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Characterization of Novel Lignocellulosic Spinifex littoreus Fibers and Their Composites

Journal of Bionic Engineering 2020年第2期17卷 393-404页

作者： Milan Soosai Christopher Thankian Winowlin Jappes Jebas Thangiah Rajini Nagarajan Mayandi Kalimuthu sikiru oluwarotimi ismail Faruq Mohammad Department of Mechanical Engineering Cape Institute of TechnologyLevengipuramTirunelveli 627114Tamil NaduIndia Department of Mechatronics Engineering Kamaraj College of Engineering&Technology VellakulamMadurai dist-622701Tamil NaduIndia Centre for Composite Materials Department of Mechanical EngineeringKalasalingam UniversityKrishnankoilVirudhunagar 626126Tamil NaduIndia Centre for Engineering Research Department of EngineeringSchool of Engineering and Computer ScienceUniversity of HertfordshireHatfieldHertfordshire AL109ABUK Surfactants Research Chair Department of ChemistryCollege of ScienceKing Saud UniversityRiyadh 11451Kingdom of Saudi Arabia

This innovative work presents mechanical,physical and chemical characterization and analysis of newly extracted fiber from naturally resourced plant stem,named Spinifex littoreus fibers(SLF).This is a novel natural,biodegradable and sustainable reinforcement for an improved ***,the chemical constituents of SLF,such as cellulose,lignin,moisture and wax content were *** raw SLF surfaces were modified by chemical treatment with sodium hydroxide(NaOH),calcium hydroxide(Ca(OH)2)and silane.A polyester matrix was reinforced with all the treated SLF,before the mechanical properties(tensile strengths)of the composites were *** all the surface chemically treated SLF/polyester composite samples,the Ca(OH)2 treated sample exhibited the highest tensile *** microscopic examination was carried out to validate this ***,this analysis established the mechanism of failure of the tensile fractured composite samples,using Scanning Electron Microscope(SEM),among other techniques.

关键词： cellulosic fiber Spinifex littoreus fibers XRD FTIR SEM tensile strength

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Isolation of Microcrystalline Cellulose from Wood and Fabrication of Polylactic Acid(PLA)Based Green Biocomposites

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Journal of Renewable Materials 2024年第8期12卷 1455-1474页

作者： Selwin Maria Sekar Rajini Nagarajan Ponsuriyaprakash Selvakumar ismail sikiru oluwarotimi Kumar Krishnan Faruq Mohammad Mohammed Rafi Shaik Nadir Ayrilmis Department of Mechanical Engineering Kalasalingam Academy of Research and EducationKrishnankoil626126India Department of Mechanical Engineering SSM Institute of Engineering and TechnologyDindigul624002India Department of Engineering Centre for Engineering ResearchSchool of PhysicsEngineering and Computer ScienceUniversity of HertfordshireHatfieldAL109ABUK INTI International University Persiaran Perdana BBNNilai71800Malaysia Department of Chemistry College of ScienceKing Saud UniversityP.O.Box 2455Riyadh11451Kingdom of Saudi Arabia Department of Wood Mechanics and Technology Faculty of ForestryIstanbul University–CerrahpasaBahcekoySariyerIstanbul34473Turkey

An innovative microcrystalline cellulose(MCC)natural fibre powder-reinforced PLA biocomposite was investigated using the hand lay-up *** polymer matrix composite(PMC)samples were prepared by varying the weight percentages(wt.%)of both PLA matrix and MCC reinforcement:pure PLA/100:0,90:10,80:20,70:30,60:40 and 50:50 wt.%,*** the results obtained,MCC powder,with its impressive aspect ratio,proved to be an ideal reinforcement for the PLA,exhibiting exceptional mechanical *** was evident that the 80:20 wt.%biocomposite sample exhibited the maximum improvement in the tensile,flexural,notched impact,compressive strength and hardness by 28.85%,20.00%,91.66%,21.53%and 35.82%,respectively compared to the pure PLA ***,during the thermogravimetric analysis(TGA),the same 80:20 wt.%biocomposite sample showed a minimum weight loss of 20%at 400℃,among *** morphological study using Field Emission Scanning Electron Microscopy(FE-SEM)revealed that the uniform distribution of cellulose reinforcement in the PLA matrix actively improved the mechanical properties of the biocomposites,especially the optimal 80:20 wt.%***,it was evident that the optimal PLA/cellulose biocomposite sample could be a suitable and alternative sustainable,environmentally friendly and biodegradable material for semi/structural applications,replacing synthetic and traditional components.

关键词： Polylactic acid micro crystalline cellulose biocomposite characterizations FESEM environmental pollution

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3D printing of PEEK–cHAp scaffold formedical bone implant

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Bio-Design and Manufacturing 2021年第1期4卷 44-59页

作者： Bankole I.Oladapo SAbolfazl Zahedi sikiru O.ismail Francis T.Omigbodun Oluwole K.Bowoto Mattew A.Olawumi Musa A.Muhammad School of Engineering and Sustainable Development De Montfort UniversityLeicesterUK Centre for Engineering Research School of PhysicsEngineering and Computer ScienceUniversity of HertfordshireHatfieldUK Mechanical Engineering Loughborough UniversityLoughboroughUK Faculty of Engineering Computing and mediaDe Montfort UniversityLeicesterUK Faculty of Engineering Environment and ComputingCoventry UniversityCoventryUK

The major drawback associated with PEEK implants is their biologically inert surface,which caused unsatisfactory cellular response and poor adhesion between the implants and surrounding soft tissues against proper bone *** this study,polyetheretherketone(PEEK)was incorporated with calcium hydroxyapatite(cHAp)to fabricate a PEEK-cHAp biocomposite,using the fused deposition modeling(FDM)method and a surface treatment strategy to create microporous architectures onto the filaments of PEEK lattice ***,nanostructure and morphological tests of the PEEK-cHAp biocomposite were modeled and analyzed on the FDM-printed PEEK-cHAp biocomposite sample to evaluate its mechanical and thermal strengths as well as in vitro cytotoxicity via a scanning electron microscope(SEM).A technique was used innovatively to create and investigate the porous nanostructure of the PEEK with controlled pore size and distribution to promote cell penetration and biological integration of the PEEK-cHAp into the *** vivo tests demonstrated that the surface-treated micropores facilitated the adhesion of newly regenerated soft tissues to form tight implant-tissue interfacial bonding between the cHAp and *** results of the cell culture depicted that PEEK-cHAp exhibited better cell proliferation attachment spreading and higher alkaline phosphatase activity than PEEK *** islands formed on the PEEK-cHAp composite after immersion in simulated body fluid of Dulbecco’s modified Eagle medium(DMEM)for 14 days and grew continuously with more or extended *** microstructure treatment of the crystallinity of PEEK was comparatively and significantly different from the PEEK-cHAp sample,indicating a better treatment of *** in vitro results obtained from the PEEK-cHAp biocomposite material showed its biodegradability and performance suitability for bone *** study has potential applications in the field of biomedical engineering to strengthen the conceptual kn

关键词： 3D printing PEEK-cHAp biocomposite Nanostructure Bone implant Composite morphing

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