065China

Easy hydrolysis in alkaline environments limits the use of polyimide fibers in environmental protection. The hydrolysis resistance levels of polyimide fibers can be improved by crosslinking of the macromolecular chains. In this work, crosslinked polyimide fibers(CPI fibers) were produced by intrinsic carboxyl decarboxylation for the first time. The thermal stability of the polyimide fibers containing the intrinsic carboxyl groups(PIC fibers) was studied, and the temperature of the decarboxylation-crosslinking reaction was determined to be 450 ℃. The PIC fibers were hotdrawn to initiate thermal crosslinking of the carboxyl groups and molecular chain orientation at high temperature. The CPI fibers had high tensile strengths(0.72-1.46 GPa) and compressive strengths(401-604 MPa). The oriented macromolecules and chemically crosslinked structure improved the tightness of the molecular chains and endowed the CPI fibers with excellent hydrolytic resistance. The CPI-50 fiber did not dissolve in a 0.5 wt% NaOH solution during heating at 90 ℃ for 10 h, and the tensile strength retention reached 87% when treated in 0.5 wt% NaOH solutions at 90 ℃ for 1 h, providing a guarantee for its application in alkaline corrosive environments.

关键词： Polyimide Carboxyl group Crosslinking Hydrolysis-resistance

燃气轮机中心分级燃烧器天然气掺氢燃烧的受迫振荡特性

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上海交通大学学报 2024年第3期58卷 304-311页

作者：史挺金明葛冰臧述升上海交通大学机械与动力工程学院上海200240

天然气掺氢燃烧是燃气轮机机组降低碳排放重要措施之一,但掺氢燃料的组分变化会导致燃烧室火焰结构及燃烧稳定性发生变化.为分析中心分级燃烧器掺氢燃烧条件下的燃烧不稳定性问题,通过试验研究了燃烧器入口速度扰动下,不同掺氢比对中心... 详细信息

天然气掺氢燃烧是燃气轮机机组降低碳排放重要措施之一,但掺氢燃料的组分变化会导致燃烧室火焰结构及燃烧稳定性发生变化.为分析中心分级燃烧器掺氢燃烧条件下的燃烧不稳定性问题,通过试验研究了燃烧器入口速度扰动下,不同掺氢比对中心分级掺氢燃烧的瞬态火焰结构、压力以及热释放响应的影响,并利用本征正交分解(POD)法提取了火焰脉动的特征模态,发现其主要包含火焰干涉区强脉动和轴向扰动两种模态.试验结果表明,随着掺氢体积比从0%增大到30%,火焰前沿向上游移动,两级火焰间距缩短,火焰干涉对应的脉动模态的能量占比增大,加强了压力与热释放的耦合,导致燃烧室内的压力响应增大9%,热释放响应增大37%.

关键词：中心分级燃烧器天然气掺氢受迫振荡本征正交分解

Effectiveness and safety of Jiawei Xiaoyao pill(加味逍遥丸)in the treatment of premenstrual syndrome(liver depression,spleen deficiency,and blood-heat syndrome):a multi-center,randomized,placebo-controlled trial

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Journal of Traditional Chinese Medicine 2024年第2期44卷 373-380页

作者： LI Xiyu YANG Yanhong SUN Jian NIE Quanfang LIU Lifen LI Guifen YU Junping ZHANG Zhuangjin XU Yi ZOU ting shi Yun Department of Gynecology Dongzhimen HospitalBeijing University of Chinese MedicineBeijing 100700China Department of Gynecology Luoyang 1st Hospital of TCMLuoyang 471099China Department of Gynecology Zaozhuang Hospital of TCMZaozhuang 277099China Department of Gynecology and Obstetrics Loudi Central HospitalLoudi 417099China Department of Gynecology and Obstetrics Yiyang 1st Hospital of TCMYiyang 413002China Department of Gynecology Harrison International Peace HospitalHengshui 053000China Department of Gynecology and Obstetrics Shanxi Fenyang HospitalFenyang 032299China Department of Gynecology and Obstetrics Hengyang Chinese Medicine HospitalHengyang 421001China Scientific Research Institute of Beijing Tongrentang Technology Development Co. Ltd.Beijing 100061China Female Reproductive and Health Medicine Research Committee of Chinese Traditional Medicine Association Beijing 100061China

