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MXene Hybridized Polymer with Enhanced Electromagnetic Energy Harvest for Sensitized Microwave Actuation and Self‑Powered Motion Sensing

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Nano-Micro Letters 2025年第3期17卷 265-279页

作者： Yu‑Ze Wang Yu‑chang Wang Ting‑Ting Liu Quan‑Liang Zhao Chen‑Sha Li Mao‑sheng Cao School of Materials Science and Engineering Beijing Institute of TechnologyBeijing 100081People’s Republic of China School of Materials Science and Engineering Peking UniversityBeijing 100871People’s Republic of China School of Mechanical and Material Engineering North China University of TechnologyBeijing 100144People’s Republic of China Key Laboratory of Functional Inorganic Material Chemistry Ministry of Education of the People’s Republic of ChinaHeilongjiang UniversityHarbin 150080People’s Republic of China

Polymeric microwave actuators combining tissue-like softness with programmablemicrowave-responsive deformation hold great promise for mobile intelligentdevices and bionic soft robots. However, their application is challenged by restricted electromagneticsensitivity and intricate sensing coupling. In this study, a sensitized polymericmicrowave actuator is fabricated by hybridizing a liquid crystal polymer with Ti3C2Tx(MXene). Compared to the initial counterpart, the hybrid polymer exhibits unique spacechargepolarization and interfacial polarization, resulting in significant improvements of230% in the dielectric loss factor and 830% in the apparent efficiency of electromagneticenergy harvest. The sensitized microwave actuation demonstrates as the shortenedresponse time of nearly 10 s, which is merely 13% of that for the initial shape memory polymer. Moreover, the ultra-low content of MXene (upto 0.15 wt%) benefits for maintaining the actuation potential of the hybrid polymer. An innovative self-powered sensing prototype that combinesdriving and piezoelectric polymers is developed, which generates real-time electric potential feedback (open-circuit potential of ~ 3 mV) duringactuation. The polarization-dominant energy conversion mechanism observed in the MXene-polymer hybrid structure furnishes a new approachfor developing efficient electromagnetic dissipative structures and shows potential for advancing polymeric electromagnetic intelligent devices.

关键词： Microwave absorption Electromagnetic response Energy harvest Self-sensing Soft actuator

Constructing 2D bismuth-based heterostructure for highly efficient photocatalytic CO2 reduction

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Tungsten 2025年第1期7卷 71-79页

作者： Ruo-Hang Xu Hao-Yu Jiang Dan-Dan Cui Kun-Rong Du Hong-Run Zhang sheng-Jie Xu Ya-Qi Li Zhi-Zhen Ren Liang Wang Wei-chang Hao Yi Du School of Physics and BUAA-UOW Joint Research Centre Beihang University Shenzhen Institute of Beihang University Centre for Catalysis and Clean Energy School of Environment and Science Griffith University

Reforming carbon dioxide（CO2） into fuels and valuable chemicals using solar energy holds significant potential for emission reduction and addressing energy supply *** recombination of photocarriers remains a major obstacle,however,to enhancing solar energy conversion efficiency in the photocatalytic reaction *** two-dimensional materials,constructing heterogeneous structures has emerged as an effective strategy to enhance the separation of photoexcited carriers by leveraging the internal electric field at the heterogeneous ***,we present a facile strategy for preparing Bi4NbO8Br/Bi2WO6plate-on-plate Z-scheme junctions with a strong internal electric field by in situ *** unique heterostructure facilitates efficient separation and transport of photoexcited charges by harnessing the internal electric field induced by chemical bonding at the lateral ***,the Bi4NbO8Br/Bi2WO6heterostructure exhibits enhanced CO2photoreduction properties,along with a CO yield rate of approximately 35 μmol·g-1·h-1under full light *** work offers novel insights into the synthesis of unique hetero structures intended to enhance the efficiency of photocatalytic CO2reduction.

