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Open Journal of Metal 2020年第3期10卷 35-44页

作者： Boris Viktorovich Borts stella fedorovna skoromnaya Viktor Ivanovich Tkachenko NSC “Kharkov Institute of Physics and Technology” Kharkov Ukraine V.N. Karazin Kharkiv National University Kharkov Ukraine

The temporal dynamics of the edge dislocation (ED) was studied in this work using the inhomogeneous dissipative sine-Gordon (SG) equation. The consideration was carried out for the force action levels both less and more critical. By SG equation numerical calculations it is shown that at the external force value below a critical one the ED takes a shape close to a semicircle. This shape was used as an initial condition for describing the ED temporal dynamics in the FR source operating mode. A particular solution of the SG equation is proposed that describes the temporal dynamics of half the ED in the FR mode, which rests on a stopper at the origin. It is shown that the proposed particular solution corresponds to the left Archimedes spiral displaced at π/2 counterclockwise relative to the azimuth angle equal to zero. It is noted that the temporal dynamics of the second half of the ED segment rested on the second stopper is described by the proposed particular solution, when it is mirrored relative to the problem symmetry axis and the center of the spiral is displaced to a point with a zero azimuthal angle and a radius equal to the distance between the stoppers. The axis of symmetry is a straight line that is perpendicular and halves the distance between the stoppers. A graphical description of the ED temporal dynamics was plotted in the Cartesian coordinate system based on the proposed particular solution and its mirror and displaced image. It is shown that the particular solution of the SG equation in the RF source operation mode involves two Archimedes spirals symmetrical relative to the problem symmetry axis with equal radii increasing linearly with time, which rotate: one (the spiral center coincides with the stopper at the origin) counterclockwise, the second (the spiral center coincides with the second stopper) clockwise.

关键词： Edge Dislocation Sine-Gordon (SG) Equation Frank-Read Source Archimedes Spiral Temporal Dynamics

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Separation of Molybdenum Isotopes at Supercritical Fluid Extraction with Carbon Dioxide in a Vertical Gradient Field of Temperatures

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Open Journal of Metal 2020年第1期10卷 1-15页

作者： Boris Viktorovich Borts stella fedorovna skoromnaya Viktor Ivanovich Tkachenко NSC Kharkov Institute of Physics and Technology NAS of Ukraine Kharkov Ukraine V. N. Karazin Kharkiv National University Kharkov Ukraine

Separation of molybdenum isotope complexes by supercritical fluid extraction (SFE) with carbon dioxide was studied experimentally. The extraction of molybdenum isotope complexes was carried out in the updated extraction chamber (reactor) of the SFE-U installation, which provided an initial pressure of P ≤ 20 MPa at constant temperatures of the upper T1 = 35°C and bottom T2 = 45°C flanges. The device, through which the eluent was discharged, involved a set of four thin tubes of different lengths located inside the reactor. The axes of the tubes and the reactor are parallel and the tubes are equally spaced circumferentially inside the reactor. The extract was removed from each tube through channels isolated from each other and located in the bottom flange with cylindrical expansion, in which several layers of filter paper were placed. After passing through the filters the extract entered a restrictor designed to remove the eluent from the reactor. The initial pressure of carbon dioxide and the holding time of the extract were specified in the experiments. The level of the eluent sampling was set by the lengths of the tubes depending on the reactor height. A method of producing molybdenum complexes was described. It was experimentally shown that at an initial pressure of 20 MPa and a given holding time a difference from the natural content of Mo isotopes for given heights of extract sampling depending on the reactor height was observed in extracts removed through filters. The ranges of deviation of the content of molybdenum isotopes in extracts from natural one were determined.

关键词： Carbon Dioxide Supercritical Fluids Extraction Molybdenum Isotopes Separation

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