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Cleaning of Chromate Manufacture Process

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International Journal of Minerals,Metallurgy and Materials 2000年第2期14卷 132-134页

作者： Xing Zou Yi Zhang(Applied Science School, University of Science and Technology beijing, beijing 100083, china)(institute of Engineering chemistry and Metallurgy, chinese academy of sciences, beijing 100080, china) Applied Science School University of Science and Technology Beijing Beijing 100083 China institute of Engineering chemistry and Metallurgy Chinese Academy of Sciences Beijing 100080 China

Sodium chromate solubility is determined in the range of NaOH concentrations from 450 to 810 g/L andsolution temperatUres from 30 to 110℃. The optimized conditions to separate sodium chromate from NaOH inleached solution are resolved. It is first found the method to efficiently separate sbdium chromate from NaOH andsodium altuninate in crude sodium chromate. Bench-scale studies on the separating are performed. Finally, goodseparation results are achieved.

关键词： chromate separation clean process

DSC study of cold and heat denaturation of β-lactoglobulin A with urea

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chinese Science Bulletin 1997年第2期42卷 123-127页

作者： WANG Bangning and TAN Fuinstitute of chemistry, chinese academy of sciences, beijing 100080, china institute of chemistry Chinese Academy of Sciences Beijing China

IN the field of thermodynamics of protein solutions, there are two kinds of denaturation induced by temperature changes. One of them is the commonest heat denaturation induced by temperature increasing and accompanied by a heat absorption and an increase of enthalpy and entropy. The other is cold denaturation, predicted by Brandts over thirty years ago: the compact ordered structure of protein molecules in the native state is induced into a

关键词： cold denaturation heat denaturation β-lactoglobulin A urea differential scanning calorimetry.

Cyclic Heating-Annealing and Boltzmann Distribution of Free Energies in a Spin-Glass System

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Communications in Theoretical Physics 2007年第7期48卷 179-182页

作者： ZHOU Hai-Jun institute of Theoretical Physics,the chinese academy of sciences,beijing 100080,china institute of Theoretical Physics the Chinese Academy of Sciences Beijing 100080 China

Ergodicity of a spin-glass is broken at low temperatures;the system is trapped in one of many ergodicconfigurational *** between different ergodic domains are achievable through a *** this experiment is repeated infinite times,all ergodic configurational domains will be visited with frequencesthat decreasing exponentially with their free *** mean free energy density of a spin-glass system on a randomgraph is calculated based on this free energy Boltzmann distribution in the present work,by means of the cavity approach.

关键词： spin-glass ergodicity-broken cavity method

Recent advances in the data analysis method of functional magnetic resonance imaging and its applications in neuroimaging

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Progress in Natural Science:Materials International 2006年第8期16卷 785-795页

作者： TIAN Jie, YANG Lei and HU Jin (institute of Automation, chinese academy of sciences, beijing 100080, china Graduate School of chinese academy of sciences, beijing 100039, china) [a]chinese academy of sciences Institute of Automation Beijing China [b]Graduate School of chinese academy of sciences Beijing China

Functional magnetic resonance imaging (fMRI) has opened a new area to explore the human brain. The fMRI can reveal the deep insights of spatial and temporal changes underlying a broad range of brain function, such as motor, vision, memory and emotion, all of which are helpful in the clinical investigation. In this paper, we introduce some recent-developed algorithms for fMRI signal detection such as model-driven method (general linear model, deconvolution model, non-linear model, etc. ) and data-driven method (principle component analysis, independent component analysis, self-organization mapping, clustered constrained non-negative matrix factorization, etc. ). We also propose several important applications of neuroimaging and point out their shortcomings and future perspectives.

关键词： fMR1 data analysis neuroimaging.

SYNTHESIS AND CHARACTERIZATION OF SILAZANE OLIGOMER CONTAINING 1,1,3,3,5,5-HEXAMETHYLCYCLOTRISILAZANE

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chinese Journal of Polymer Science 2000年第5期18卷 449-452页

作者： Cai-hong Xu Ning Zhou Ze-min Xie Center for Molecular Science, institute of chemistry, chinese academy of sciences, beijing 100080, china chinese Acad Sci Inst Chem Ctr Mol Sci Beijing 100080 Peoples R China

A new silazane oligomer containing cyclotrisilazane was synthesized by KH-catalyzed dehydro-coupling reactions between diphenylsilane and 1,1,3,3,5,5-hexamethylcyclotrisilazane (D-3(N)).

关键词： silazane oligomer diphenylsilane cyclotrisilazane dehydro-coupling reaction

Mass Spectrometric Evidence of Heparin Disaccharides for the Catalytic Characterization of A Novel Endolytic Heparinase

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Acta Biochimica et Biophysica Sinica 2004年第12期36卷 840-844页

作者： Yapeng CHAO1,3, Shaoxiang XIONG2, Xiulan CHENG1, and shijun QIAN1* 1institute of Microbiology, chinese academy of sciences, beijing 100080, china 2Center of Mass Spectrometry, institute of chemistry, chinese academy of sciences, beijing 100080, china 3Graduate School of the chinese academy of sciences, beijing 100039, china institute of Microbiology Chinese Academy of SciencesBeijing 100080 China Graduate School of the chinese academy of sciencesbeijing 100039 China Center of Mass Spectrometry Institute of Chemistry Chinese Academy of SciencesBeijing 100080 China

Heparinase from different sources can eliminate heparin or/and heparan sulfate into various low-molecular weight heparins with different characteristics. Porcine intestinal mucosa heparin was de- graded into a series of oligosaccharides by a novel heparinase from the species Sphingobacterium. Disaccha- ride components from the digests were separated and purified by ultrafiltration and HPLC. Five major peaks appeared as three types according to their retention time. The mass spectrometry of peak I mainly gave the non-sulfated disaccharide with the mass of 379 Da. Peak II and III were indicated as two major monosulfated disaccharides with molecular mass of 417 and 459 Da respectively. Moreover, the peak III represented an N- acetyl disaccharide. Both peak IV and V showed the same mass of 496 Da, hinting that they were disulfate- substituted disaccharides. No trisulfate-substituted disaccharides were detected in the mixture of the heparin digest though they were abundant in the heparin structure. The results revealed that the heparinase might specifically cut the sites with low sulfated domain in heparin.