OBJECTIVE:To investigate the effectiveness and safety of Jiawei Xiaoyao pill(加味逍遥丸,JXP)in the treatment of symptoms associated with premenstrual syndrome(PMS).METHODS:A total of 144 regularly menstruating women with PMS were recruited at 8 sites in China from August 2017 to December 2018,and randomized to receive either a JXP or a matching placebo(12 g/d,6 g twice a day)for 3 menstrual *** primary indicator was the reduced Daily Record of Severity of Problems(DRSP)scores in the luteal phase after 3 months of *** safety outcomes included clinical adverse events(AEs),adverse reactions(ARs),changes in vital signs,and laboratory ***:JXP surpassed the placebo in reducing DRSP scores(psychological/somatic dysfunction)in the luteal phase over 3 menstrual cycles of treatment(PFAS=0.002,PPPS=0.001).Additionally,there were no significant differences in the incidence of AEs,severe AEs,withdrawal due to AEs and ARs between the two groups(all P>0.05),and no clinically significant adverse medical events related to the test drug ***:JXP was superior to the placebo in relieving the symptoms associated with PMS,which signified that JXP may be effective,safe,and welltolerated as an alternative therapy.

关键词： premenstrual syndrome randomized controlled trial double-blind method Jiawei Xiaoyao pill

Transcutaneous electrical acupoint stimulation benefits postoperative pain relief of oocyte retrieval:A randomized controlled trial

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Journal of Integrative Medicine 2024年第1期22卷 32-38页

作者： Li-ying Liu Yang Su Rong-rong Wang Yuan-yuan Lai Lei Huang Yi-ting Li Xin-yue Tao Meng-hua Su Xiao-yan Zheng shi-chen Huang Yong-na Wu Si-yi Yu Fan-rong Liang Jie Yang Acupuncture and Tuina School Chengdu University of Traditional Chinese MedicineChengdu 610000Sichuan ProvinceChina Traditional Chinese Medicine Department Sichuan Jinxin Xi’nan Women's and Children's HospitalChengdu 610000Sichuan ProvinceChina

Background Transvaginal oocyte retrieval is frequently followed by adverse events related to anesthesia and the *** research showed that transcutaneous electrical acupoint stimulation(TEAS)can relieve intraoperative pain and postoperative *** This study examined whether TEAS can alleviate pain and relieve adverse symptoms after oocyte ***,setting,participants and interventions Altogether 128 patients were randomly divided into the TEAS group and the mock TEAS *** two groups received a 30-minute-long TEAS or mock TEAS treatment that began 30 min after oocyte *** outcome measures The primary outcome was the visual analog scale(VAS)pain *** outcomes were pressure pain threshold,McGill score,pain rating index(PRI),present pain intensity(PPI),VAS stress score,VAS anxiety score,and postoperative adverse *** The baseline characteristics of the two groups were comparable(P>0.05).The VAS pain scores of the TEAS group were lower than those of the mock TEAS group at 60 and 90 min after oocyte retrieval(P0.05).The TEAS group was superior to the mock TEAS group for relieving postoperative adverse symptoms(P<0.05).Conclusion TEAS treatment can relieve postoperative pain and postoperative adverse symptoms for patients undergoing oocyte retrieval.

关键词： Transcutaneous electrical acupoint stimulation Fertilization Embryo transfer Oocyte retrieval Pain Randomized controlled trial

Evolution of helium bubbles in FeCoNiCr-based high-entropy alloys containing γ′ nanoprecipitates

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Chinese Physics B 2024年第7期33卷 491-500页

