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Experimental and Numerical Analysis of Thermal Deformation of Electronic Packages,QFP and MCM

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实验力学 2006年第1期21卷 11-19页

作者： Yasuyuki morita Kazuo Arakawa Mitsugu Todo Research Institute for Applied Mechanics Kyushu University 6-1 Kasuga-koen Kasuga-shi Fukuoka 816-8580 Japan

Moiré inteferometry and FEA (finite element analysis) were used to evaluate the thermal deformation of two electronic packages, QFP (quad flat package) and MCM (multi chip module).Thermal loading was applied by cooling the packages from 100℃ to room temperature (25℃). Moiré fringes were obtained on the cross sections of the packages to clarify the effect of the CTE (coefficient of thermal expansion) mismatch of the micro components, such as silicon, metal and resin. In QFP, the effects of packaging resin and PCB (printed circuit board) on the thermal deformation were investigated. The effect of location of three silicon chips in MCM was also examined.

关键词：数字分析热形变电子仪器组件 QFP MCM

Experimental and Numerical Evaluation of the Performance of Supersonic Two-Stage High-Velocity Oxy-Fuel Thermal Spray (Warm Spray) Gun

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Journal of Thermal Science 2011年第1期20卷 88-92页

作者： H.Katanoda H.morita M.Komatsu S.Kuroda Department of Mechanical Engineering Kagoshima University1-21-40 KorimotoKagoshima 890-0065Japan Hybrid Materials Center National Institute for Materials Science1-2-1SengenTsukubaIbaraki 305-0047Japan

The water-cooled supersonic two-stage high-velocity oxy-fuel (HVOF) thermal spray gun was developed to make a coating of temperature-sensitive material,such as titanium,on a *** gun has a combustion chamber (CC) followed by a mixing chamber (MC),in which the combustion gas is mixed with the nitrogen gas at room *** mixed gas is accelerated to supersonic speed through a converging-diverging (C-D) nozzle followed by a straight passage called the *** paper proposes an experimental procedure to estimate the cooling rate of CC,MC and barrel ***,the mathematical model is presented to predict the pressure and temperature in the MC for the specific mass flow rates of fuel,oxygen and nitrogen by assuming chemical equilibrium with water-cooling in the CC and MC,and frozen flow with constant specific heat from stagnant condition to the throat in the CC and ***,the present mathematical model was validated by comparing the calculated and measured stagnant pressures of the CC of the two-stage HVOF gun.

关键词： Supersonic flow Two-stage HVOF thermal spray gun Warm spray

Fatigue properties of rolled AZ31B magnesium alloy plate

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Transactions of Nonferrous Metals Society of China 2010年第B07期20卷 523-526页

作者： S.morita N.OHNO F.TAMAI Y.KAWAKAMI Faculty of Science and Engineering Saga University Material and Environment Department Industrial Technology Center of Saga

Fatigue strength,crack initiation and propagation behavior of rolled AZ31B magnesium alloy plate were investigated. Axial tension-compression fatigue tests were carried out with cylindrical smooth *** types of specimens were machined with the loading axis parallel(L-specimen)and perpendicular(T-specimen)to rolling *** compressive 0.2%proof stress,tensile strength and tensile elongation were similar for both *** the other hand,monotonic tensile 0.2%proof stress of the L-specimen was slightly higher than that of the ***,monotonic compressive 0.2%proof stresses were lower than tensile ones for both *** fatigue strengths of 107cycles of the L-and T-specimens were 95 and 85 MPa,respectively. Compared with the monotonic compressive 0.2%proof stresses,the fatigue strengths were higher for both *** other words, the fatigue crack did not initiate and propagate even though deformation twins were formed in compressive stress under the cyclic tension-compression *** fatigue crack initiated at early stage of the fatigue life in low cycle regime regardless of specimen *** crack growth rate of the L-specimen was slightly lower than of the ***,the fatigue lives of the L-specimen were longer than those of the T-specimen in low cycle regime.

关键词： magnesium alloy compressive proof stress fatigue strength crack initiation crack propagation

High-strain-rate superplasticity in oxide ceramics:a trial of microstructural design based on creep-cavitation mechanisms

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Acta Metallurgica Sinica(English Letters) 2011年第3期24卷 195-204页

作者： Keijiro HIRAGA Byung-Nam KIM Koji morita Hidehiro YOSHIDA Yoshio SAKKA Masaaki TABUCHI National Institute for Materials Science

From existing knowledge about high-temperature cavitation mechanisms, necessary conditions were discussed for the suppression of cavitation failure during superplastic deformation in ceramic materials. The discussion, where special attention was placed on the relaxation of stress concentrations during grain-boundary sliding and cavity nucleation and growth, leaded to a conclusion that cavitation failure could be retarded by the simultaneous controlling of the initial grain size, the number of residual defects, diffusivity, dynamic grain growth and the homogeneity of microstructure. On the basis of this conclusion, high-strain-rate superplasticity （defined as superplasticity at a strain rate higher than 0.01 s^-1） could be intentionally attained in some oxide ceramic materials. This was shown in tetragonal zirconia and composites consisting of zirconia, a-alumina and a spinel phase.

