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Surface Nanocrystallization of Magnesium Alloy AZ91D by High-Energy Shot Peening

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Journal of Wuhan University of technology(Materials science) 2009年第4期24卷 515-519页

作者：张津 School of Materials science & Engineering University of Science and Technology Beijing College of Materials science & Engineering Chongqing University of Technology

High-energy shot peening （HESP）, a method to produce severe plastic deformation by high velocity flying balls, was applied on die cast magnesium alloy AZ91D. Effects of surface nanocrystallization by HESP and heat treatment at different temperatures were investigated. The mi- crostructure evolution was conducted using X-ray diffraction （XRD） and field emission scanning electronic microscopy （FESEM）. The hardness was measured by microhardness tester. The experimental results show that surface nanocrystrallization of AZ91D obtained by HESP would lead to the increase of microhardness. Low temperature heated at 100℃ for 1 h do not change the property obviously. However, both the microstructure and microhardness vary greatly after heat treatment at 400℃ for 1 h.

关键词： AZ91 D surface nanocrystallization HESP microhardnss corrosion resistance

Magnetron sputtering synthesis of large area well-ordered boron nanowire arrays

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science China(Physics,Mechanics & Astronomy) 2004年第4期47卷 403-415页

作者： CAO Limin1,2. ZHANG Ze2.& WANG Wenkui1,2.1. Key Laboratory of Metastable Materials science and technology and College of Materials science and Engineering, Yanshan University, Qinhuangdao 066004, China 2. Institute of Physics, Chinese Academy of sciences, Beijing 100080, China Key Laboratory of Metastable Materials science and technology and College of Materials science and Engineering Yanshan University Qinhuangdao China Institute of Physics Chinese Academy of Sciences Beijing China

One-dimensionally nanostructured materials, such as nanowires and nanotubes, are the smallest dimensional structures for efficient transport of electrons and excitons, and are therefore critical building blocks for nanoscale electronic and mechanical devices. In this paper, boron nanowires with uniform diameters from 2. to 80 nm were synthesized by radio-frequency magnetron sputtering of pure boron powder and B2.3 powder mixtures in argon atmosphere. The boron nanowires produced stand vertically on the substrate surface to form well-ordered arrays over large areas with self- organized arrangements without involvement of any template and patterned catalyst. The high-density boron nanowires are parallel to each other and well distributed, forming highly ordered and uniform arrays. A more interesting and unique feature of the boron nanowires is that most of their tips are flat rather than hemispherical in morphologies. Detailed studies on its structure and composition indicate that boron nanowires are amorphous. Boron nanowire appears as a new member in the family of one-dimensional nanostructures. Considering the unique properties of boron-rich solids and other nanostructures, it is reasonable to expect that the boron nanowires will display some exceptional and interesting properties. A vapor-cluster-solid (VCS) mechanism was proposed to explain the growth of boron nanowires based on our experimental observations.

关键词： boron nanowires, magnetron sputtering, arrays, self-assembly.

Further study of sources of the imported cobalt-blue pigment used on Jingdezhen porcelain from late 13 to early 15 centuries

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science China(Technological sciences) 2008年第3期51卷 249-259页

作者： DU Feng1 & SU BaoRu2.1 Institute of Chemistry & Molecular Engineering, Qingdao University of science & technology, Qingdao 2.6000, China 2.College of Information science technology, Qingdao University of science & technology, Qingdao 2.6000, China Institute of Chemistry & Molecular Engineering Qingdao University of Science & Technology Qingdao China College of Information science technology Qingdao University of Science & Technology Qingdao China

Based on the conclusion of modern scientific analysis: the cobalt-blue pigment applied on Jingdezhen official porcelain during Yuan Dynasty and prior to Xuande reign of Ming Dynasty (12.1―142.) contains high iron and low manganese con- tents, and the cobalt during Xuande and after Xuande periods (after 142.) of Ming Dynasty contains high manganese and low iron contents, in combination with the traditional archaeological method, the related historical textual records were in- vestigated and analyzed, the imported cobalt employed on Jingdezhen official porcelain was studied comprehensively, systematically and logically. In fact, 'Su Ma Li Qing' (Samarra-blue) and 'Su Bo Ni Qing' (Sumatra-blue) are definitely different cobalt ores originated in different places, because of their very similar translitera- tions in Chinese, the confusion has appeared in ancient books for more than 400 years, which considered 'Su Ma Li Qing' and 'Su Bo Ni Qing' as the same co- balt-blue pigment. In this article the mistake was corrected, the possible producing places and the approximate eras of the two pigments imported to China and used at Jingdezhen were also suggested.