关键词： Bi4NbO8Br/Bi2WO6 CO2 reduction Heterostructures Photocatalysts

Enhanced subacute ischemic stroke treatment via multistage drug delivery system design for combination therapy

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Science China Chemistry 2025年

作者： Xihan Xu Juan-Juan Li Jiamin Li Hui-Yan Zhang Yilin Qi Bing-Sen Shi Tianqi Li Shan-Shan Su Weitao Zhao chang Chen Zhongying Gong Huiyu Liu Ke-Rang Wang Dong-sheng Guo Xue Xue State Key Laboratory of Medicinal Chemical Biology College of Pharmacy Nankai University College of Chemistry State Key Laboratory of Elemento-Organic Chemistry Key Laboratory of Functional Polymer Materials (Ministry of Education) Frontiers Science Center for New Organic Matter Collaborative Innovation Center of Chemical Science and EngineeringNankai University College of Chemistry and Materials Science State Key Laboratory of New Pharmaceutical Preparations and Excipients Key Laboratory of Medicinal Chemistry and Molecular Diagnosis (Ministry of Education) Key Laboratory of Chemical Biology of Hebei Province Hebei Research Center of the Basic Discipline of Synthetic Chemistry Hebei University Department of Neurology Tianjin First Central Hospital School of Medicine Nankai University Beijing Advanced Innovation Center for Soft Matter Science and Engineering State Key Laboratory of Organic-Inorganic Composites Beijing Laboratory of Biomedical Materials Bionanomaterials & Translational Engineering Laboratory Beijing Key Laboratory of BioprocessBeijing University of Chemical Technology

The management of acute ischemic stroke remains challenging due to its abrupt onset and the narrow treatment window,resulting in high rates of disability and *** therapy for neuroprotection and neurorepair strategies provided new hopes for subacute stroke *** we designed a multistage nanodelivery system that matches the unique microenvironment of the subacute phase of stroke,which utilizes calixarene as a building block to effectively load the neuroprotective drug *** calixarene is designed with glycosidic linkages targeting the glucose transporter 1 (GLUT1)on the blood-brain barrier (BBB) and azo bonds that are responsive to hypoxic ***,the decomposed calixarene molecules themselves possess intrinsic bio-activation to modulate inflammatory responses,achieving a multistage therapeutic approach that transitions from targeting to release and finally to *** approach combines anti-inflammation and neuroprotection,providing a multi-level treatment *** system was validated in a rat model of permanent middle cerebral artery occlusion (pMCAO),demonstrating that intravenous administration of the nanodelivery system repairs brain damage and improves motor function 24 h post-pMCAO *** work offers a precise and integrative strategy for stroke patients missing the acute therapy window to improve functional recovery and enhance the effect of comprehensive treatment.

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Quercetin inhibits truncated isoform of dopamine-and cAMP-regulated phosphoprotein as adjuvant treatment for trastuzumab therapy resistance in HER2-positive breast cancer

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Food Science and Human Wellness 2024年第5期13卷 2653-2667页

作者： Han-sheng chang Tzu-Chun Cheng Shih-Hsin Tu Chih-hsiung Wu You-Cheng Liao Jungshan chang Min-hsiung Pan Li-Ching Chen Yuan-Soon Ho Department of Biological Science&Technology College of Life SciencesChina Medical UniversityTaichung 406TaiwanChina Institute of Biochemistry and Molecular Biology College of Life SciencesChina Medical UniversityTaichung 406TaiwanChina Department of Surgery School of MedicineCollege of MedicineTaipei Medical UniversityTaipei 110TaiwanChina Department of Surgery Taipei Medical University HospitalTaipei 110TaiwanChina Graduate Institute of Medical Sciences College of MedicineTaipei Medical UniversityTaipei 110TaiwanChina Institute of Food Sciences and Technology National Taiwan UniversityTaipei 106TaiwanChina

Trastuzumab resistance is one of the causes of poor prognosis in patients with human epidermal growth factor receptor 2(HER2)-positive(HER2+)breast cancer(BC).The truncated isoform of dopamine-and cAMPregulated phosphoprotein(t-DARPP)has been reported to be involved in trastuzumab therapy resistance and promoting tumor *** evaluate the t-DARPP expression in BC,paired tumors and surrounding normal tissues were analyzed by real-time polymerase chain reaction and confirmed higher DARPP-32 kDa family mRNA expression in HER2+BC tumor *** established 2 patient-derived xenografts(PDX)mice models to test the efficacy of trastuzumab,named model 1(non-responder)and model 2(responder).t-DARPP and p95-HER2 protein-protein interactions were detected in PDX tumor tissue from non-responders using Förster resonance energy transfer ***,there is no response from the ***,mechanistic studies using transwell and western blot assays demonstrated that t-DARPP could upregulate epithelial-mesenchymal transition signaling proteins,enhance p95-HER2 expression and promote cell *** found that quercetin effectively reduced t-DARPP expression in HER2+BC *** t-DARPP ShRNA-suppressed cells,quercetin synergistically enhanced trastuzumab-induced apoptotic cell death and G2/M phase *** conclusion,the combination of quercetin and trastuzumab treatment by targeting t-DARPP in HER2+BC patients has the potential as a biomarker for mitigating drug resistance.