作者：冯婷蒋胜明胡潇天张子骏黄子敬董士刚张建 College of Energy Xiamen UniversityXiamen 361005China16

A series of high-entropy alloys(HEAs) containing nanoprecipitates of varying sizes is successfully prepared by a non-consuming vacuum arc melting *** order to study the irradiation evolution of helium bubbles in the FeCoNiCrbased HE As with γ' precipitates,these samples are irradiated by 100-keV helium ions with a fluence of 5 × 10^(20) ions/m^(2) at 293 K and 673 K,*** the samples irradiated at room temperature are annealed at different temperatures to examine the diffusion behavior of helium *** electron microscope(TEM) is employed to characterize the structural morphology of precipitated nanoparticles and the evolution of helium *** results reveal that nanosized,spherical,dispersed,coherent,and ordered L1_(2)-type Ni_(3)Ti γ' precipitations are introduced into FeCoNiCr(Ni_(3)Ti)_(0.1) HEAs by means of ageing treatments at temperatures between 1073 K and 1123 *** the ageing treatment conditions adopted in this work,γ' nanoparticles are precipitated in FeCoNiCr(Ni_(3)Ti)_(0.1) HE As,with average diameters of 15.80 nm,37.09 nm,and 62.50 nm,*** average sizes of helium bubbles observed in samples after 673-K irradiation are 1.46 nm,1.65 nm,and 1.58 nm,*** improvement in the irradiation resistance of FeCoNiCr(Ni_(3)Ti)_(0.1) HEAs is evidenced by the diminution in bubbles ***,the FeCoNiCr(Ni_(3)Ti)_(0.1) HEAs containing γ' precipitates of 15.8 nm exhibits the minimum size and density of helium bubbles,which can be ascribed to the considerable helium trapping effects of heterogeneous coherent phase ***,annealing experiments conducted after 293-K irradiation indicate that HEAs containing precipitated phases exhibits smaller apparent activation energy(E_(a)) for helium bubbles,resulting in larger helium bubble *** study provides guidance for improving the irradiation resistance of L1_(2)-strengthened high-entropy alloy.

关键词： high-entropy alloys irradiation resistance coherent precipitates helium bubbles

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Dynamic intrauterine crosstalk promotes porcine embryo implantation during early pregnancy

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Science China(Life Sciences) 2024年第8期67卷 1676-1696页

作者： Xupeng Zang Shengchen Gu Wenjing Wang Junsong shi Jianyu Gan Qun Hu Chen Zhou Yue Ding Yanjuan He Lei Jiang ting Gu Zheng Xu Sixiu Huang Huaqiang Yang Fanming Meng Zicong Li Gengyuan Cai Linjun Hong Zhenfang Wu State Key Laboratory of Swine and Poultry Breeding Industry National Engineering Research Center for Breeding Swine IndustryCollege of Animal ScienceSouth China Agricultural UniversityGuangzhou 510642China Guangdong Provincial Key Laboratory of Agro-Animal Genomics and Molecular Breeding South China Agricultural UniversityGuangzhou 510642China Yunfu Subcenter of Guangdong Laboratory for Lingnan Modern Agriculture Yunfu 527300China Guangdong Key Laboratory of Animal Breeding and Nutrition Institute of Animal ScienceGuangdong Academy of Agricultural SciencesGuangzhou 510640China Key Laboratory of South China Modern Biological Seed Industry Ministry of Agriculture and Rural AffairsGuangzhou 510520China

Dynamic crosstalk between the embryo and mother is crucial during ***,we comprehensively profile the single-cell transcriptome of pig peri-implantation embryos and corresponding maternal endometrium,identifying 4 different lineages in embryos and 13 cell types in the ***-specific gene expression characterizes 4 distinct trophectoderm subpopulations,showing development from undifferentiated trophectoderm to polar and mural *** expression of genes in different types of endometrial cells illustrates their molecular response to embryos during ***,we developed a novel tool,ExtraCellTalk,generating an overall dynamic map of maternal-foetal crosstalk using uterine luminal proteins as *** cross-species comparisons,we identified a conserved RBP4/STRA6 pathway in which embryonic-derived RBP4 could target the STRA6 receptor on stromal cells to regulate the interaction with other endometrial *** results provide insight into the maternal-foetal crosstalk during embryo implantation and represent a valuable resource for further studies to improve embryo implantation.

关键词： endometrial remodeling ExtraCellTalk implantation maternal-foetal crosstalk trophoblast

Prediction of hepatic artery occlusion after liver transplantation by ultrasound characteristics and clinical risk factors

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World Journal of Radiology 2024年第6期16卷 196-202页

作者： Yu-ting Lai Yi Chen Tai-shi Fang Zhi-Yan Li Ning-Bo Zhao Department of Ultrasound National Clinical Research Centre for Infectious DiseasesThe Third People’s Hospital of ShenzhenThe Second Hospital Affiliated with the Southern University of Science and TechnologyShenzhen 518112Guangdong ProvinceChina Department of Liver Surgery National Clinical Research Centre for Infectious DiseasesThe Third People’s Hospital of ShenzhenThe Second Hospital Affiliated with the Southern University of Science and TechnologyShenzhen 518112Guangdong ProvinceChina