关键词： imported cobalt-blue pigments employed on official blue-and-white porcelain Yuan Dynasty early Ming Dy- nasty Mn/Fe content ratio Su Ma Li Qing (Samarra-blue) Su Bo Ni Qing (Sumatra-blue) scientific archae- ological research transliteration

Adsorption of zinc on manganite(γ-MnOOH): particle concentration effect and adsorption reversibility

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Journal of Environmental sciences 2004年第4期16卷 627-630页

作者： QIN Yan-wen1, PAN Gang 1,2., ZHANG Ming-ming1, LI Xian-liang1 (1. State Key Laboratory of Environmental Aquatic Chemistry, Research Center for Eco-Environmental sciences, Chinese Academy of sciences, Beijing 100085, China. 2. Qingdao University of science & technology, Qingdao 2.6042. China) State Key Laboratory of Environmental Aquatic Chemistry Research Center for Eco-Environmental Sciences Chinese Academy of Sciences Beijing 100085 China.

The adsorption and desorption processes of Zn(Ⅱ) on γ-MnOOH as a function of particle concentrations(C p) were studied. An obvious C p effect was observed in this adsorption system. The degree of adsorption hysteresis increased greatly with the increasing of C p, indicating that the extent of the real metastable-equilibrium states deviating from the ideal equilibrium state was enhanced with the increasing of C p. The C p-reversibility relationship confirmed the metastable-equilibrium adsorption(MEA) inequality(Pan, 1998a), which was the core formulation of the MEA theory. Because the MEA inequality was based on the basic hypothesis of MEA theory that adsorption density Γ is not a state variable, the C p-reversibility relationship gave indirect evidence to the basic hypothesis of MEA theory.

关键词： zinc γ-MnOOH adsorption reversibility

Refractive index changes induced by sheet beams with various intensity distributions in LiNbO_(3):Fe crystal

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science China(Physics,Mechanics & Astronomy) 2005年第4期48卷 399-412页

作者： ZHANG Peng1, ZHAO Jianlin1, XU Honglai1, SUN Yidong2. YANG Dexing1 & WANG Meirong1 1. Institute of Optical Information science and technology, School of science, Northwestern Polytechnical University, Xi’an 710072. China 2. School of science, Xi’an Jiaotong University, Xi’an 710049, China Institute of Optical Information science and Technology School of Science Northwestern Polytechnical University Xi’an China School of science Xi’an Jiaotong University Xi’an China

According to the Kukhtarev equations and a simplified model based on the photovoltaic charge carriers transport mechanism, the distributions of the index changes (DICs) in LiNbO3:Fe crystals induced by sheet beams with various intensity profiles are theoretically analyzed. The numerically simulated results coincide with the analytic expressions deduced from the simplified model. The DICs in a LiNbO3:Fe crystal induced by sheet beams with rectangular, Gaussian and square law profiles are measured by using the interferometric method. By employing the analytic expressions, the experimental data points are well fitted. By utilizing the angular spectrum theory and the ray equation, the uniformities of the intensity profiles of the writing beams along the propagation directions and the influences of the self-defocusing effect of the crystal are numerically simulated, respectively. The results show that the experimental results are reliable. The numerically simulated method and the analytic expressions can be both employed to predict the DICs induced by sheet beams with various light intensity profiles. Furthermore, utilizing writing beams with proper intensity profiles, any desired index distributions could be obtained.

关键词： LiNbO3:Fe crystal, light intensity profile, distribution of refractive index changes, sheet beam.

Progress of Lyman-alpha-based beam emission spectroscopy(Ly BES)diagnostic on the HL-2. tokamak

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Plasma science and technology 2024年第3期26卷 118-125页

作者：周艺轩余羿许敏柯锐聂林徐皓赵光义刘灏袁子豪肖晨雨李继全肖池阶 the HL-2. Team southwestern Institute of Physics Chengdu 610041People's Republic of China Sino-French Institute of Nuclear Engineering and technology Sun Yat-sen UniversityZhuhai 519082People's Republic of China State Key Laboratory of Nuclear Physics and technology School of PhysicsPeking UniversityBeijing 100871People's Republic of China