关键词： p95-Human epidermal growth factor receptor 2 (HER2) HER2-positive breast cancer Quercetin Trastuzumab resistance Truncated isoform of dopamine-and cAMPregulated phosphoprotein

AN APPROXIMATION SCHEME FOR BLACK-SCHOLES EQUATIONS WITH DELAYS

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Journal of Systems Science & Complexity 2010年第3期23卷 438-455页

作者： Mou-hsiung chang Tao PANG Moustapha PEMY Mathematics Division US Army Research Office P. O. Box 12211 RTP NC 27709 USA Department of Mathematics North Carolina State University Raleigh NC 27695 USA Department of Mathematics Towson University Towson MD 21252 USA

This paper addresses a finite difference approximation for an infinite dimensional Black-Scholesequation obtained by chang and Youree (2007).The equation arises from a consideration ofan European option pricing problem in a market in which stock prices and the riskless asset prices havehereditary *** a general condition on the payoff function of the option,it is shown thatthe pricing function is the unique viscosity solution of the infinite dimensional Black-Scholes *** addition,a finite difference approximation of the viscosity solution is provided and the convergenceresults are proved.

关键词： Black-Scholes equation finite difference stochastic functional differential equations viscosity solutions.

Seismic performance of an existing bridge with scoured caisson foundation

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Earthquake Engineering and Engineering Vibration 2014年第S1期13卷 151-165页

作者： Kuo-Chun chang Yu-Chi Sung Kuang-Yen Liu Ping-hsiung Wang Zheng-Kuan Lee Lu-sheng Lee Witarto Department of Civil Engineering Taiwan University (NTU) Professor Department of Civil Engineering Taipei University of Technology (NTUT) Center for Research on Earthquake Engineering (NCREE) Associate Researcher Associate Technologist Technologist Department of Civil Engineering The University of Houston Ph.D Student

This paper presents in-situ seismic performance tests of a bridge before its demolition due to accumulated scouring problem. The tests were conducted on three single columns and one caisson-type foundation. The three single columns were 1.8 m in diameter,reinforced by 30-D32 longitudinal reinforcements and laterally hooped by D16 reinforcements with spacing of 20 cm. The column height is 9.54 m,10.59 m and 10.37 m for Column P2,P3,and P4,respectively. Column P2 had no exposed foundation and was subjected to pseudo-dynamic tests with peak ground acceleration of 0.32 g first,followed by one cyclic loading test. Column P3 was the benchmark specimen with exposed length of 1.2 m on its foundation. The exposed length for Column P4 was excavated to 4 m,approximately 1/3 of the foundation length,to study the effect of the scouring problem to the column performance. Both Column P3 and Column P4 were subjected to cyclic loading tests. Based on the test results,due to the large dimension of the caisson foundation and the well graded gravel soil type that provided large lateral resistance,the seismic performance among the three columns had only minor differences. Lateral push tests were also conducted on the caisson foundation at Column P5. The caisson was 12 m long and had circular cross-sections whose diameters were 5 m in the upper portion and 4 m in the lower portion. An analytical model to simulate the test results was developed in the OpenSees platform. The analytical model comprised nonlinear flexural elements as well as nonlinear soil springs. The analytical results closely followed the experimental test results. A parametric study to predict the behavior of the bridge column with different ground motions and different levels of scouring on the foundation are also discussed.