BACKGROUND Hepatic artery occlusion(HAO)after liver transplantation(LT)is a devastating complication,resulting in early graft loss and reduced overall ***-sound is an established assessment method for HAO in patients following LT,especially those with complex hepatic artery *** We retrospectively analyzed the ultrasound characteristics and the clinic risk factors associated with HAO in 400 adult LT patients who were enrolled and treated at the Third People's Hospital of Shenzhen between November 2016 and July *** patients diagnosed with acute HAO(A-HAO)by surgery and fifteen diagnosed with chronic HAO(C-HAO)were included.A control group of 33 patients without HAO complications during the same period were randomly selected using a random number *** patients underwent an ultrasono-graphy *** including resistance index(RI),peak systolic velocity(PSV),and portal vein velocity(PVV)were compared across the ***,basic clinical data were collected for all patients,including gender,age,primary diagnosis,D-dimer concentration,total operation time,cold ischemia time,hot ischemia time,intraoperative blood loss and transfusion,intraoperative urine volume,infusion,model for end-stage liver disease(MELD)score,and whether complex hepatic artery reconstructions were ***,risk factors influencing HAO formation after LT were *** Compared to the non-HAO group,PVV and RI were higher in the A-HAO group,while PSV was ***,both PSV and RI were lower in the C-HAO group compared to the non-HAO *** proportion of patients undergoing complex hepatic artery reconstructions and the gamma-glutamyltransferase(GGT)level before occlusion were significantly higher in the A-HAO group compared to the non-HAO ***,there were no distinct differences between the two groups in D-dimer,MELD score,pre-occlusion alanine transaminase and aspartate transaminase levels,or intrao

关键词： Hepatic artery occlusion Ultrasonography Diagnostic performance Risk factors Liver transplantation

Radiomics-based quantitative contrast-enhanced CT analysis of abdominal lymphadenopathy to differentiate tuberculosis from lymphoma

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Precision Clinical Medicine 2024年第1期7卷 87-89页

作者： Meng-ting Shen Xi Liu Yue Gao Rui shi Li Jiang Jin Yao Department of Radiology West China HospitalSichuan UniversityChengdu 610041China Key Laboratory of Carcinogenesis and Translational Research(Ministry of Education) Department of RadiologyPeking University Cancer Hospital and InstituteBeijing 100142China

Dear Editor,Tuberculosis(TB)is a significant cause of morbidity and mortality in developing countries,with a global burden of∼10.0 million cases in *** accounts for 8.4%of TB cases globally,ranking third after India and Indonesia[1].Abdominal TB is a common extrapulmonary manifestation,often presenting as *** differentiation between abdominal tuberculosis lymphadenopathy(ATBL)and lymphoma holds significance for treatment decisions and prognosis.

关键词： tuberculosis lymphoma abdominal

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复用传统仪表的火化机工况监测系统

现代电子技术 2024年第4期47卷 6-10页

作者：史峰朱挺民政部一零一研究所北京100070 广西科技大学自动化学院广西柳州545006

火化机工况监测是火化机质量检测和环保监测的必要基础。为降低火化机工况监测建设成本,快速提升监测覆盖率,设计一种可复用传统仪表的火化机工况监测系统。通过分析现有火化机工况,将火化机工况监测的内容归纳为包括主燃室温度、再燃... 详细信息

火化机工况监测是火化机质量检测和环保监测的必要基础。为降低火化机工况监测建设成本,快速提升监测覆盖率,设计一种可复用传统仪表的火化机工况监测系统。通过分析现有火化机工况,将火化机工况监测的内容归纳为包括主燃室温度、再燃室温度、主燃室压差、油耗、含氧量等的燃烧状况和包括一氧化碳、二氧化硫、氮氧化物等排放气体的监测。针对火化机工况监测需求,将传统监测仪表按数据输出接口归纳为热电偶电压信号和电流信号,并基于这两类信号开发可采集传统仪表数据的采集设备。数据采集后,通过无线网络上传至数据服务器,利用Web技术实现终端用户对火化机工况的远程实时监测。测试结果表明,所设计系统对火化机相关工况数据的监测精度均在1%F.S.以内,可满足火化机工况监测的要求,其低成本建设方案具有较强的应用前景。

关键词：火化机工况监测系统传统仪表实时监测数据采集复用技术

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