关键词： Grain-boundary sliding Accommodation Stress concentration Diffusional relaxation Cavity nucleation Cavity growth Dynamic grain growth

Recent progress in upgrading metallurgical-grade silicon to solar-grade silicon via pyrometallurgical routes

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International Journal of Minerals,Metallurgy and Materials 2022年第4期29卷 767-782页

作者： Yun Lei Xiaodong Ma Ye Wang Zhiyuan Chen Yongsheng Ren Wenhui Ma Kazuki morita Faculty of Metallurgical and Energy Engineering Kunming University of Science and TechnologyKunming 650093China Sustainable Minerals Institute The University of QueenslandSt Lucia 4072QLDAustralia School of Chemical Engineering Sichuan UniversityChengdu 610065China Separation and Conversion Technology Flemish Institute for Technological ResearchMol 2400Belgium Department of Materials Engineering Graduate School of EngineeringThe University of TokyoTokyo 113-8656Japan

Si-based photovoltaic solar power has been rapidly developed as a renewable and green energy *** widespread use of Sibased solar cells requires large amounts of solar-grade Si(SoG-Si)to manufacture Si *** routes,mainly the modified Siemens process,have dominated the preparation of polycrystalline SoG-Si;however,traditional chemical techniques employ a series of complex chemical reactions involving various corrosive and hazardous *** addition,large amounts of complex waste solar cells and Si kerf slurry waste gradually accumulate and are difficult to recycle using these *** methods are required to meet the demand for SoGSi preparation and Si waste *** metallurgical route shows promise but is hindered by the problem of eliminating B and P from metallurgical-grade Si(MG-Si).Various pyrometallurgical treatments have been proposed to enhance the removal of B and P from *** article reviews Si refining with slag treatment,chlorination,vacuum evaporation,and solvent refining,and summarizes and discusses the basic principles and recent representative studies of the four *** these,solvent refining is the most promising and environmentally friendly approach for obtaining low-cost SoG-Si and is a popular research ***,a simple and green approach,i.e.,a combination of solvent refining,slag treatment,or vacuum directional solidification,is proposed for low-cost SoG-Si preparation using MG-Si or Si wastes as raw materials.

关键词： silicon refining solar-grade silicon solvent refining vacuum evaporation slag treatment Si kerf slurry waste

Observation of the Two-Dimensional Distribution of Impurity Line Emissions Using a Space-Resolved EUV Spectrometer in LHD

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Plasma Science and Technology 2013年第2期15卷 106-109页

作者：王二辉 S.morita M.GOTO 董春凤 Department of Fusion Science Graduate University for Advanced StudiesToki 509-5292Gifu Japan National Institute for Fusion Science Toki 509-5292 Gifu Japan

A space-resolved EUV spectrometer for measuring the one-dimensional distribution of impurity line emissions in Large Helical Device （LHD） has been upgraded to measure two- dimensional distributions of impurity line emissions with an extension of working wavelength range to 30-650% The two-dimensional measurement is performed by scanning the observation chord horizontally. A rectangular plasma region of 520 × 700 mm2 in vertical and horizontal sizes can be observed during a single horizontal scan. The horizontal scan requires a time duration of 5 s at least. The spatial resolution is 10 mm in the vertical direction when a spatial-resolution slit of 0.2 mm in width is adopted. Although a spatial resolution in the toroidal direction is 75 mm, it is a function of CCD exposure time and horizontal scanning speed. Two-dimensional distribution of EUV line emissions from several impurities has been successfully observed for the first time from steady discharges in LHD. In this paper two-dimensional distributions of He II （303.78A）, C V （40.27A）, C VI （33.73A） and Fe XX （132.85A） located at different radial positions are presented with simple analysis on the magnetic field structure of LHD.