关键词： Analytical models Cyclic loads Hydraulic structures Piles Pressure vessels Reinforcement Seismic waves Seismology Soil structure interactions Soils Textile scouring Underwater foundations

Tetra-detector size exclusion chromatography characterization of molecular and solution properties of soluble microbial polysaccharides from an anaerobic membrane bioreactor

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Frontiers of Environmental Science & Engineering 2017年第2期11卷 165-174页

作者： Qingbin Guo sheng chang School of Engineering University of Guelph Guelph Ontario N 1G 2W1 Canada

Characterization of the molecular properties of soluble microbial products （SMP） is critical for understanding the membrane filtration and fouling mechanisms in anaerobic and aerobic membrane bioreactors （AnMBR ＆ MBR）. In this study, the distributions of the absolute molecular weight and intrinsic viscosity of SMP polysaccharides from an AnMBR were effectively determined by a high pertbrmance size exclusion chromatography （HPSEC） that was coupled with the refractive index （RI）,cliode array UV （DAUV）, right and low angle light scattering （LS）, and viscometer （Vis） detectors. Based on the tetra-detector HPSEC determined absolute molecular weights and intrinsic viscosity, a universal calibration relationship for the SMP polysaccharides was developed and the molecularconformations, average molecular weights~ and hydrodynamic sizes of the SMP polysaccharides were also explored. Two factors which can be derived from the tetra-detector HPSEC analysis were proposed for the characterization of the viscous and osmotic pressure properties of the SMP polysaccharides. In addition, it was also extrapolated how to analyze the resistance characteristics of the concentration polarization layers formed in membrane filtration based on the molecular properties determined by the tetra-detector HPSEC analysis.

关键词： Soluble microbial productExtracellular polymeric substanceMembrane bioreactorMembrane foulingMolecular weightIntrinsic viscosity

Effects of Doped Elements on Electrochemical Performance of Ni(OH)_2 Materials

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Chemical Research in Chinese Universities 2007年第4期23卷 452-455页

作者： LEE chang-sheng School of Chemical Engineering and Technology Tianjin University

High energy ball milling （HEBM） method was applied to synthesize Ni （OH）2 with different doped elements sub-stitution for Ni^2＋. The morphology, structure and electrochemical behavior of prepared powders were studied. The re-suits reveal that all the synthesized Ni（OH）2 particles were in sub-micron sizes and greatly agglomerated. Co-, Mg-,Fe- or Mn-doped Ni （OH） 2 was of β-phase with 0.400-0.500 nm crystal interlayer distance, while A1- and Zn-doped products displayed a-phase with larger crystal interlayer spaces. The electrochemical mechanisms of synthe-sized Ni（OH）2 electrodes were discussed by EIS spectra. The specific capacity of Co-doped Ni （OH）2 is 245 mA·h · g^-1, i. e. , 60 mA· h · g^-1 higher than that of Al-doped electrode, which has the highest discharging plat-form of a mid-voltage of 1.30 V.

关键词： Nickel hydroxide High energy ball milling method Metallic ion adulteration Electrochemical discharging capacity

Phase field simulation of single bubble behavior under an electric field

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Chinese Physics B 2018年第9期27卷 389-395页

作者： chang-sheng Zhu Dan Han sheng Xu School of Computer and Communication Lanzhou University of Technology State Key Laboratory of Gansu Advanced Processing and Recycling of Non-Ferrous Metal Lanzhou University of Technology

Based on the Cahn-Hilliard phase field model, a three-dimensional multiple-field coupling model for simulating the motion characteristics of a rising bubble in a liquid is established in a gas-liquid two-phase flow. The gas-liquid interface motion is simulated by using a phase-field method, and the effect of the electric field intensity on bubble dynamics is studied without electric field, or with vertical electric field or horizontal electric field. Through the coupling effect of electric field and flow field, the deformation of a single rising bubble and the formation of wake vortices under the action of gravity and electric field force are studied in detail. The correctness of the results is verified by mass conservation, and the influences of different electric field directions and different voltages on the movement of bubbles in liquid are considered. The results show that the ratio of the length to axis is proportional to the strength of the electric field when the air bubble is stretched into an ellipsoid along the electric field line under the action of electrostatic gravity and surface tension. In addition, the bubble rising speed is affected by the electric field, the vertical electric field accelerates the bubble rise, and the horizontal direction slows it down.

关键词： electro-hydro dynamics numerical simulation phase field method bubble