关键词： electrospray ionization-mass spectrometry heparin disaccharides heparinase high perfor- mance liquid chromatography Sphingobacterium sp.

Special relativity and theory of gravity via maximum symmetry and localization

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Science china Mathematics 2008年第4期51卷 568-603页

作者： GUO HanYing institute of Theoretical Physics chinese academy of sciences beijing 100080 china 1. institute of Theoretical Physics Chinese Academy of Sciences Beijing 100080 China

Like Euclid, Riemann and Lobachevski geometries are on an almost equal footing, based on the principle of relativity of maximum symmetry proposed by Professor Lu Qikeng and the postulate on invariant universal constants c and R, the de Sitter/anti-de Sitter (dS/AdS) special relativity on dS/AdS-space with radius R can be set up on an almost equal footing with Einstein’s special relativity on the Minkowski-space in the case of R→∞.Thus the dS-space is coin-like: a law of inertia in Beltrami atlas with Beltrami time simultaneity for the principle of relativity on one side, and the proper-time simultaneity and a Robertson-Walker-like dS-space with entropy and an accelerated expanding S 3 fitting the cosmological principle on another side.If our universe is asymptotic to the Robertson-Walker-like dS-space of R ? (3/Λ)1/2, it should be slightly closed in O(Λ) with entropy bound S ? 3πc 3 k B /ΛG?. Contrarily, via its asymptotic behavior, it can fix on Beltrami inertial frames without ‘an argument in a circle’ and acts as the origin of inertia.There is a triality of conformal extensions of three kinds of special relativity and their null physics on the projective boundary of a 5-d AdS-space, a null cone modulo projective equivalence [ $ \mathcal{N} $ ] ? ? P (AdS 5). Thus there should be a dS-space on the boundary of S 5 × AdS 5 as a vacuum of supergravity.In the light of Einstein’s ‘Galilean regions’, gravity should be based on the localized principle of relativity of full maximum symmetry with a gauge-like dynamics. Thus, this may lead to the theory of gravity of corresponding local symmetry. A simple model of dS-gravity characterized by a dimensionless constant g ?(ΛG?/3c 3)1/2 ～ 10?61 shows the features on umbilical manifolds of local dS-invariance. Some gravitational effects out of general relativity may play a role as dark matter.The dark universe and its asymptotic behavior may already indicate that the dS special relativity and dS-gravity be the foundati

关键词： special relativity de Sitter invariance gravity local de Sitter invariance umbilical manifold 83A05 83D05 53A35 53B50

POLYMERIZATION OF p-DIETHYNYLBENZENE INITIATED BY Ni(C≡CC_6H_4C≡CH)_2(PPH_3)_2

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chinese Journal of Polymer Science 2001年第3期19卷 303-309页

作者： Mu-jie Yang xiao-wei Zhan Department of Polymer Science and Engineering Zhejiang University Hangzhou 310027, china Present address: institute of chemistry, chinese academy of sciences, beijing 100080, china 浙江大学浙江杭州

Homogeneous polymerization of p-diethynylbenzene initiated by nickel acetylide Ni(C ≡ C C_6H_4 C ≡ CH)_2(PPh_3)_2has been investigated in terms of different solvents, addition agents, atmosphere gases, catalyst concentrations, monomerconcentrations and polymerization temperatures. The yield and catalytic efficiency approach 88% and 11. 1 kg polymer/molNi, respectively, under the optimum conditions: [cat] = 0.01 mol/L, [M] = 1.0 mol/L, NEt_3/cat (mol ratio) = 3～5, 1,4-dioxane/toluene (volume ratio) = 1 and T = 25℃ for 5 h. The polymerization rate equation can be expressed as R_p =k_p[M][cat]~2, where k_p= 0.47 L^2. mol^(-2)·S^(-1) (25℃). The overall polymerization activation energy was found to be203 kJ·mol^(-1). Poly(p-diethynylbenzene) so obtained is soluble in THF, CHCl_3 and toluene with weight-average molecularweights as high as 27, 100 and a rich-trans extended π-conjugated polyene chain structure with pendent groups ofp-C_6H_4C≡CH.

关键词： Polymerization p-Diethynylbenzene Nickel acetylide Catalyst

RADIAL BASIS FUNCTION INTERPOLATION IN SOBOLEV SPACES AND ITS APPLICATIONS

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Journal of Computational Mathematics 2007年第2期25卷 201-210页

作者： Manping Zhang (School of Mathematical sciences,Fudan University,Shanghai 200433,china institute of Computational Mathematics,chinese academy of sciences,beijing 100080,china School of Mathematical sciences Fudan University Shanghai 200433 China institute of Computational Mathematics Chinese Academy of Sciences Beijing 100080 China

In this paper we study the method of interpolation by radial basis functions and give some error estimates in Sobolev space H^k（Ω）（k 〉 1）. With a special kind of radial basis function, we construct a basis in H^k（Ω） and derive a meshless method for solving elliptic partial differential equations. We also propose a method for computing the global data density.

关键词： Sobolev space Radial basis function Global data density Meshless method