An edge Lyman-alpha-based beam emission spectroscopy(LyBES)diagnostic,using a heating NBI(neutral beam injection)system,is currently under development on the HL-2. *** 2.-channel edge LyBES,which is intended to measure the density fluctuation in plasma edge(from R=1960 mm to R=2.2. mm)with an improved spatial resolution of 3.3 mm,is a complement to the existing conventional beam emission spectroscopy(BES)*** this article,we introduce the progress of LyBES diagnostic,including the collection optics,the monochromator,and the detector *** reflectance of the collection mirrors is measured to be~82.at 12. nm,and the aberration geometrical radius of the collection optics is tested to be~150μm in the aimed *** linear dispersion of the LyBES monochromator is designed to be~0.09 nm mm^(-1).The bandwidth of the detector system with the 5×10^(7)V A^(-1)preamplifier gain is measured to be~2.0 kHz,and the peak-to-peak noise of the detector system is tested to be~16 *** finalized design,components development and testing of the LyBES diagnostic have been completed at present,and an overall performance of the LyBES diagnostic is to be confirmed in the next HL-2. campaign.

关键词： density fluctuation Ly BES BES vacuum ultraviolet

Binding Materials of Dehydrated Phases of Waste Hardened Cement Paste and Pozzolanic Admixture

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Journal of Wuhan University of technology(Materials science) 2009年第1期24卷 140-144页

作者：吕林女 School of science Wuhan University of Technology

Fly ash （FA） and ground granulated blast-furnace slag （GGBFS） were added to improve the performances of regenerated binding materials （RBM） which refer to dehydrated phases with rebinding ability of waste hardened cement paste. Flowability tests, compressive strength tests, SEM, TG-DSC, and non-evaporable water content tests were employed to study the performances of the combined binding materials and the interactions between RBM, FA, and GGBFS. Results show that adding FA or GGBFS can improve the workability of RBM paste, and GGBFS has positive effects on strength of RBM. Pozzolanic reactions happen between RBM, FA, and GGBFS. And the activation effect of RBM to FA and GGBFS is superior to that of P.O grade-32.5 cement, especially at earlier ages, because of the high reactive f-CaO existing in RBM. On the advantages of the synergetic effects of RBM and pozzolanic admixtures such as FA and GGBFS, new combined binding materials can be prepared by blending them together.

关键词： combined binding materials dehydrated phase fly ash granulatedblast-furnace slag

Development of Expert Controller for Plasma Spraying Process

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材料热处理学报 2004年第5B期25卷 783-786页

作者： LIChun-xu CHENKe-xuan LIHe-qi LIDe-wu EducationMinistryKeyLab.ofAdvancedProcessingtechnologyforNon-ferrousMaterials LanzhouUniversityofScience＆TechnologyLanzhouChina CollegeofMaterialsscienceandEngineering LanzhouUniv.ofScience＆TechnologyLanzhouChina

Aiming at the plasma spraying process control, the control system model is developed on the basis of analyzing control parameters and coating properties and their correlation, and the corresponding control method and regulations are also given. With the developed expert controller for plasma spraying process, stable spraying can be realized using ordinary spraying powder and the coating of compaction, homogeneity and high bonding strength can be obtained.

关键词：等离子喷涂控制器粉末熔炼镀层厚度

Ecological Footprint and Ecological Security Evaluation in the Upper Min River Basin

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Wuhan University Journal of Natural sciences 2005年第4期10卷 641-646页

作者： TU Jian-jun 1, 2.1. School of Resources and Environment science, southwest China Normal University, Chongqing 400715, China 2. Institute of Mountain Hazards and Environment, Chinese Academy of sciences, Chengdu 610041, Sichuan, China School of Resources and Environment science Southwest China Normal University Chongqing China Institute of Mountain Hazards and Environment Chinese Academy of Sciences Chengdu Sichuan China

On the basis of the ecological footprint (EF) model, this paper studied theecological security in the Upper Min River Basin ecosystem. The result shows that with 2. 038 2.hm^2.er capita ecological capacity (0. 42. 2.hm^2.higher than per capita EF) ,and 165 82. hm^2.ecologysurplus , the ecosystem in Upper Min River is generally secure at present. But the arable land isoverweighed and omens an eco-security crisis. Meanwhile, problems such as low forest coverage rate,severe loss of water and soil,enlargement of arid-valley area, frequent occurrence of mountainhazards and degradation of pastures have been major threats to the eco-security of this region. Thecalculation result of ten-thousand-yuan ( RMB) GDP shows that the use of natural resources isextensive, and there will be a rapid increase tendency of EF in the future. In order to maintain thepresent eco-security, the ways of use natural resources must be improved in the Upper Min RiverBasin.

关键词： ecological security ecological footprint ecological capacity quantitativeevaluation the Upper Min River Basin