关键词： EUV spectrometer impurity line emission two-dimensional distribution

Syntheses of Soluble Biopolyimides Using 4-Aminophenylalanine

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Chinese Journal of Polymer Science 2020年第10期38卷 1117-1123,I0007页

作者： Kenji Takad Hiromasa shinagaw Yuki morita Manjit SGrewal Kazuya Taya Amit Kumar Tatsuo Kaneko Graduate Schoo/of Advanced Science and Technology Energy and Environment AreaJapan Advanced Institute of Science and Technology(AISTI1-1 AsahidaiNomiIshikawa923-1292Japan Marialnrganomeallics Laboratony Department ofChemisty Atma Ram Sanatan Dharma CllegeUniversity of DelhiNew Delhi-10021India

4-Aminophenylalanine(4APhe),an exotic amino acid which is obtained as a microorganism metabolite of glucose,is polycondensed with various tetracarboxylic dianhydrides as a diamine monomer to obtain poly(amic acid)*** thermal imidization of poly(amic acid)s is made at 220°C with stepwise heating from 100°*** of the obtained polyimides(PIs)exhibited good solubility in organic solvents such as N,N-dimethylformamide,N.N dimethylacetamide,and *** progress of imidization was observed by proton nuclear magnetic resonance and infrared spectroscopy to confrm that the imidization ratio was up to 98%.Carboxylate group of the side-chains of PIs affected their solubilities despite the high imidization ratio,and the solubility was lost for any organic solvents by decarboxylation at 280。C,confirmed from mass-loss of thermogravimetric ***,a new series of PIs were obtained with abilities of solvent-molding in PI state and thermal resistivityt enhancement by further heating after molding.

关键词： Bio-based polymers Polyimides Amino acids 4-Aminophenylalanine Soluble polyimides

Hybrid Polyaniline Systems under Chiral and Redox Control

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复旦学报（自然科学版） 2005年第5期44卷 707-708页

作者： Toshikazu Hirao Toshiyuki Moriuchi Kenji morita Department of Applied Chemistry Graduate School of Engineering Osaka University Yamada-oka Suita Osaka 565-0871 JapanDepartment of Applied Chemistry Graduate School of Engineering Osaka University Yamada-oka Suita Osaka 565-0871 JapanDepartment of Applied Chemistry Graduate School of Engineering Osaka University Yamada-oka Suita Osaka 565-0871 Japan

Polyanilines are one of the promising electrically conducting π-conjugated polymers with chemical stability. In recent year, there has been increased interest in chiral induction of polyanilines because of their potential use in diverse areas. Chiral polyaniline has been reported to be formed only by the chiral acid dopant[1]. In our previous papers, complexation of polyanilines or their oligomers with transition metals modulates the redox properties of the quinonediimine unit, which is related to the catalytic function in the oxidation reaction[2].The controlled complexation with palladium(Ⅱ) compounds has been achieved to afford the cross-linked network conjugated complexes, in which the quinonediimine moieties serve as bridging coordination sites[3].Another hybrid system consisting of π-conjugated polymer and transition metal is also described.

关键词：氨苯聚乙烯混合物氧化还原控制共轭聚合体手性合成

Surgical resection for pulmonary recurrence of esophageal cancer after curative esophagectomy

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Journal of Cancer Metastasis and Treatment 2021年第1期7卷 412-421页

作者： Masaru morita Manabu Yamamoto Yuichiro Nakashima Keiichi Shiokawa Yuki shin Yoshiaki Fujimoto Tomonori Nakanoko Hideo Uehara Masahiko Sugiyama Mitsuhiko Ota Yohei Mano Keishi Sugimachi Tatsuro Okamoto Yasushi Toh Department of Gastroenterological Surgery National Hospital Organization Kyushu Cancer CenterFukuoka 811-1395Japan Department of Hepatobiliary-Pancreatic Surgery National Hospital Organization Kyushu Cancer CenterFukuoka 811-1395Japan Department of Thoracic Oncology National Hospital Organization Kyushu Cancer CenterFukuoka 811-1395Japan.

Aim:To clarify the significance of surgical resection for pulmonary recurrence after curative esophagectomy for esophageal ***:Clinical details,such as the recurrence site,timing,and contents of therapies for recurrence,and the prognosis,were examined in 14 patients who underwent surgical resection for pulmonary recurrence that developed after curative ***:The median disease-free interval after esophagectomy was 17.2 *** patients underwent pulmonary resection two times,and in one patient,three *** pulmonary resections were performed when other extra-pulmonary recurrences had been controlled,and R0 resection was *** and/or radiotherapy were additionally performed for pulmonary metastasis in 13 *** median survival time after initial pulmonary resection was 45.5 months,and the 1-,3-,and 5-year overall survival rates were 93%,68%,and 43%,*** 5-year overall survival rate after initial pulmonary resection was 13%in patients with Stage III or IV esophageal cancer and 100%in those with Stage I or II disease(P=0.010).The rate was 56%in patients with tumors<20 mm in size,while all 5 patients with lesions≥20 mm in size died within 3 years(P=0.005).Conclusion:Surgical resection along with systemic therapy is a promising treatment strategy for pulmonary recurrence after curative esophagectomy when it is solitary and *** factors,such as the esophageal cancer stage and the size of the pulmonary metastasis,are useful for deciding on the surgical indication.

关键词： Esophageal cancer pulmonary metastasis recurrence surgical resection